• Title/Summary/Keyword: Material dispersion

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WIDEBAND SPECTRAL DISPERSER MADE OF ZnS FOR EXOPLANET CHARACTERIZATION USING SPACE-BORNE TELESCOPES

  • Enya, Keigo;Fujishiro, Naofumi
    • Publications of The Korean Astronomical Society
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    • v.32 no.1
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    • pp.343-345
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    • 2017
  • We present the development of a spectral dispersion device for wideband spectroscopy for which the primary scientific objective is the characterization of transiting exoplanets. The principle of the disperser is simple: a grating is fabricated on the surface of a prism. The direction of the spectral dispersion power of the prism is crossed with the grating. Thus, the prism separates the spectrum into individual orders while the grating produces a spectrum for each order. In this work, ZnS was selected as the material for the cross disperser, which was designed to cover the wavelength region, ${\lambda}=0.6-13{\mu}m$, with a spectral resolving power, $R{\geq}50$. A disperser was fabricated, and an evaluation of its surface was conducted. Two spectrometer designs, one adopting ZnS (${\lambda}=0.6-13{\mu}m$, $R{\geq}300$) and the other adopting CdZnTe (${\lambda}=1-23{\mu}m$, $R{\geq}250$), are presented. The spectrometers, each of which has no moving mechanical parts, consist simply of a disperser, a focusing mirror, and a detector.

Analysis of Hybrid Emulsion Surfaces by the Phase Lag Mapping Atomic Force Microscopy (위상지연 원자간력 현미경법에 의한 혼성 에멀젼 표면의 분석)

  • Han, Sang-Hoon;Kim, Jong-Min;Park, Dong-Won
    • Applied Chemistry for Engineering
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    • v.17 no.4
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    • pp.381-385
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    • 2006
  • We applied a new analyzing technique for the polyurethane acrylate hybrid emulsion sample composed of polyurethane resin and acrylate resin using the phase-lag mapping techniques of atomic force microscopy. For the analysis, we synthesized similarly sized pure polyurethane dispersion and acrylate emulsion particles, which were used for measuring the standard phase-lag intensities for each material. Based on these signal intensity, we could discriminate acryl particle in the polyurethane dispersion matrix with the resolution of a few tens of nanometers. Thus, the techniques show a new possibility in the analysis of the organic two-phase particles, and we believe the techniques are helpful to design organic particles.

Development and Stability Evaluation of Enteric Coated Diclofenac Sodium Tablets Using AquaPolish E.

  • Zaid, A.N.;Fadda, A.M.;Nator, S.;Qaddumi, A.
    • Journal of Pharmaceutical Investigation
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    • v.41 no.4
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    • pp.211-215
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    • 2011
  • The aim of this study was to develop a stable enteric coated diclofenac sodium (DFS) tablets using Aqua-Polish E without using a subcoat. DFS uncoated tablets were manufactured through the non direct compression process. AquaPolish E white aqueous coating dispersion was used as enteric coating material. This film forming polymer is a mixture of selected polymethacrylic/ethylacrylate copolymers. The stability of the obtained enteric coated tablets was evaluated according to ICH guidelines. No signs of disintegration or cracking was observed when they placed in 0.1N HCl solution (pH1.2), but they were completely disintegrated within 10 minutes when they placed in buffered solution at pH6.8. Dissolution test was also conducted by placing tablets in 0.1 N HCl for 2 hours and then 1 hour in phosphate buffer at pH 6.8. Less than 0.9 % of drug was released in the acidic phase and up to 97% in the basic medium. These findings suggest that aqueous enteric coating with AquaPolish E system is an easy and economical approach for preparing stable DFS enteric coat without the use of a subcoating layer.

