• 한국자기학회:학술대회 개요집
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• 한국자기학회 2013년도 임시총회 및 하계학술연구발표회
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• pp.15-16
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• 2013

Magnetization behavior of ultra thin $Fe_xCo_{1-x}$ alloy (where x varies from 0 to 100) has been investigated as functions of composition on Cr (100) substrate by using in situ surface magneto optical Kerr effect (SMOKE). It's always show in plane uniaxial magnetic anisotropy at room temperature (RT) & Low temperature (LT). It is observed that composition dependent coercive force maximum at about 30 at % Co and 70 at % Co atomic ratio and minimum near equiatomic site. The relative magnetic moments as composition variation also show magnetization collapse near equiatomic site. The magnetization behaviors of Fe-Co alloy on Cr (100) due to composition varies are supported the order-disordering as well as structural stability bcc (ferromagnetic)/fcc (anti-ferromagnetic) phase stability magnetism.

• Journal of Electrical Engineering and Technology
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• 제10권1호
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• pp.325-330
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• 2015

With approval from the Asia Pacific Metrology Program Working Group on Materials Metrology (APMP WGMM), an international comparison for sheet resistance standards for silicon wafers was firstly conducted among Korea Research Institute of Standards and Science (KRISS) in Korea, CMS/ITRI in Taiwan, and NIM in China, which are national metrology institutes (NMIs), from August 2011 to January 2012. The sheet resistance values of the standards are $10{\Omega}$, $100{\Omega}$, and $1000{\Omega}$; the measurement was conducted in sequence at KRISS, CMS/ITRI, NIM, and KRISS again using the four-point probe method with single and dual configuration techniques. The reference value for the measurement results of the three NMIs was obtained through averaging the values of the three results for each sheet resistance range. The differences between the reference value and the measured values is within 0.22% for $10{\Omega}$, 0.17% for $100{\Omega}$, and 0.12% for $1000{\Omega}$. Therefore, the international consistency for conducting sheet resistance measurements is confirmed within 0.22% through the APMP WGMM approved comparison.

• Journal of Magnetics
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• 제16권3호
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• pp.225-228
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• 2011

Magnetic properties and Rockwell hardness of 1Cr-0.5Mo steel have been investigated as a function of isothermal aging time. Our results showed that coercivity, hysteresis loss and Rockwell hardness in the aged samples decreased as aging time increased. This phenomenon was analyzed using optical microscopy and scanning electron microscopy. A significant diffusion of Cr and Mo atoms formed $M_2C$ and $M_7C$ carbides, lowering the matrix strength. $M_2C$ and $M_7C$ carbides partially segregated inside grains, diffused into grain boundaries, and finally resulted in a soft ferrite matrix and a hard grain boundary. The magnetic and mechanical softening of the matrix is likely to govern the properties of the sample more than the hardening of the grain boundary by carbide precipitations.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2006년도 추계학술발표회 초록집
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• pp.64-64
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• 2006

• 대한화학회지
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• 제47권1호
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• pp.31-37
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• 2003

측정 및 화학분석에 많이 이용되는 한 점 교정식에 대하여 측정 불확도 표기 지침서(GUM)의 근사법과 Monte-Carlo Simulation에 의해 계산된 각각의 확장불확도를 비교하였다. 이 비교를 위하여 임의의 자료들을 여러 농도 수준에서 정규 분포 또는 t-분포로 가정하여 계산하였다. 나눗셈에 의한 한 점 교정식의 비선형성과 t-분포 형식을 함에 따른 입력량의 과도한 퍼짐으로 인하여, 경우에 따라서, GUM의 근사법으로 계산된 불확도가 Monte-Carlo Simulation에 의해 계산된 것보다 약 50% 이상의 오류가 있다는 것이 확인되었다. 그러나, 검출 하한을 계산하기 위하여 한 점 교정식을 이용하는 경우, 반응량의 표준불확도가 상대적으로 매우 크고 비선형성에 희한 계산 오류가 상대적으로 무시되므로 근사식에 따른 계산 오류가 발생하지 않았다.

