• Title/Summary/Keyword: Magnetic powder

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Analysis Torque Characteristics and Improved Efficiency of Permanent Magnet Multi-D.O.F. Spherical Motor (영구자석형 다자유도 구형전동기의 토크특성 분석과 효율 향상에 대한 연구)

  • Lee, Ho-Joon;Kim, Yong;Jang, Ik-Sang;Park, Hyun-Jong;Kang, Dong-Woo;Won, Sung-Hong;Lee, Ju
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.61 no.1
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    • pp.57-63
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    • 2012
  • A surfaced permanent magnet spherical motor is capable of operating as three degree of freedom that used for the joints of the robot's arm, leg, and eyes. Ongoing research like new concept is essential part of motor field, it will make a great contribution in the future the overall portion of the motor, is becoming expected. The author analysis torque characteristics in spherical motor with state of rotating and positioning. And future design direction is smaller motors with equivalent or higher output. Solutions as torque and efficiency improvements are selecting the core with special processing type like powder metallurgy materials. Their special characteristic is high permeability and low eddy current losses at high speed, so improved the torque and efficiency.

Fabrication of High Tc Superconducting Nano Powder Using Chemical Process (화학공정을 이용한 초전도 나노 분말 활성)

  • Lee, Sang-Heon;Kim, Chan-Jung;Jang, Kun-Ik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2006.06a
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    • pp.547-548
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    • 2006
  • In order to realize the commercial application of HTSC materials, it is necessary to develop the fabrication process of high Tc oxide superconductor materials with desired shape and for practical application and high critical current density as well as good mechanical strength which can withstand high lorenz force generated at high magnetic field. Much studies have been concentrated to develop the fabrication technique for high critical current density but still there are a lot of gap which should be overcome for large scale application of HTSC materials at liquid nitrogen temperature. Recently some new fabrication techniques have been developed for YBaCuO bulk superconductor with high mechanical strength and critical current density. In this project, the establishment of fabrication condition and additive effects of second elements were examined so as to improve the related properties to the practical use of YBaCuO superconductor, and we reported the production of the YBaCuO high Tc superconductor by the pyrolysis method.

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Substitutional Effects of Na in the YB$a_2Cu_3O_{7-y}$ Oxide Superconductors

  • Hur Nam Hwi;Ha, Dong Han;Park Yong Ki;Park, Jong Chul
    • Bulletin of the Korean Chemical Society
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    • v.13 no.4
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    • pp.425-428
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    • 1992
  • Sodium substituted samples of $Y_{1-x}Na_xBa_2Cu_3O_{7-y}$ for $0.00{\leq}x{\leq}0.16$ were prepared and characterized by X-ray powder pattern, electrical resistivity and magnetic susceptibility measurements, Raman spectroscopy, and idometric titration. The Na substituted compounds have narrow solid solution limits where $0.00{\leq}x{\leq}0.16.$ As the Na concentration increases, the parent orthorhombic structure tends to gradually change to tetragonal. Small changes in the superconducting transition temperature, Tc, are observed in this solid solution region. Raman spectra for the Na phases are virtually identical with that of $YBa_2Cu_3O_7$ except that the Cu(1)-O(4) stretching mode at 504 $cm^{-1}$ and the Cu(2)-O(2,3) bending mode at 340 $cm^{-1}$ for x = 0.16 are slightly shifted. The hole concentrations of the sodium substituted compounds ranged from 0.31 to 0.33 per Cu site are increased with Na content. The substitution of $Na^+$ for $Y^{3+}$ site appears to create oxygen vacancies in the Cu-O chains, causes structural change from orthorhombic to tetragonal, and increases hole concentration in the substituted system.

The Electromagnetic Wave Absorption Characteristics of Cu-Ni-Zn Ferrite by Thermal Decomposition of Organic Acid Salt (유기산염 열분해법에 의한 Cu-Ni-Zn 페라이트의 전자파 흡수 특성)

  • 정재우;이완재
    • Journal of the Korean Magnetics Society
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    • v.5 no.6
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    • pp.947-951
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    • 1995
  • The electromagnetic interference is prevented by the high magnetic loss of the ferrite. The absorbing property of electromagnetic wave could be improved by the ferrite that has a finer and more uniform microstructure. The thermal decomposition of organic acid salt provided the uniform composition and fine powder. The absorbing properties of electromagnetic wave were evaluated by the relative complex permeability, permittivity, and the attenuation which is calculated from the results of network analyzer. The permeability and permittivity were increased with increase of the density and with decrease of the grain size. The matching thickness could be reduced with increasing sintered temperature. The attenuation of the Cu-Ni-Zn ferrite showed over 20dB when the matching thickness and the matching frequency range were 6.75mm and from 160MHz to 640MHz, respectively.

