• Title/Summary/Keyword: Materials aging

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Effect of Thermal Aging on Intermetallic Compound Growth Kinetics of Au Stud Bump (Au stud 범프의 금속간화합물 성장거동에 미치는 시효처리의 영향)

  • Lim, Gi-Tae;Lee, Jang-Hee;Kim, Byoung-Joon;Lee, Ki-Wook;Lee, Min-Jae;Joo, Young-Chang;Park, Young-Bae
    • Korean Journal of Materials Research
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    • v.18 no.1
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    • pp.45-50
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    • 2008
  • Microstructural evolution and the intermetallic compound (IMC) growth kinetics in an Au stud bump were studied via isothermal aging at 120, 150, and $180^{\circ}C$ for 300hrs. The $AlAu_4$ phase was observed in an Al pad/Au stud interface, and its thickness was kept constant during the aging treatment. AuSn, $AuSn_2,\;and\;AuSn_4$ phases formed at interface between the Au stud and Sn. $AuSn_2,\;AuSn_2/AuSn_4$, and AuSn phases dominantly grew as the aging time increased at $120^{\circ}C,\;150^{\circ}C,\;and\;180^{\circ}C$, respectively, while $(Au,Cu)_6Sn_5/Cu_3Sn$ phases formed at Sn/Cu interface with a negligible growth rate. Kirkendall voids formed at $AlAu_4/Au$, Au/Au-Sn IMC, and $Cu_3Sn/Cu$ interfaces and propagated continuously as the time increased. The apparent activation energy for the overall growth of the Au-Sn IMC was estimated to be 1.04 eV.

The Influence of Aging Treatment on the Mechanical and Electrical Properties of Cu-Be Alloy (시효 열처리에 따른 Cu-Be 합금의 전기.기계적 특성 고찰)

  • Ryou, Min;Lee, Byoung-Soo;Jeong, Bong-Yong;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.31 no.6
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    • pp.366-370
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    • 2011
  • The influence of aging treatment on the microstructure, mechanical and electrical properties of Cu-Be alloy for connector material applications was investigated. The properties of mechanical strength and electrical conductivity were found to increase with increasing aging temperature. By the way, SEM/EDS and TEM analysis exhibited that beryllides precipitation (CoBe and NiBe) with a size of 50 nm were distributed in grains. It was, therefore concluded that these beryllide precipitates improved the mechanical strength and also it was favor in increasing of electrical conductivity.

Cryogenic Fracture Toughness Evaluation for Austenitic Stainless Steels by Means of Unloading Compliance Method

  • Yu, Hyo-Sun;Kwon, Il-Hyun
    • Journal of Mechanical Science and Technology
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    • v.15 no.1
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    • pp.26-34
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    • 2001
  • Most research to date concerning the cryogenic toughness of austenitic stainless steels has concentrated on the base metal and weld metal in weldments. The most severe problem faced on the conventional austenitic stainless steel is the thermal aging degradation such as sensitization and carbide induced embrittlement. In this paper, we investigate the cryogenic toughness degradation which can be occurred for austenitic stainless in welding. The test materials are austenitic stainless JN1, JJ1 and JK2 steels, which are materials recently developed for use in nuclear fusion apparatus at cryogenic temperature. The small punch(SP) test was conducted to detect similar isothermally aging condition with material degradation occurred in service welding. The single-specimen unloading compliance method was used to determine toughness degradation caused by thermal aging for austenitic stainless steels. In addition, we have investigated size effect on fracture toughness by using 20% side-grooved 0.5TCT specimens.

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Long-Term Aging Diagnosis of Rotor Steel Using Acoustic Nonlinearity

  • Kim, Chung-Seok;Park, Ik-Keun;Jhang, Kyung-Young;Hyun, Chang-Yong
    • Journal of the Korean Society for Nondestructive Testing
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    • v.31 no.6
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    • pp.642-649
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    • 2011
  • The long-term aging of ferritic 2.25CrMo steel was characterized using the acoustic nonlinear effect in order to apply to diagnose the degradation behavior of structural materials. We measured the acoustic nonlinearity parameter for each thermally aged specimen by the higher harmonic-generation technique. The acoustic nonlinearity parameter increased with aging time due to equilibrium M6C carbide precipitation, and has a favorable linear relation with Rockwell hardness. This study suggests that acoustic nonlinearity testing may be applicable to diagnostics on strength degradation in rotor steels.

