• Title/Summary/Keyword: Material Evaluations

Search Result 246, Processing Time 0.025 seconds

The Effects of Electron Beam Exposure Time on Transmission Electron Microscopy Imaging of Negatively Stained Biological Samples

  • Kim, Kyumin;Chung, Jeong Min;Lee, Sangmin;Jung, Hyun Suk
    • Applied Microscopy
    • /
    • v.45 no.3
    • /
    • pp.150-154
    • /
    • 2015
  • Negative staining electron microscopy facilitates the visualization of small bio-materials such as proteins; thus, many electron microscopists have used this conventional method to visualize the morphologies and structures of biological materials. To achieve sufficient contrast of the materials, a number of imaging parameters must be considered. Here, we examined the effects of one of the fundamental imaging parameters, electron beam exposure time, on electron densities generated using transmission electron microscopy. A single site of a negatively stained biological sample was illuminated with the electron beam for different times (1, 2, or 4 seconds) and sets of micrographs were collected. Computational image processing demonstrated that longer exposure times provide better electron densities at the molecular level. This report describes technical procedures for testing parameters that allow enhanced evaluations of the densities of electron microscopy images.

Display System Design Based On The Abstraction Hierarchy

  • Sohn, Kwang-Young;Shin, Hyun-Kook
    • Nuclear Engineering and Technology
    • /
    • v.28 no.3
    • /
    • pp.339-348
    • /
    • 1996
  • Plant monitoring algorithm developments seem to be saturated which means that display system to show the results from the algorithm should be the well-defined and interactive tools for operator's diagnosing, controlling, restoring the abnormal plant situations. On the other hand, very little generalized display design concepts and evaluations are available. Events that are unfamiliar to operators and that has not been anticipated by designers may cause great threats to the nuclear power plant system safety operation. The abstraction hierarchy, considered most popular display design methodology but not generalized for nuclear power plant design space, has ken proposed as a representation frame work that can be adopted to design interfaces and supports operators in diagnosing overlooked events that should have been considered to operate plant safely. However most practical plant display systems do not fully stick to this design concept but partially rely on their philosophy from design experiences. Abstraction hierarchy display design concept will be do scribed and the trend of Advanced Control Room(ACR) CRT design will also be presented with the conventional display for the several type of plants. Consequently this complementary material should be of interest to designer and regulators concerned with nuclear power plant.

  • PDF

Devised New Amorphous Alloys for Magneetoelastic Resonators (Magneetoelastic Resonators에 사용되는 새로운 비정질 함금)

  • C. K. Kim; C. K. Yoo; R.C. O'Handley
    • Journal of the Korean institute of surface engineering
    • /
    • v.31 no.5
    • /
    • pp.245-250
    • /
    • 1998
  • There is clear pressing need to reduce bias field(Ha,) used on linear magenetomechanical resonator tag by at least a factor of two to allow low-bias operation near the frequency minimum since reducing Ha causes a dramatic increase in well depth, which implies increased stability. However, this makes it more difficult to maintain tight frequncy specs. It can be solved by a reduction of magnetomechanical coupling(k). We determined from an equivalent circuit model that optimal reduced, k, is near 0.3 Also, We determiend the material properties($lambda_s$, :saturated magenetostriction, $M_s$, and,$H_a$) that give k=0.3. From these evaluations, we suggested that on optimal comosition with adequate mathrial properties is $Fe_{55}Co_{15}Cr_6Nb_2B_{18}Si_4$.

  • PDF

Structural Evaluations of Bellows for a Gasgenerator Lox Shut-off Valve (가스발생기 산화제 개폐밸브용 벨로우즈 구조 평가)

  • Yoo, Jae-Han;Lee, Joong-Youp;Lee, Soo-Yong
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2011.04a
    • /
    • pp.279-282
    • /
    • 2011
  • The analysis and experimental results for the bellows of gasgenerator liquid oxygen shut-off valve are presented. The analyses are performed using EJMA (Expansion Joint Manufacturing Association) standard and the commercial FE (finite element) analysis program, Abaqus v6.9, at room and cryogenic temperatures. The results include the spring rate, the stress and the fatigue life of the bellows. The effects of the contact and material plasticity on the FE analysis results are also analyzed.

