• Title/Summary/Keyword: Matrix Crack

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치과용 주조합금의 주조방법에 따른 부식거동 (Corrosion Behavior of Dental Alloys Cast by Various Casting Methods)

  • 최한철;고영무
    • 한국표면공학회지
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    • 제37권5호
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    • pp.296-300
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    • 2004
  • The defects of partial denture frameworks are mainly shrinkage porosity, inclusions, micro-crack, particles from investment, and dendritic structure. In order to investigate a good casting condition of partial denture frameworks, the three casting alloys and casting methods were used and detected casting defects were analyzed by using electrochemical methods. Three casting alloys (63Co-27Cr-5.5Mo, 63Ni-16Cr, 63Co-30Cr-5Mo) were prepared for fabricating partial denture frameworks with various casting methods; centrifugal casting (Kerr, USA), high frequency induction casting (Jelenko Eagle, USA), vacuum pressure casting (Bego, Germany). The casting temperature was $1,380^{\circ}C$ (63Co-27Cr-5.5Mo and 63Ni-16Cr) and $1,420^{\circ}C$ (63Co-30Cr-5Mo). The casting morphologies were analyzed using FE-SEM and EDX. The corrosion test of the dendritic structure was performed through potentiodynamic method in 0.9% NaCl solutions at $36.5^{\circ}C$ and corrosion surface was observed using SEM. The defects of partial denture frameworks improved in the order of centrifugal casting, high frequency induction casting, and vacuum pressure casting method, especially, pore defects were found at part of clasp in the case of centrifugal casting method. The structure of casting showed dendritic structure for three casting alloys. In the 63Co-27Cr-5.5Mo and 63Co-30Cr-5Mo, $\alpha$-Co and $\varepsilon$-Co phases were identified at matrix and $${\gamma}$-Ni_2$Cr second phase were shown in 63Ni-16Cr. Also, the corrosion resistance of cast structure increased in the order of vacuum pressure casting, high frequency induction casting, and centrifugal casting method.

Mechanical properties and failure mechanisms of sandstone with pyrite concretions under uniaxial compression

  • Chen, Shao J.;Ren, Meng Z.;Wang, Feng;Yin, Da W.;Chen, Deng H.
    • Geomechanics and Engineering
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    • 제22권5호
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    • pp.385-396
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    • 2020
  • A uniaxial compression test was performed to analyse the mechanical properties and macroscale and mesoscale failure mechanisms of sandstone with pyrite concretions. The effect of the pyrite concretions on the evolution of macroscale cracks in the sandstone was further investigated through numerical simulations with Particle Flow Code in 2D (PFC2D). The results revealed that pyrite concretions substantially influence the mechanical properties and macroscale and mesoscale failure characteristics of sandstone. During the initial loading stage, significant stress concentrations occurred around the edges of the pyrite concretion accompanied by the preferential generation of cracks. Meanwhile, the events and cumulative energy counts of the acoustic emission (AE) signal increased rapidly because of friction sliding between the concretion and sandstone matrix. As the axial stress increased, the degree of the stress concentration remained relatively unchanged around the edges of the concretions. The cracks continued growing rapidly around the edges of the concretions and gradually expanded toward the centre of the sample. During this stage, the AE events and cumulative energy counts increased quite slowly. As the axial stress approached the peak strength of the sandstone, the cracks that developed around the edges of the concretion started to merge with cracks that propagated at the top-left and bottom-right corners of the sample. This crack evolution ultimately resulted in the shear failure of the sandstone sample around the edges of the pyrite concretions.