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Synthesis, spectral, thermal, structural study and theoretical treatment of new complexes of mannich base with Ni(II) and study of cytotoxicity effect on (Hepa-2) cell line and antimicrobial activity

  • Omar H. Al-Obaidi
    • Analytical Science and Technology
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    • v.36 no.2
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    • pp.70-79
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    • 2023
  • The synthesis of the Mannich base as a ligand (L) N-(morpholino (phenyl) methyl) acetamide is the subject of this study. Elemental analyses, FT-IR spectra, UV-vis, 1H-NMR, and magnetic measurements were used to confirm the synthesis of the [Ni(L)2]Cl2 complex, thermal analysis (TG/DTG), atomic absorption, and scanning, and structurally explained as electron microscopy (SEM), and X-ray powder diffraction (XRD) methods. The melting point of the complex and its molar conductivity were also measured. The suggested geometries of the complexes formed have a tetrahedral structure, according to the data acquired using various techniques. Theoretical approaches to the complex formation have been investigated. For molecular mechanics and semi-empirical calculations, the HYPERCHEM6 program had been used. The effect of the novel Ni(II) complex on the cancer cell Hepa-2 (human hepatocellular ademocarcinoma), that is the human laryngeal cancer, was studied. It has been found that these ligand and complex have potent effects on the cancer cell. The antibacterial activity of the free ligand and its complex was evaluated against two kinds of human pathogenic bacteria. The first category is Gram-positive (Staphylococcus aureas, epiderimids), whereas the second group is Gram-negative (Psedamonas aeruginosa, Escherichia coli) (from the diffusion method). Finally, it was discovered that various chemicals had varied growth-inhibiting effects on bacteria.

Crystallographic and magnetic properties of (CoFe2O4)1-X(Y3Fe5O12)X ((CoFe2O4)1-X(Y3Fe5O12)X 분말의 구조적 특성과 자기적 특성)

  • Lee, Jae-Gwang;Chae, Kwang-Pyo;Jang, Joon-Sik;Lee, Sung-Ho;Lee, Yong-Bae
    • Journal of the Korean Magnetics Society
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    • v.13 no.1
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    • pp.1-5
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    • 2003
  • Magnetic and structural properties of $(CoFe_2O_4)_{1-x}(Y_3Fe_5O_{12})_x$ powders (0 $\leq$ x $\leq$ 1) grown by a conventional ceramic method were investigated using X-ray diffractormeter (XRD), scanning electron microscopy (SEM), Mossbauer spectroscopy and vibrating sample magnetometer (VSM). The XRD results for the powders annealed at 120$0^{\circ}C$ indicated that no other peak was observed except for the ones from cobalt ferrite and the garnet powder. SEM micrographs indicated that cobalt ferrite and garnet powders were aggregated and completely formed together. It was hard to identify which part of the powders was the garnet or the cobalt ferrite. Mossbauer spectra for powders grown separately and mixed mechanically consisted of sub-spectra of cobalt ferrite and garnet, however, powders annealed together had an extra sub-spectrum, which was related with the interaction between iron ions at the grain surfaces of cobalt ferrite and the garnet: cobalt ferrite and garnet particles were located very closely. The value of the saturation magnetization measured by a VSM as a function of composition ratio agreed very well with the ones based on the theoretical calculation.

Nonstoichiometry and Magnetic Properties of the $Eu_{1-x}Sr_xCoO_{3-y}$ System ($Eu_{1-x}Sr_xCoO_{3-y}$계의 비화학량론과 자기적 특성)

  • Ryu, Kwang Hyun;Min, Ji Young;Yo, Chul Hyun
    • Journal of the Korean Chemical Society
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    • v.39 no.7
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    • pp.508-512
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    • 1995
  • A series of samples in the $Eu_{1-x}Sr_xCoO_{3-y}$ system has been prepared by heating the proper amount of reactant mixture to 1150$^{\circ}C$ under an ambient atmosphere, and the solid solutions are identified by X-ray powder diffraction analysis. The crystal system of samples for the compositions of x=0.00 and 0.25 are found to be orthorhombic whose local symmetry is similiar to the distorted octahedra with orthoferrite type one, whereas those of x=0.50 and 0.75 to be the cubic system, and that of x=1.00 to the orthorhombic similiar to be the brownmillerite type. The amount of $Co^{4+}$ ion (${\tau}$ value) is maximized at the composition of x=0.50, and the oxygen vacancies increase with the x value. The nonstoichiometric chemical formula of each compound could be determined from the mole ratio of $Co^{4+}$ ion and oxygen vacancies. The $Co^{3+}$ ion located in octahedral site has spin transition from low spin to high spin states with increasing temperature. Therefore, the effective magnetic moment of each samples obtained from the magnetic measurement is increased with the increasing temperature. The $EuCoO_{3.00}$ has strong antiferromagnetic interaction between the neighboring $Co^{3+}$ ions through the intermediate oxygen ions. With the increasing ${\tau}$ value, the absolute {\theta}_p$ value is decreased by the ferromagnetic interaction of $Co^{3+}-O^2-Co^{4+}$ and thus the {\theta}_p$ has positive value at x=0.50.