  • PDF

Characteristic evaluations and production of triode magnetron sputtering system (Triode magnetron sputtering system의 제작 및 특성평가)

  • Kim, H.H.;Lee, M.Y.;Kim, K.T.;Yoon, S.H.;Yoo, H.K.;Kim, J.M.;Park, C.H.;Lim, K.J.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2003.07b
    • /
    • pp.787-790
    • /
    • 2003
  • A rf triode magnetron sputtering system is designed and installed its construction in vacuum chamber. In order to calibrate the rf triode magnetron sputtering for thin films deposition processes, the effects of different glow discharge conditions were investigated in terms of the deposition rate measurements. The basic parameters for calibrating experiment in this sputtering system are rf power input, gas pressure, plasma current, and target-to-substrate distance. Because a knowledge of the deposition rate is necessary to control film thickness and to evaluate optimal conditions which are an important consideration in preparing better thin films, the deposition rates of copper as a testing material under the various sputtering conditions are investigated. Furthermore, a triode sputtering system designed in our team is simulated by the SIMION program. As a result, it is sure that the simulation of electron trajectories in the sputtering system is confined directly above the target surface by the force of $E{\times}B$ field. Finally, some teats with the above 4 different sputtering conditions demonstrate that the deposition rate of rf triode magnetron sputtering is relatively higher than that of the conventional sputtering system. This means that the higher deposition rate is probably caused by a high ion density in the triode and magnetron system. The erosion area of target surface bombarded by Ar ion is sputtered widely on the whole target except on both magnet sides. Therefore, the designed rf triode magnetron sputtering is a powerful deposition system.

  • PDF

Evaluations of Y2O3 Powder Synthesized Using Oxalic Acid (옥살산을 이용한 Y2O3 분말제조와 특성 평가)

  • Son, Bo-Young;Jung, Mi-Ewon
    • Korean Journal of Materials Research
    • /
    • v.21 no.8
    • /
    • pp.444-449
    • /
    • 2011
  • Nano-sized $Y_2O_3$ powders were prepared via a sol-gel method starting with $Y(NO_3)_3{\cdot}6H_2O$ (Yttrium(III) nitrate hexahydrate) and water with ethanol as a cosolvent. $Y_2O_3$ is an important rare earth oxide and has been considered for use in nuclear applications, such as ceramic materials, due to its excellent optical and refractory characteristics. It has been used as a chemically stable substrate, a crucible material for melting reactive metals, and a nozzle material for jet casting molten rare earth-iron magnetic alloys. Oxalic acid ($C_2H_2O_4$) has been adopted as a chelating agent in order to control the rate of hydrolysis and polycondensation, and ammonia was added in order to adjust the base condition. The synthesized $Y_2O_3$ powder was characterized using TG/DTA, XRD, FE-SEM, BET and Impedance Analyzer analyses. The powder changed its properties in accordance with the pH conditions of the catalyst. As the pH increases according to the FE-SEM, the grain grew and it showed that the pore size decreased while confirming the effect of the grain size. The nano-material $Y_2O_3$ powders demonstrated that the surface area was improved with the addition of oxalic acid with ammonium hydroxide.

Construction of Street Cleaner Uniform for the Funtional Improvement (기능성 향상을 위한 환경미화원복 설계)

  • Huh, Jin-Kyung;Choi, Hei-Sun
    • Journal of the Korean Society of Clothing and Textiles
    • /
    • v.30 no.8
    • /
    • pp.1178-1187
    • /
    • 2006
  • The purpose of this study is to conduct a questionnaire survey on the actual conditions of the working uniform and protective equipment put on by street cleaners, then to identify their inconvenience and problems and to draw solutions to improve them, and finally to design a spring-and-autumn street cleaner uniform which has enhanced functionalities such as motional flexibility, safety and soil proof. The questionnaire survey of this study was done by street cleaners who were in charge of street cleaning and collecting the recyclable waste. The result of this study, easily worn-out parts of the working clothing were the sleeve hems and the front part on the upper uniform, and the trouser hems and zipper on the lower uniform. Easily soiled parts were the sleeve hems, parts of arm on the upper uniform, and the trouser hems and knee parts on the lower uniform. Based on the results of the questionnaire survey, the sample uniforms were designed in consideration of material, design and pattern. A soil-proof material was used for easily soiled parts such as sleeve hems, knee parts and trouser hems. Reflective material was applied to the parts such as chest, back and the side lines of sleeves and trousers to raise visibility in working and to ensure safety. A crease was given to each side of the back. The height of sleeve cap was lowered to lift the motional flexibility of back and arm parts. Darts were applied to elbow and knee parts for a three-dimensional design. Gussets were inserted in the thigh part to give it activity. Then quantitative evaluation and a sensory evaluation, which was composed of outward appearance, motional flexibility and fitness for field operation, were conducted. According to these evaluations, the sample uniform was found to be more satisfactory than current uniform.