Electrical Conductivity Behavior of 6FDA-based Fluorinated Polyimide/PMMA-g-MWCNT Nanocomposite Film (6FDA를 포함한 불소계 폴리이미드와 PMMA가 그래프트된 카본나노튜브 나노복합필름의 전기 전도성 연구)

  • Yun, Sung-Jin;Im, Hyun-Gu;Kim, Joo-Heon
    • Polymer(Korea)
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    • v.34 no.2
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    • pp.97-103
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    • 2010
  • PMMA was grafted on MWCNT surface in order to prepare conducting film composed of 6FDAbased polyimide/MWCNT. The electrical conductivity of 6FDA-based polyimide/PMMA-g-MWCNT was investigated as a function of PMMA-g-MWCNT content. Dispersion of MWCNT in 6FDA-based polyimide composite film was better than the pristine MWCNT due to the interaction force between PMMA and 6FDA-based polyimide. Electrical conductivity was interpreted by percolation threshold theory. As a result, 6FDA-6FpDA/PMMA-g-MWCNT which have high critical exponents and low critical concentration showed better dispersion than polyimide composite material that contains DABA(diamino benzoic acid).

Fabrication and Characterization of ODS 316L Stainless Steels (산화물 분산강화형 316L 스테인리스강의 제조와 특성 연구)

  • Kim, Min-Ho;Ryu, Ho-Jin;Kim, Sung-Soo;Han, Chang-Hee;Jang, Jin-Sung;Kwon, Oh-Jong
    • Journal of Powder Materials
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    • v.16 no.2
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    • pp.122-130
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    • 2009
  • Austenitic oxide-dispersion-strengthened (ODS) stainless steel was fabricated using a wet mixing process without a mechanical milling in order to reduce contaminations of impurities during their fabrication process. Solution of yttrium nitrate was dried after a wet mixing with 316L stainless steel powder. Carbon and oxygen contents were effectively reduced by this wet processing. Microstructural analysis showed that coarse yttrium silicates of about 150 nm were formed in austenitic ODS steels with a silicon content of about 0.8 wt%. Wet-processed austenitic ODS steel without silicon showed higher yield strength by the presence of finer oxide of about 20 nm.

Modified Effects or Surfactants with Polymer-Clay Nanocomposites (고분자-점토 나노복합체에 관한 계면활성제의 개질 영향)

  • Kim, Hong-Un;Bang, Yun-Hyuk;Choi, Soo-Myung;Lim, Kyung-Hee
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.4
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    • pp.290-299
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    • 2006
  • This article investigated to polymer-clay nanocomposite, especially in interfacial respect clay structure, its dispersion into polymer matrix, and clay modification is studied. The cationic exchange of surfactants with clay gallery results in preparing organo-clay capable of compatiblizing to monomer or polymer and increasing interlayer adhesion energy due to expansion of interlayer spacing. The orientation of surfactant in clay gallery is affected by chemical structure and charge density of clay, and interlayer spacing and volume is increased with alkyl chain length of surfactant, or charge density of clay. Also, the interaction between clay and polymer in preparing polymer-clay nanocomposite is explained thermodynamically. In the future, the study and development of polymer-clay nanocomposite is paid attention to the interfacial adhesion, clay dispersion within polymer, mechanism of clay intercalation or exfoliation.

Acoustic emission source location and noise cancellation for crack detection in rail head

  • Kuanga, K.S.C.;Li, D.;Koh, C.G.
    • Smart Structures and Systems
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    • v.18 no.5
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    • pp.1063-1085
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    • 2016
  • Taking advantage of the high sensitivity and long-distance detection capability of acoustic emission (AE) technique, this paper focuses on the crack detection in rail head, which is one of the most vulnerable parts of rail track. The AE source location and noise cancellation were studied on the basis of practical rail profile, material and operational noise. In order to simulate the actual AE events of rail head cracks, field tests were carried out to acquire the AE waves induced by pencil lead break (PLB) and operational noise of the railway system. Wavelet transform (WT) was first utilized to investigate the time-frequency characteristics and dispersion phenomena of AE waves. Here, the optimal mother wavelet was selected by minimizing the Shannon entropy of wavelet coefficients. Regarding the obvious dispersion of AE waves propagating along the rail head and the high operational noise, the wavelet transform-based modal analysis location (WTMAL) method was then proposed to locate the AE sources (i.e. simulated cracks) respectively for the PLB-induced AE signals with and without operational noise. For those AE signals inundated with operational noise, the Hilbert transform (HT)-based noise cancellation method was employed to improve the signal-to-noise ratio (SNR). Finally, the experimental results demonstrated that the proposed crack detection strategy could locate PLB-simulated AE sources effectively in the rail head even at high operational noise level, highlighting its potential for field application.

