• Title/Summary/Keyword: Material separation

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Transmission Electron Microscopy Study of Stacking Fault Pyramids Formed in Multiple Oxygen Implanted Silicon-on-Insulator Material

  • Park, Ju-Cheol;Lee, June-Dong;Krause, Steve J.
    • Applied Microscopy
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    • v.42 no.3
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    • pp.151-157
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    • 2012
  • The microstructure of various shapes of stacking fault pyramids (SFPs) formed in multiple implant/anneal Separation by Implanted Oxygen (SIMOX) material were investigated by plan-view and cross-sectional transmission electron microscopy. In the multiple implant/anneal SIMOX, the defects in the top silicon layer are confined at the interface of the buried oxide layer at a density of ${\sim}10^6\;cm^{-2}$. The dominant defects are perfect and imperfect SFPs. The perfect SFPs were formed by the expansion and interaction of four dissociated dislocations on the {111} pyramidal planes. The imperfect SFPs show various shapes of SFPs, including I-, L-, and Y-shapes. The shape of imperfect SFPs may depend on the number of dissociated dislocations bounded to the top of the pyramid and the interaction of Shockley partial dislocations at each edge of {111} pyramidal planes.

Electro-Optical Characterization of Polymer Dispersed Liquid Crystals for Various Concentrations of Prepolymer (전폴리머 조성에 따른 고분자 분산형 액정의 전기 광학 특성 평가)

  • Yang, Kee-Jeong;Yoon, Do-Young
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.23 no.11
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    • pp.891-895
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    • 2010
  • Polymer dispersed liquid crystal (PDLC) films were prepared by the phase separation method using the liquid crystal (E7) and prepolymers. This work investigated the electro-optical characteristics of various PDLC films. In order to have good contrast ratio, the polymer refractive index must be adjusted to the ordinary refractive index of the liquid crystal. The driving voltage of PDLC films were mainly affected by elastic deformation. E7-Ebecryl810-IOA-TMPTA-HMPPO system had good threshold voltage and driving voltage and E7-Ebecryl810-EHA-PEGDA-HMPPO system had good contrast ratio.

Design Characteristics Analysis for Very High Temperature Reactor Components (VHTR 초고온기기 설계특성 분석)

  • Kim, Yong Wan;Kim, Eung Seon
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.12 no.1
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    • pp.85-92
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    • 2016
  • The operating temperature of VHTR components is much higher than that of conventional PWR due to high core outlet temperature of VHTR. Material requirements and technical issues of VHTR reactor components which are mainly dominated by high temperature service condition were discussed. The codification effort for high temperature material and design methodology are explained. The design class for VHTR components are classified as class A or B according to the recent ASME high temperature reactor design code. A separation of thermal boundary and pressure boundary is used for VHTR components as an elevated design solution. Key design characteristics for reactor pressure vessel, control rod, reactor internals, graphite reflector, circulator and intermediate heat exchanger were analysed. Thermo-mechanical analysis of the process heat exchanger, which was manufactured for test, is presented as an analysis example.

Dielectric Characteristics of SF$_6$ Gas in Non-uniform Fields (불평등전계중에서 SF$_6$ 가스의 절연특성)

  • 이복희;전덕규;이경옥;안창환;이창준
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.04a
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    • pp.334-337
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    • 1997
  • This paper describes dielectric characteristics of SF$_{6}$ gas stressed by the non-oscillating and oscillating impulse voltages in inhomogeneous fields disturbed by metallic protrusion. The breakdown voltage-time (V-t) characteristics and breakdown voltage-gas pressure (V-p) characteristics and their characteristics are statistically investigated with positive and negative very fast transient overvoltages. The experiments were carried out using a needle-to-plane gap geometry in the gas pressure ranges from 0.1 to 0.5 MPa. The gap separation gas 22 mm, and the needle-shaped protrusions were made of stainless steel 10 mm in length and 1.0 mm in diameter.r.

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The Correlation between Gas Transport Properties and Physical Properties of Modified Polysulfones (변형 폴리술폰의 기체 투과 성질과 물리적 성질의 상관관계)

  • ;;;;;Guiver, Michael D.;R
    • Proceedings of the Membrane Society of Korea Conference
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    • 1997.10a
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    • pp.67-68
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    • 1997
  • 1. Introduction : Gas transport through dense polymeric membranes is predominantly determined by the chain packing density as well as the chain flexibility. Thus, improved permeation properties can be obtained by controlling these two factors. In this work, the introduction of bulky substituents was attempted to improve permeation properties. Polysulfone, widely used material for gas separation membrane, was the starting material of this modification. Gas transport properties of resulting modified polysulfones were examined, and the improved properties were explained by probing the change of physical properties.