Approach of Antiaging Care in Cosmetics (항노화 화장품 연구 개발 동향)

  • Chang, Ih-Seop;Son, Ui-Dong;Hwang, Jae-Seong
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.31 no.3 s.52
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    • pp.213-218
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    • 2005
  • Recently, with the remarkable increase in elderly persons and improvement of skin care technique, the requirements of customer for anti-aging care have become very important. Also, after cosmeceutical-product law was done in 2001, the major interesting field in cosmetic industry has been focused to developing anti-aging materials having safety and efficacy by basic science. In this review, we ill introduce the trend of anti-aging research and materials to prevent wrinkle or improve elasticity of skin.

A study on analyzing the terms describing anti-aging effects in Dongeuibogam to propose the methodology for selecting medicinal herbs related to anti-aging effects (『東醫寶鑑』에 수록된 항노화 효능어와 이에 근거한 항노화 한약재 선별 방법론 연구)

  • Lee, Dong-Woo;Baek, Jin-Ung
    • Journal of Korean Medical classics
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    • v.27 no.2
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    • pp.25-48
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    • 2014
  • Objectives : This study aims to analyze the terms describing anti-aging effects in Dongeuibogam, and to propose the methodology for selecting medicinal herbs related to anti-aging effects. Methods : We considered aging or anti-aging theories by reviewing the major literature in korean medicine or traditional chinese medicine, and then we deduced the concepts describing anti-aging effects and the medicinal herbs for anti-aging effects. We investigated the medicinal herbs based on the terms describing anti-aging effects in Dongeuibogam and drew the methodology for selecting and classifying the medicinal herbs related to anti-aging. Results & Conclusions : The following conclusions could be drawn. 1. A set of causes and signs of aging in Dongeuibogam and a set of therapies for alleviating the aging signs in Chengumikbang, Yanglobongchinseo, and Nolohangeon was found. 2. Anti-aging effects should not be confused with disease treatments. Therefore, we defined the medical terms of anti-aging effects as "the terms expressing the effect of delaying or alleviating the subjective or objective signs of aging concretely". Based upon the terms of anti-aging effects, we defined the medicinal herbs for anti-aging effects as "the medicinal herbs whose effects are described in medical terms expressing the effects of delaying or alleviating the subjective or objective signs of aging concretely". 3. We considered Lycii Fructus, Asparagi Tuber in Dongeuibogam as examples of medicinal herbs whose effects are described in medical terms expressing anti-aging effects. It shows that we can select medicinal herbs for anti-aging effects by comparing the effects of 937 single therapies in Dongeuibogam to the terms describing anti-aging effects defined in this study. Futhermore, the results could be utilized as the basic materials of experimental study on anti-aging.

COLOR STABILITY OF CURRENT PROSTHETIC COMPOSITES UNDER ACCELERATED AGING AND IMMERSION IN A COFFEE SOLUTION

  • Kim, Hyo-Jin;Heo, Seong-Joo;Koak, Jai-Young;Chang, Ik-Tae
    • The Journal of Korean Academy of Prosthodontics
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    • v.40 no.3
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    • pp.225-235
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    • 2002
  • The color stability of current prosthetic composites is unknown, even though the quality of composite materials has been improving. This study examined the intrinsic color stability of various current prosthetic resins (ceramic-polymers) after an accelerated aging process and the extrinsic color stability after immersion in a coffee solution. By comparing the amount of discoloration after aging with that without aging, the effect of the accelerated aging process on external discoloration could be evaluated. Three current prosthetic composites (Artglass, Targis, Sculpture), one light polymerized direct composite (Z100) and one dental porcelain control (Ceramco) were assessed. The color changes (${\Delta}$E) of all the specimens were determined using the CIE $L^{*}a^{*}b^{*}$ color order system with a reflected spectrophotometer. The results were as follows: 1. The prosthetic composite materials subjected to the accelerated aging test showed no significant difference in color changes (p >.05). 2. In the coffee solution immersion test after the aging process, the color changes of the Targis and Artglass groups were not different from that of the Z100 group, which showed the highest color change. 3. In the immersion only test, a significantly high color change was observed in the sculpture glazing group. 4. The aging process influenced on the color changes more in the Targis, Artglass and Z100 groups than in the Sculpture and Ceramco groups.

