• Bulletin of the Korean Chemical Society
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• 제31권11호
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• pp.3139-3144
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• 2010

A model system has been established for the evaluation of the uncertainty of the value from measurements of multiple subsamples by isotope dilution mass spectrometry (IDMS). In this report, we apply this model system for the evaluation of measurement uncertainty in determination of folic acid in infant formula. Five subsamples were analyzed by IDMS. The mean of the measurement results of the five subsamples was assigned as the final measurement value. The standard deviation (s) of the results from five subsamples was attributable to repeatability of the measurement. The uncertainty components in the IDMS measurement methods were categorized into two groups. Group I includes uncertainty components which give common systematic effects to all subsamples and do not contribute to the variation among multiple measurements (repeatability). Group II includes uncertainty components that give random effects on the measurement results, and are related with the measurement repeatability. These random effects are attributed to s. Therefore, the uncertainty of the final value was calculated by combining the standard deviation of the mean of multiple measurements, $s/{\surd}n$ (where n = 5), and the measurement uncertainty associated with the uncertainty components that give systematic effects.

• 대한기계학회논문집B
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• 제29권10호
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• pp.1130-1138
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• 2005

A national standard system for the petroleum field has been developed to calibrate and test the oil flow meters in Korea. The operating system and the uncertainty of the system were evaluated by the peer reviewers of foreign national metrology institutes in 2002. Since the characteristics of the system might be changed by time, the uncertainty of the system is reevaluated with the consideration of the long term stability of the system. It is found that the system has a relative expanded uncertainty of 0.048 $\%$ in the range of $15\~120\;m^3/h$. According to the uncertainty budget, the uncertainties of the fluid density and the final mass measurement, which are temperature dependent, contribute about $94\%$ of the total uncertainty in the oil flow standard system

• 터널과지하공간
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• 제16권2호
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• pp.135-145
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• 2006

본 연구에서는 조건부 모사 기법 중 순차 가우시안 시뮬레이션(SGS)과 순차 지시 시뮬레이션(SIS)을 이용하여 터널설계 시 미시추구간의 암반등급(RMR)을 예측하여 보았다. 총 30개의 시추공자료 가운데 25개의 시추공자료를 이용하여 순차 가우시안 시뮬레이션과 순차 지시 시뮬레이션을 수행하였으며, 나머지 5개의 시추공에서의 실제 암반등급과 예측 암반등급을 비교하여 보았다. 그 결과 조건부 모사 기법은 암반등급의 공간적 분포특성을 비교적 잘 예측할 수 있고, 예측의 불확실성을 정량적으로 평가할 수 있는 효과적인 방법임을 확인할 수 있었다. 따라서 조건부 모사 기법의 결과는 미시추구간의 암반등급을 예측하는데 있어서 유용한 정보를 제공 해 줄 수 있을 것으로 판단된다.

• 전기학회논문지
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• 제62권9호
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• pp.1264-1269
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• 2013

In this paper, we study a disturbance observer (DOB) based controller for an EMS(Electro-Magnetic Suspension) system in presence of mass uncertainty and input disturbance. The DOB based controller is employed in order to compensate the modeling uncertainty and attenuate disturbance signals. For the design of DOB based controller, the Jacobain linearization of nonlinear system model equation is used. Computer simulation is carried out for nonlinear model in order to compare the performance of the proposed DOB controller with that of the conventional PID controller. The simulation results show that the substantial improvement in the performance can be achieved by the proposed DOB controller.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2004년도 추계학술대회 논문집
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• pp.3-9
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• 2004

The machining parts must be produced within the specification of drawing and those will be able to meet function and efficiency. At that time. it is necessary not only precision machine or machining technique but also the measurement technique is very important. So. the improvement of precise measurement technique is to be joined together at once with improvement of product technique. Finally. he quality and value of the parts are decided by precision measurement. This paper aims to study on he measurement uncertainty when the machined parts are inspected with 3-dimensional coordinate measuring machine. The objectives are to remove an error of measurement and to improve quality and productivity of the mass products.

• Bulletin of the Korean Chemical Society
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• 제20권8호
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• pp.910-916
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• 1999

A current interest in chemistry concerns traceability of analytical measurements to the International System of Units (SI) and the proper estimation of their uncertainties in accordance with the internationally agreed guide provided by the International Organization for Standardization (ISO). Isotope dilution mass spectrometry (IDMS) is regarded as a primary method, which make the measurement results traceable to SI units without significant empirical correction factors. Our laboratory, as the national standards institute of Korea, participated in an intercomparison of environmental analysis, pp'-DDE in corn oil, which was organized by the CCQM under supervision of the CIPM to test feasibility of IDMS as a primary method for the trace analysis of organic compounds. In this report, we provide basic equations used for the calculation of the concentration of the analyte in a sample and a precise description of the processes for the evaluation of the uncertainties of the measurement results. Also, we report the experimental conditions adopted to improve the accuracy of the IDMS measurement. The principles contained in ？？Guide to the Expression of Uncertainty in Measurement'' provided by ISO are followed for the uncertainty evaluation.