슬러리형 셀룰로오즈 파이버를 혼입한 시멘트 모르타르의 강도 특성 (Strength Properties of Cement Mortar with Slurry-Typed Cellulous Fiber)

  • 류화성;신상헌;권성준
    • 한국건설순환자원학회논문집
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    • 제7권3호
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    • pp.210-215
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    • 2019
  • 비표면적이 큰 콘크리트 구조체의 균열의 경우 재료적인 거동(수화열 및 건조수축)으로 균열이 발생하기 쉽다. 최근 들어 섬유를 혼입함으로서 콘크리트의 강도 및 균열 저항성 개선에 대한 많은 연구가 진행 중인데 주로 압축강도 개선보다는 인장강도 개선을 통하여 재료적 균열에 대한 저항을 높이는 연구에 집중되고 있다. 본 연구에서는 셀룰로오즈 섬유를 슬러리형으로 제조하여 이를 혼입한 시멘트 모르타르의 작업성, 압축강도 및 휨강도를 평가하였으며, SEM 측정을 통하여 섬유재의 뽑힘특성을 평가하였다. CF 혼입률을 $0.5kg/m^3{\sim}1.0kg/m^3$으로 혼입할 경우, 휨강도를 크게 향상 시킬 수 있으며, 일반 플라스틱 섬유재와 달리 뽑힘 시 충분한 조도를 가지고 있음이 관측되었다.

열습환경을 고려한 핀 체결부 복합재 파괴거동 (Failure Behavior of Pin-jointed Composites under Hygrothermal Environments)

  • 김찬규;황영은;윤성호
    • 한국추진공학회지
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    • 제17권2호
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    • pp.31-38
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    • 2013
  • 본 연구에서는 열습환경에 노출된 탄소섬유/에폭시 복합재의 핀 체결부에 대해 핀 하중시험을 수행하고 수집된 음향방출신호를 분석하여 열습환경이 복합재 핀 체결부의 파괴거동에 미치는 영향을 조사하였다. 이때 시편은 환경조건에 노출되기 전의 시편(Base), 상온침수환경에 노출된 시편(RT), 고온침수 환경에 노출된 시편(HT)으로 구분하였다. 연구결과에 의하면 RT 시편과 HT 시편의 베어링 강도는 Base 시편에 비해 각각 2.2%와 13% 감소하였다. 음향방출신호의 경우 시편 종류에 따라 파손이 가속화되는 시점이 달라짐을 나타내었으며 RT 시편과 HT 시편은 Base 시편에 비해 모재균열에 의한 이벤트가 감소하는 경향이 나타났다. 이로 미루어 판단하면 열습환경은 복합재 핀 체결부의 음향방출신호뿐 아니라 계면특성의 저하도 초래함을 알 수 있었다.

EVA, EVCL 분말수지와 플라이애시를 혼입한 시멘트 모르타르의 고온특성 (High Temperature Properties of Cement Mortar Using EVA, EVCL Redispersible Polymer Powder and Fly Ash)

  • 송훈;신현욱
    • 한국건설순환자원학회논문집
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    • 제6권4호
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    • pp.365-372
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    • 2018
  • 건축물에서의 3D 프린팅은 구조재 및 비구조재로의 적용으로 구분되며, 비구조재는 내 외장 패널이나 조형물로의 적용 등이 주를 이룬다. 연속적으로 적층하여 제조하는 3D 프린팅 방식은 시멘트 모르타르의 경화속도나 특성을 개질하며 이를 위한 재료의 혼입과 경화속도나 시공성, 접착성의 개선을 위한 시멘트 혼화용 폴리머의 사용이 필수적이다. 본 연구는 적층방식 3D 프린팅 적용을 위해 시멘트, 플라이애시, EVA 및 EVCL 분말수지의 혼입률을 달리하여 고온에서의 특성을 검토하였고 혼입에 따른 유효성 여부를 확인하였다. 실험결과, EVA 및 EVCL 분말수지에 혼입에 따라 시멘트 모르타르는 연행된 공기에 의해 특성이 개질되었고 EVA보다는 EVCL을 혼입한 시험체가 고온에서 유리하였다.