• 분석과학
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• 제35권6호
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• pp.249-255
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• 2022

본 연구에서는 기체 크로마토그래피-불꽃이온화검출기(GC-FID)를 이용한 고순도 질소의 새로운 순도분석법을 개발하였다. 고순도 질소에 존재할 수 있는 불순물인 일산화탄소(CO), 이산화탄소(CO₂), 및 메탄(CH₄)에 대한 3 µmol/mol 수준의 인증표준물질(Certified reference material, CRM)을 중량법을 이용하여 제조하였고, 이를 순도분석에 활용하였다. 개발된 순도분석법에서는 운반가스로 초고순도 질소와 순도분석 대상 질소를 사용하여, 제조된 인증표준물질의 기체 크로마토그래피에서 얻어지는 크로마토그램의 면적 값 차이를 비교함으로써 순도분석 대상 질소의 불순물을 정량 분석하였다. 순도분석 대상 질소로는 액체질소 및 제조사가 각기 다른 3곳의 고순도 질소를 사용하였다. 또한, 개발된 순도분석법의 유효성을 평가하기 위하여 순도분석 대상 질소 내 불순물의 물질량 분율을 기존 순도분석법과 비교하였다. 두 가지 순도분석법을 이용하였을 때 대상 질소 내 불순물의 물질량 분율이 불확도 (k = 2) 내에서 서로 일치함을 확인함으로써, 개발된 순도분석법이 유효함을 확인하였다.

• 한국분말재료학회지
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• 제20권2호
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• pp.129-133
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• 2013

In this paper we have studied the effect of water droplet size on nano-particle size distribution using SMPS(Scanning Mobility Particle Sizer)system. It can be seen that the unknown peak at >100 nm was caused by water droplets which did not dry completely when DI water was used as a solvent in the SMPS system. Therefore, it is important to dry water droplets generated from atomizer in the SMPS system when measuring the particle size distribution using less than 100 nm nano-particles in diameter. From this study, It can be concluded that the napion was a useful material as dryer ones and using EAG(Electro Aerosol Generator) as a particle generator was the most effective in reducing the effect of water droplets.

• 열처리공학회지
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• 제12권4호
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• pp.294-302
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• 1999

Evaluation of Brinell standard hardness tester was carried out to secure its application as a national standard for Brinell hardness. Accuracies and reliabilities in load application, indenter diameter and indentation measurement were tested through evaluation of these components. The accuracies of load application for various loading conditions were within the limit of ISO and KS specifications. Errors in the indentation measurement due to the difference in personnel characters were successfully removed by utilising automatic indentation measurement system. In overall, the tester and the indentation measuring system were found to be eligible as a national standard of Brinell hardness.

• Environmental Engineering Research
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• 제13권1호
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• pp.14-18
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• 2008

Photocatalytic oxidations of benzene gas using the closed system (batch reactor) were induced to determine its by-products and investigate the effect of humidity and oxygen concentration on their generation. The study was able to identify 11 gaseous by-products: 2-methylpropene, acetaldehyde, acetone, pentane, methylcyclobutane, methylcyclopentane, cyclohexane, 2,3-dimethylbutane, 2-methylpentane, 3-methylpentane, and hexane. All the by-products were saturated hydrocarbons, which are less toxic than benzene and were probably formed through hydrogenation reaction on the photocatalytic surface. The photocatalytic oxidation of benzene under higher humidity produced less by-products. However, the amount of acetone released increased with higher humidity and oxygen concentration.

• 열처리공학회지
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• 제14권5호
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• pp.275-281
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• 2001

To improve the reliability of hardness test results, Rockwell hardness round robin test was carried out for 10 laboratories. The test condition was the same with the ISO(International Standards Organization) standards. Korea Research Institute of Standards and Science(KRISS) supplied the hardness standard blocks and an indenter to laboratories for the measurement. The participating laboratories measured hardness of the specified areas on the blocks for 6 times with their own indenter as well as common indenter, respectively, and reported the results to KRISS. The result showed that quite large amount of the differences came from the indenter and it is necessary to change indenter with better quality for improved reliability in hardness measurement.