Histological comparison of different compressive forces on particulate grafts during alveolar ridge preservation: a prospective proof-of-concept study

  • Lee, Sung-Jo;Kang, Dae-Young;Cho, In-Woo;Shin, Hyun-Seung;Shin, Seung-Il;Fischer, Kai R.;Park, Jung-Chul
    • Journal of Periodontal and Implant Science
    • /
    • v.50 no.3
    • /
    • pp.197-206
    • /
    • 2020
  • Purpose: The aim of this study was to determine the impact of different compressive forces on deproteinized bovine bone mineral (DBBM) particles covered by native bilayer collagen membrane (NBCM) during alveolar ridge preservation (ARP) in the molar area, and to identify any histomorphometric and clinical differences according to the compressive force applied. Methods: Sockets were filled with DBBM after tooth extraction, and different compressive forces (30 N and 5 N, respectively) were applied to the graft material in the test (30 N) and control (5 N) groups. The DBBM in both groups was covered with NBCM in a double-layered fashion. A crossed horizontal mattress suture (hidden X) was then made. A core biopsy was performed using a trephine bur without flap elevation at the implant placement site for histomorphometric evaluations after 4 months. The change of the marginal bone level was measured using radiography. Results: Twelve patients completed the study. The histomorphometric analysis demonstrated that the mean ratios of the areas of new bone, residual graft material, and soft tissue and the implant stability quotient did not differ significantly between the groups (P>0.05). However, the mean size of the residual graft material showed a significant intergroup difference (P<0.05). Conclusions: The application of 2 compressive forces (5 N, 30 N) on particulate DBBM grafts during open-healing ARP in the posterior area led to comparable new bone formation, implant feasibility and peri-implant bone level.

STUDY ON COLOR DIFFERENCE BETWEEN NATURAL TEETH AND COMPOSITE RESINS (자연치와 복합레진의 색분포에 관한 연구)

  • 김희선;이인복;엄정문
    • Restorative Dentistry and Endodontics
    • /
    • v.26 no.2
    • /
    • pp.180-187
    • /
    • 2001
  • The structure of current guides is largely illogical and without any rational use of color ordering. The shade guides are generally made of plastic (rather than the actual composite material) and do not accurately depict the true shade. translucency. or opacity of the composite resin after polymerization. To solve this problem, information based on evaluations of natural teeth and material that use the same method and experimental conditions is necessary. The present investigation measured the color of natural maxillary anterior teeth in vivo and compared the results with those of composite resins. 269 Korean subjects were selected for this study. Intact central incisor. lateral incisor. and canine were selected. The clinical crowns were free of caries or restorations. The middle site of the coronal portion on the labial surface of the tooth was measured by Chroma Meter. The five light activated. resin-based materials (Amelogen, Denfil, Elitefil, Spectrum, Z100) were used in this study. Resin composite was condensed into plastic mold with a diameter of 8mm and a thickness of 4mm. pressed between glass plates to flatten the surfaces. and polymerized using a Visilux II visible light activation unit. The surfaces were polished sequentially on wet sandpaper. Color measurements of each specimen were accomplished by Chroma Meter. A computer program that compares each tooth color with each composite resin color was written and the minimum CIELAB color difference ($\Delta$E$^*$) between tooth and each material was calculated. Under the conditions of this study: 1. Teeth tend to become darker with advancing age. 2. Canines were darker. more yellow. and less green than incisors. 3. The teeth from the women were lighter. more green. and less yellow than the male teeth. 4. In general. composite resins were lighter. more green. and less yellow than teeth. Deficiencies were noted in Hues in YR range. 5. Mean color differences between the five composite resin products and teeth were detectable to the naked eye($\Delta$E$^*$>1.0). 6. In comparing the mean $\Delta$E$^*$ values of materials. Spectrum showed the least followed by Z100, Elitefil, Amelogen, Denfil in increasing order.

  • PDF

Strength and sulfuric acid resistance properties of cement mortar containing copper slag (동 제련 슬래그를 사용한 시멘트 모르타르의 강도 및 황산저항 특성)

  • Hong, Chang Woo;Lee, Jung-Il;Ryu, Jeong Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.26 no.3
    • /
    • pp.101-108
    • /
    • 2016
  • Each year, more than seven hundred thousand tons of copper slag are generated in Korea as a byproduct during the production of copper. Due to the large amount of copper slag produced, there has been increased interest in the use of copper slag as a construction material. To evaluate the potential of copper slag as a construction material, laboratory evaluations were conducted in this study, and three particle shapes and replacement rates of river sand were selected as experimental variables. Strength, air-void characteristics, and sulfuric acid resistance were the three properties evaluated to assess whether copper slag can be used as a construction material. Test results indicate that the gradation of copper slag has an effect on strength, and the maximum strength was achieved when 60 % of river sand was replaced with copper slag. In addition, when compared with ordinary Portland cement mortar, replacing river sand with copper slag reduced air void size and increased sulfuric acid resistance.