(Mg + Al2Ca)로 개량된 AA7075 합금의 미세조직, 기계적 특성, 그리고 고주기 피로 특성에 미치는 T6 및 T73 열처리의 효과 (Effect of T6 and T73 Heat Treatments on Microstructure, Mechanical Responses and High Cycle Fatigue Properties of AA7075 Alloy Modified with Mg and Al2Ca)

  • 황유진;김관영;김규식;김세광;윤영옥;이기안
    • 소성∙가공
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    • 제30권1호
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    • pp.5-15
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    • 2021
  • The effects of heat treatments (T6 and T73) on the microstructure, mechanical properties, and high cycle fatigue behavior of modified AA7075 alloys were investigated. A modified 7075 alloy was manufactured using modified-Mg (Mg-Al2Ca) instead of the conventional element Mg. Based on the microstructure, the average grain size was 4.5 ㎛ (T6) and 5.2 ㎛ (T73). Regardless of heat treatment, the modified AA7075 alloys consisted of Al matrix containing homogeneously distributed Al2CuMg and MgZn2 phases with reduced Fe-intermetallic compound. Room temperature tensile tests showed that the properties of modified 7075-T6 (Y.S.: 622MPa, T.S: 675MPa, elongation: 15.4%) were superior to those of T73 alloy (Y.S.: 492MPa, T.S: 548MPa, elongation: 12.8%). Experimental data show that the fatigue life of T6 was 400 MPa, about 64% of its yield strength. However, the fatigue life of T73 alloy was 330 MPa and 67%. Irrespective of the stress level, all crack initiation points were located on the specimen surface, and no inclusions acting as stress concentrators were seen. Superior mechanical properties and high cycle fatigue behavior of modified AA7075-T6 alloy are attributed to the fine grains and homogeneous distribution of small second phases such as MgZn2 and Al2CuMg, in addition to reduced Fe-intermetallic compounds.

일방향 및 평직 CF/Mg 복합재 적층판의 부식에 따른 미세조직 및 기계적 특성 변화 (Microstructure and Mechanical Property Changes of Unidirectional and Plain Woven CF/Mg Composite Laminates after Corrosion)

  • 임시온;이정무;이상관;박용호;박익민
    • 대한금속재료학회지
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    • 제50권9호
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    • pp.697-702
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    • 2012
  • In this study, unidirectional and plain woven carbon fiber reinforced magnesium matrix composite laminates were fabricated by the liquid pressing infiltration process, and evolutions of the microstructure and compressive strength of the composite laminates under corrosion were investigated by static immersion tests. In the case of the unidirectional composite laminate, the main microstructural damage during immersion appeared as a form of corrosion induced cracks, which were formed at both CF/Mg interfaces and the interfaces between layers. On the otherhand, wrap/fill interface cracks were mainly formed in the plain woven composite laminate, without any cracks at the CF/Mg interface. The formation of these cracks was considered to be associated with internal thermal residual stress, which was generated during cooling after the fabrication process of these materials. As a consequence of the corrosion induced cracks, the thickness of both laminates increased in directions vertical to the fibers with increasing immersion time. With increasing immersion time, the compressive strengths of both composite laminates also decreased continuously. It was found that the plain woven composite laminates have superior corrosion resistance and stability under a corrosive condition than unidirectional laminates.

철계 반비정질 합금 분말과 VC 분말을 고에너지 전자빔으로 투사하여 제조된 표면복합재료의 미세조직, 경도, 파괴인성 (Microstructure, Hardness, and Fracture Toughness of Surface Composites Fabricated by High-Energy Electron-Beam Irradiation of Fe-Based Metamorphic Alloy Powders and VC Powders)