Effect of Aging Treatment on the Tensile Properties of Mg-Nd-Y-Zr-Zn Casting Alloys (Mg-Nd-Y-Zr-Zn 주조합금의 인장특성에 미치는 시효처리의 영향)

  • Kim, Hyun-Sik;Ye, Dea-Hee;Kang, Min-Cheol;Kim, In-Bea
    • Korean Journal of Materials Research
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    • v.18 no.5
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    • pp.266-271
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    • 2008
  • Magnesium alloys are alloyed with rare earth elements (Re, Ca, Sr) due to the limited use of magnesium in high-temperature conditions. In this study, the influences of Zr and Zn on the aging behavior of a Mg-Nd-Y alloy were investigated. magnesium alloys containing R.E elements require aging treatments Specifically, Nd, Y and Zr are commonly used for high-temperature magnesium alloys. Various aging treatments were conducted at temperatures of 200, 250 and $300^{\circ}C$ for 0.5, 1, 3, 6, and 10 hours in order to examine the microstructural changes and mechanical properties at a high temperature ($150^{\circ}C$). Hardness and high-temperature ($150^{\circ}C$) tensile tests were carried out under various aging conditions in order to investigate the effects of an aging treatment on the mechanical properties of a Mg-3.05Nd-2.06Y-1.13Zr-0.34Zn alloy. The maximum hardness was 67Hv; this was achieved after aging at $250^{\circ}C$ for 3 hours. The maximum tensile, yield strength and elongation at $150^{\circ}C$ were 237MPa, 145MPa and 13.6%, respectively, at $250^{\circ}C$ for 3 hours. The strengths of the Mg-3.05Nd-2.06Y-1.13Zr-0.34Zn alloy increased as the aging time increased to 3 hours at $250^{\circ}C$ This is attributed to the precipitation of a Nd-rich phase, a Zr-rich phase and $Mg_3Y_2Zn_3$.

Effect of Thermal Aging on The Strength of Laminate Composites Structure (라미네이트 강도 특성에 미치는 Thermal Aging의 영향)

  • 정연운;김국진;한중원;김윤해
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.24-28
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    • 2002
  • Composite reinforced fiber materials are used in lots of fields such as a part of aeronautic space, ship, machinery and so on because can make structure wished for necessary condition by control fiber direction and laminated sequence. As the use of advanced composites increase, specific techniques have been developed to repair changed composite structures. In order to repair the damaged part production high quality composite reinforced fiber are completed by control the surrounding temperature and press in autoclave. The quality is influenced heat exposure degree by chemical reaction for precessing. This study considerated influence limit of using by repair structure part and change of properties according to heat exposure degree for repairing.

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Evaluation on the Electrical Properties of Outdoor Epoxy Resin Insulators under Accelerated Agings (가속열화에 따른 옥외용 epoxy 수지 애자의 전기적특성 평가)

  • Cho, H.G.;Kim, I.S.;Ahn, M.S.
    • Proceedings of the KIEE Conference
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    • 1994.07b
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    • pp.1360-1363
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    • 1994
  • Epoxy resin insulator have good electrical properties (high electric strength, high resistivity, low dielectric loss) in addition to high mechanical strength, small dimensions and design versatility. Polymer insulator, however, are subjected to aging processes, caused by the surrounding atmosphere, which may lead to degradation of their properties. This paper describes the results of a important study on the artificial pollution test, Weather-Ometer properties and rotating wheel dip test of high voltage different aging insulators which are the most important factors for outdoor uses. Also, the objects of this paper are to (a)result of insulator under dry(wet) flashover voltage, (b)artificial pollution test of salt spay, (c)Accelerated aging test of Weather-Ometer, (d) wet and dry flashover voltage under rotating wheel dip test.

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