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The Relationship Between the Permeation Rate and the Solubility Parameter for Polyethylene-n-Hexane-Benzene System in Pervaporation (폴리에틸렌-n-헥산-벤젠계에 대한 투과속도와 용해도 파라메타 사이의 관계)

  • Rhim, Ji-Won
    • Membrane Journal
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    • v.3 no.3
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    • pp.136-139
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    • 1993
  • It is well known that the membrane permeation in pervaporation is governed by both the chemical nature of the membrane material and the physical structure of the membrane and also the separation can be achieved by differences in either solubility, size or shape. The solubility of the penerrant in the polymeric membrane can be described qualitively by applying the Hildebrand relation [1] which relates the energy of mixing of the penerrant and the polymer material. Froehling et al. have tried to predict the swelling behavior of polymers for the systems of polyvinylchloride(PVC)-toluene-methanol, PVC-trichloroethylene-nitromethane and PVC-n-butylacetate-nitromethane[2]. The former two systems which do not show the donor/acceptor interactions upon mixing showed the successful results[2]. In addition to this technique, there are several other possible approaches to predict the swelling behaviors of polymers, such as the surface thermodynamic approach[3, 4], the comparison of the membrane polarity with the solvent polarity in terms of Dimroth's solvent polarity value[5].

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Measurement of Plasma Density Generated by a Semiconductor Bridge: Related Input Energy and Electrode Material

  • Kim, Jong-Dae;Jungling, K.C.
    • ETRI Journal
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    • v.17 no.2
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    • pp.11-19
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    • 1995
  • The plasma densities generated from a semiconductor bridge (SCB) device employing a capacitor discharge firing set have been measured by a novel diagnostic technique employing a microwave resonator probe. The spatial resolution of the probe is comparable to the separation between the two wires of the transmission lines (${\approx}$3 mm). This method is superior to Langmuir probes in this application because Langmuir probe measurements are affected by sheath effects, small bridge area, and unknown fraction of multiple ions. Measured electron densities are related to the land material and input energy. Although electron densities in the plasma generated by aluminum or tungsten-land SCB devices show a general tendency to increase steadily with power, at the higher energies, the electron densities generated from tungsten-land SCB devices are found to remain constant.

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The Study on Improvement in Subcooling of TMA Clathrate for PCM in Ice Storage System (빙축열시스템 PCM용 TMA-포접화합물의 과냉도 개선에 대한 연구)

  • Kim, J.H.;Chung, N.K.;Kim, C.O.
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.1663-1666
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    • 2003
  • TMA clathrate that is used by PCM of ice storage system in this research creates hydrate crystallization at higher temperature than pure water, and application is expected as PCM because having comparative big dormant temperature without phase separation phenomenon. In case this research uses TMA clathrate by PCM, choose admixture by purpose to control or remove subcooling of TMA clathrate and evaluated experimentally. Subcooling is improved and can expect contraction of freezing machine running time and increase of coefficient of performance as that add admixture to TMA clathrate conclusively. Also, may supply thermal storage system that apply low temperature potential heat thermal storage material that subcooling is improved more extensively laying stress on medium size building and small size building, can expect allowance through localization of ice storage system.

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Preparation and Characterization of a Surface Renewable Solid State Hg/HgO Reference Electrode Utilizing Gold Amalgam

  • Kim, Won;Park, Jong-Man
    • Bulletin of the Korean Chemical Society
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    • v.28 no.3
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    • pp.439-442
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    • 2007
  • A solid state Hg(Au)/HgO reference electrode was prepared utilizing gold amalgam solid particles. Solid fine powder of the gold amalgam was prepared by chemical reduction of Au(III) with NaBH4 followed by reduction of Hg(II) in the presence of gold fine particles. The solid content in the suspension of the gold amalgam particles and fine mercury oxide particles in DMF containing PVC was precipitated by the addition of a large amount of water to give solid Hg(Au)/HgO/PVC mixture. After drying, the mixture was pressure-molded to a physically stable Hg(Au)/HgO composite reference electrode material. The electrochemical characteristics of the electrode as a reference electrode were very similar to an ordinary Hg/HgO reference electrode. The electrode material can be molded and fabricated in any desired shape and size. The surface can be renewed by a simple polishing process whenever contaminated or deactivated. The applicability of the electrode in the electrochemical detection of carbohydrates after anion exchange separation was evaluated.

Recent Development of Bulk High-Tc Superconductors

  • Yoo, Sang-Im
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.04a
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    • pp.88-95
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    • 2002
  • Recent development in the field of RE-Ba-Cu-O (REBCO, RE: Y or rare earth elements) bulk high-Tc superconductors (HTS) is reviewed in the present paper. After the fatal weak link problem of sintered REBCO superconductors has been overcome by melt processing, this field has been greatly advanced during last ten years. The critical current density $J_c$ at 77 K has been enhanced by introducing effective flux pinning sites into the $REBa_2Cu_3O_y$ (RE123) superconducting matrix. Large melt-textured REBCO bulk crystals have been fabricated with the TSMG(top-seeded melt growth) technique. Mechanical properties of REBCO bulks have been improved by using the Ag additive or epoxy resin. Real bulk applications such as current lead, fault current limiter, flywheel energy storage system, magnetic field source, magnetic separation system, and etc., surely come true near future.

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