  • 남덕현;도정현;이성학
    • 대한금속재료학회지
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    • 제46권10호
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    • pp.634-645
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    • 2008
  • In this study, surface composites were fabricated with Fe-based amorphous alloy powders and VC powders by high-energy electron beam irradiation, and the correlation of their microstructure with hardness and fracture toughness was investigated. Mixture of Fe-based metamorphic powders and VC powders were deposited on a plain carbon steel substrate, and then electron beam was irradiated on these powders without flux to fabricate surface composites. The composite layers of 1.3~1.8 mm in thickness were homogeneously formed without defects and contained a large amount (up to 47 vol.%) of hard $Cr_2B$ and $V_8C_7$ crystalline particles precipitated in the solidification cell region and austenite matrix, respectively. The hardness of the surface composites was directly influenced by hard $Cr_2B$ and $V_8C_7$ particles, and thus was about 2 to 4 times greater than that of the steel substrate. Observation of the microfracture process and measurement of fracture toughness of the surface composites indicated that the fracture toughness increased with increasing additional volume fraction of $V_8C_7$ particles because $V_8C_7$ particles effectively played a role in blocking the crack propagation along the solidification cell region heavily populated with $Cr_2B$ particles. Particularly in the surface composite fabricated with Fe-based metamorphic powders and 30 % of VC powders, the hardness and fracture toughness were twice higher than those of the surface composite fabricated without mixing of VC powders.

생체정보 진단을 위한 생체모사 계층구조 기반 피부 고점착 전자 패치 개발 (Development of bio-inspired hierarchically-structured skin-adhesive electronic patch for bio-signal monitoring)

  • 김다완
    • 문화기술의 융합
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    • 제8권5호
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    • pp.749-754
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    • 2022
  • 다양한 의료 응용 분야에서 웨어러블 및 피부 부착형 전자 패치에 피부 표면의 높은 접착력과 내수성이 요구된다. 본 연구에서는 탄소 기반 전도성 고분자 복합 소재에 개구리 발바닥의 육각 채널와 문어 빨판의 흡착 구조 패턴을 모사한 신축성 있는 전자 패치를 보고한다. 개구리의 발바닥을 모사한 육각 채널 구조는 수분을 배수하며, 균열억제 효과를 통해 점착력을 향상 시키며, 문어 빨판을 모사한 흡착 구조는 젖은 표면에서 높은 점착력을 나타낸다. 또한 고점착 전자패치는 실리콘(max. 4.06 N/cm2), 피부 복제 표면(max. 1.84 N/cm2) 등 다양한 표면에 건조 및 젖은 조건에서 우수한 접착력을 가지고 있다. 고분자 매트릭스와 탄소 입자를 기반으로한 고분자 복합소재를 통해 제작된 고점착 전자 패치는 건조 및 습한 환경에서 심전도(ECG)을 안정적으로 감지할 수 있다. 이 연구에서 보여진 특성을 기반으로 제안된 전자 패치는 다양한 생체 신호의 진단을 위한 웨어러블 및 피부 부착 센서 디바이스를 구현하는 잠재적 응용 가능성을 제시한다.

건조수축에 따른 균열 억제를 위한 규사 혼입 CLC의 특성 (Properties of CLC using Silica to Suppress Cracking due to Drying Shrinkage)

  • 이창우;이상수
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2021년도 가을 학술논문 발표대회
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    • pp.125-126
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    • 2021
  • In order to improve the housing culture, construction changes for the utilization of diverse and multifunctional spaces are appearing in response to the increasing diverse needs of consumers. Cellular Light-weight Concrete (CLC) is being developed for use in fire-resistant heat-insulating walls and non-bearing walls. However, manufacturing non-uniformity has become a problem as a drawback due to the use of foamed bubbles and normal temperature curing, and additional research is required. Therefore, in order to suppress cracks due to drying shrinkage, silica sand is mixed with CLC to try to understand its characteristics. In the experiment, the compressive strength from 7 to 28 days of age was measured via a constant temperature and humidity chamber, and the drying shrinkage was analyzed according to each condition using a strain gauge. The compressive strength of matrix tends to decrease as the substitution rate of silica sand increases. This is judged by the result derived from the fact that the specific surface area of silica sand is smaller than that of slag. Based on KS F 2701 (ALC block), the compressive strength of 0.6 products is 4.9 MPa or more as a guide, so the maximum replacement rate of silica sand that satisfies this can be seen at 60%. Looking at the change in drying shrinkage for just 7 days, the shrinkage due to temperature change and drying is 0.7 mm, and the possibility of cracking due to shrinkage can be seen, and it seems that continuous improvement and supplementation are needed in the future.

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