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Magnetic Resonance Imaging uses 3D Printed Material of Headset (Noise Reduction Effect) (자기공명영상 검사 시 3D 프린팅 재료를 이용한 헤드셋 연구 (소음저감 효과))

  • Choi, Woo Jeon;Kim, Dong Hyun
    • Journal of the Korean Society of Radiology
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    • v.12 no.3
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    • pp.335-341
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    • 2018
  • With the improvement of medical state, patients' expectations for the most advanced medical equipment are increasing. Particularly, Magnetic Resonance Image (MRI) is used as one of the core image diagnosis methods in all clinical area. However, it has been reported that many of patients who go through the examination suffer from anxiety to the severe noise level during the examination. In this study, both the noise reduction evaluation of headsets with sound-blocking materials added to existing sound-absorbing materials and the existence of sound blocking materials as artifacts on the examination image are tested. An MRI test noise is recorded as a speaker by cross-ordination the sound material (sponge) and the sound material (acrylic plate, copper plate, and 3D copper plate) inside the headset made from 3D pring. A quantitative assessment of headsets showed that the average headset value was 81.8 dB. The average dB value of the most soundproof material combination(Copper, acrylic plate, sponge, sponge) headsets on headsets with added charactering material was measured at 70.4 dB, and MRI showed that the copper was diamagnetic substance and excluded. The second most soundproof headset(Sponge, acrylic plate, 3D copper plate, sponge) was measured at 70.6 dB and MRI showed no artifacts. The same simulation of the material printed with a 3D copper PLA containing approximately 40 % copper powder resulted in no artifacts, therefore, the material output as a 3D printing was better suited for use. For MRI related research, the mutual development of 3D printing is highly anticipated.

Superparamagnetic Properties of γ-Fe2O3 Nanoparticles (초미세 나노분말 γ-Fe2O3의 초상자성 특성연구)

  • Lee, Seung-Wha;Lee, Jae-Gwang;Chae, Kwang-Pyo;An, Sung-Yong
    • Journal of the Korean Magnetics Society
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    • v.20 no.5
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    • pp.196-200
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    • 2010
  • $\gamma-Fe_2O_3$ nanoparticles have been prepared by a sol-gel method. The structural and magnetic properties have been investigated by XRD, VSM and Mossbauer spectroscopy. $\gamma-Fe_2O_3$ powder annealed at $150^{\circ}C$ has a spinel structure and superparamagnetical behavior. The estimated size of superparammagnetic $\gamma-Fe_2O_3$ nanoparticle is around 7 nm. The hyperfine fields at $-261^{\circ}C$ for the A and B patterns were found to be 503 and 485 kOe, respectively. The blocking temperature ($T_B$) of superparammagnetic $\gamma-Fe_2O_3$ nanoparticle is about $-183^{\circ}C$. The magnetic anisotropy constant of $\gamma-Fe_2O_3$ nanoparticle was calculated to be $1.6{\times}10^6ergs/cm^3$. $\gamma-Fe_2O_3$ nanoparticle annealed at $150^{\circ}C$ can be a candidate for biomedicine applications as magnetic carriers.

The Characterizations of Tape Casting for Low Temperature Sintered Microwave Ceramics Composite (저온소성 마이크로파 유전체 세라믹스 복합체의 Tape Casting특성)

  • Lee, Woo-Suk;Kim, Chang-Hwan;Ha, Mun-Su;Jeong, Soon-Jong;Song, Jae-Sung;Ryu, Bong-Ki
    • Journal of the Korean Ceramic Society
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    • v.42 no.2 s.273
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    • pp.132-139
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    • 2005
  • Sintering behavior of $BaO-Nd_{2}O_3-TiO_2$ with a Pb-based glassceramics frit were investigated in order to understand an effect of glassceramics as a low temperature sintering agent on dielectric ceramics. A green sheet form was fabricated through tape casting method with the glassceramic fut added $BaO-Nd_{2}O_3-TiO_2$. The dispersion properties, rheological properties and final density of dielectric composit slurry as a function of amount and composition of organic additives was examined. The dispersants' addition was effective in controlling dispersion of the ceramics in solution. The addition of excessive dispersant showed adverse effect on dispersion. The prepared slurries, containing ceramic : powders, glass-ceramics and various kinds of organic viechles, exhibited typical shear thinning behavior. The best properties of tape casting appeared powder to solvent ratio 65 : 35 and amount of the binder 6 wt$\%$ and plasticizer 3 wt$\%$. The viscosity of the slurry was 677 cps and green/sintered density in the tape was $3.3 g/cm^3,\;5.56 g/cm^3$ respectively.