The Influence of Magnetic Particle Size and Its Properties on The Electromagnetic Particle in Magnetic Tape (자기 Tape의 전자 변환 특성에 대한 자성분의 Size와 그 특성의 영향)

  • 김상문;김태옥
    • Journal of the Korean Magnetics Society
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    • v.6 no.5
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    • pp.334-339
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    • 1996
  • In order to investigate the influence of the magnetic paticle size and its properties on the particulate magnetic material, we evaluated the dispersion of magnetic particles and the electromagnetic properties in magnetic tape made from the magnetic paints by use of each magnetic particles witch were different from particle size and its propertis. The dispersion of magnetic particles depends on the surface chemical properties rather than particle size. As particle size is smaller, the packing ratio of magnetic particle and the magnetic flux density in tape increase. The output levels in playing back of tape incerase in wide frequency range from 315 Hz to 10 kHz and the noises decrease. It is very important to choose the size, the shape, the surface chemical properties and the magnetic properties of the magnetic particle in producing the high quality magnetic tape.

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AC Electrical and Mechanical Properties of Epoxy-Nano-Microsilica Mixed Composites for Eco-Friendly GIS Spacer (친환경 GIS Spacer용, 에폭시-나노-마이크로실리카 혼합 콤포지트의 교류 전기적, 기계적 특성)

  • Park, Jae-Jun
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.67 no.9
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    • pp.1181-1188
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    • 2018
  • In order to develop new insulating materials for GIS Spacer using environmentally friendly insulating gas, three kinds of dispersed liquid nano composites of solid epoxy /nano layered silicate filled material were prepared. And the epoxy/nano/micro silica composite was prepared by mixing epoxy/nano 3 phr dispersion/4 kinds of filler contents(40,50,60, 70wt%). The electrical insulation breakdown strengths of the nano and nano/micro mixed composites were evaluated by using 8 kinds of samples including the original epoxy. The mechanical tensile strength of the epoxy / nano / micro silica composite were evaluated, also. The TEM was measured to evaluate the internal structure of nano/micro composites. As a result, it was confirmed that the layered silicate nano particles was exfoliated through the process of inserting epoxy resin between silicate layers and the layers. In addition, dispersion of nano / micro silica resulted in improvement of electrical insulation breakdown strength with increase of filling amount of dense tissue with nanoparticles inserted between microparticles. In addition, the tensile strength showed a similar tendency, and as the content of microsilica filler increased, the mechanical improvement was further increased.

Evaluation of Mechanical Properties and Fiber Dispersing Characteristics of Fiber Reinforced Lean Concrete Using Fly Ash and Reject Ash (도로 기층 재료로 활용하기 위한 섬유보강 빈배합 콘크리트에 플라이애시와 리젝트애시를 사용한 경우 역학적 특성 및 섬유 분산성 분석)

  • Jang, Young Jae;Park, Cheol Woo;Park, Young Hwan;Yoo, Pyeong Jun;Jung, Woo Tae;Kim, Yong Jae
    • International Journal of Highway Engineering
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    • v.15 no.1
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    • pp.11-21
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    • 2013
  • PURPOSES: As pavement generally provides service shorter than an expected life cycle, maintenance cost increases gradually. In order to help extending the service life and reduce maintenance cost, a new multi-functional composite pavement system is being developed in Korea. METHODS: This study is a part to develop the multi-functional composite pavement and is to investigate the mechanical performances of fiber-reinforced lean concrete for pavement subbase. The inherent problem of fiber reinforced concrete is dispersion of fibers in concrete mix. This study additionally evaluated fiber dispersion characteristics with respect to different fiber types. RESULTS: From the test results, the compressive strengths of the concretes satisfied the required limit of 5MPa at 7days. The standard deviation of the measured number of fibers were lower in the order of nylon, steel fiber and polypropylene. CONCLUSIONS: Reject ash was shown to be satisfactory as a replacement material to Portland cement in lean concrete base. The fiber volume fraction is suggested to be 0.4% even though the fracture toughness did not vary significantly with respect to fiber types. However, fracture energy absorbed up to complete failure increased with the increased fiber volume fraction increment.