• Earthquakes and Structures
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• 제17권5호
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• pp.463-475
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• 2019

In this paper, a procedure to develop fragility curves of structures equipped with semi-active tuned mass dampers (SATMDs) considering multiple failure criteria has been presented while accounting for the uncertainties of the input excitation, structure and control device parameters. In this procedure, Latin hypercube sampling (LHS) method has been employed to generate 30 random SATMD-structure systems and nonlinear incremental dynamic analysis (IDA) has been conducted under 20 earthquakes to determine the structural responses, where failure probabilities in each intensity level have been evaluated using Monte Carlo simulation (MCS) method. For numerical analysis, an eight-story nonlinear shear building frame with bilinear hysteresis material behavior has been used. Fragility curves for the structure equipped with optimal SATMDs have been developed considering single and multiple failure criteria for different performance levels and compared with that of uncontrolled structure as well as structure controlled using passive tuned mass damper (TMD). Numerical analysis has shown the capability of SATMDs in significant enhancement of the seismic fragility of the nonlinear structure. Also, considering multiple failure criteria has led to increasing the fragility of the structure. Moreover, it is observed that the influence of the uncertainty of input excitation with respect to the other uncertainties is considerable.

• 한국화재소방학회논문지
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• 제27권2호
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• pp.75-79
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• 2013

본 연구는 구획화재의 출입구를 통한 연기밀도를 정량적으로 측정하고 측정기법의 신뢰성을 평가하기 위해 불확실성 해석을 수행한다. 메탄 화재 강도에 따른 축소모형 구획공간의 출입구 상층부를 통해 유출되는 연기 유동에 대해 광소멸 측정을 수행하고 Bouguer's의 법칙을 적용하여 연기밀도를 산정하였다. 광투과율, 경로길이, 질량비광소멸상수에 대하여 연기밀도의 측정 불확실도를 평가하였으며 계산된 연기밀도 측정의 확장불확실도는 20% 정도이며 신뢰수준은 95% 이다. 준정상상태의 화재 발열량에 대하여 출입구에서의 평균 연기밀도를 산정하였으며 구획공간내부의 총괄당량비 증가에 따라 출입구의 연기농도가 선형적으로 증가하는 경향을 보였다.

• 소음진동
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• 제10권4호
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• pp.575-583
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• 2000

In this paper, we design a vibration control system that includes a 3-D.O.F. mass-spring-damper structure for the analytical model of a building that is excited at the base of this structure by an external dynamic force, and one Active Mass Damper(AMD) on the top of this structure to generate control forces fro attenuation of the structural response. Two robust controllers based on $\mu$-synthesis and H$\infty$ optimal control are designed for the structural system to show that the performance of a control system can be degraded by some parameter uncertainties such as mass, stiffness coefficients, and/or damping coefficients. The performance of the two controllers are compared in terms of nominal performance, robust stability and robust performance by simulations.

• Bulletin of the Korean Chemical Society
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• 제34권8호
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• pp.2394-2398
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• 2013

Nicotine is the main component of environmental tobacco smoke, and its presence in indoor air is widely used as a secondhand-smoke indicator. Environmental tobacco smoke is a major source of indoor air pollution, but sufficient investigation of the uncertainty of its measurement, which mirrors the reliability of nicotine measurement, has not been performed. We calculated the uncertainty of measurement of indoor air nicotine concentration at low, medium, and high concentrations of 11.3798, 10.1977, $98.3768{\mu}g/m^3$, respectively, and we employed the Guide to the Expression of Uncertainty in Measurements (GUM), proposed by the International Organization for Standardization (ISO). The factors considered in determining the uncertainty were uncertainty of the calibration curve (calibration curve and repeated measurements), desorption efficiency, extraction volume, and sampling airflow (accuracy and acceptable limits of flowmeter). The measurement uncertainty was highest at low concentrations; the expanded measurement uncertainty is $0.9435{\mu}g/m^3$ and is represented as a relative uncertainty of 63.38%. At medium and high (concentrations, the relative uncertainty was 13.1% and 9.1%, respectively. The uncertainty of the calibration curve was largest for low indoor nicotine concentrations. To increase reliability of measurement in assessing the effect of secondhand smoke, measures such as increasing the sample injection rate ($1{\mu}L$ or more), increasing sampling volume to increase collected nicotine, and using gas chromatography-mass spectrometry (GC/MS) or GC/MS/MS, which has a lower quantitation threshold, rather than gas chromatography with nitrogen phosphorous detector, should be considered.