• Title/Summary/Keyword: Magnetic Materials

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Fabrication of Nanostructured Fe-Co Alloy Powders by Hydrogen Reduction and its Magnetic Properties

  • Lee, Young-Jung;Lee, Baek-Hee;Kim, Gil-Su;Lee, Kyu-Hwan;Kim, Young-Do
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.120-121
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    • 2006
  • Magnetic properties of nanostructured materials are affected by the microstructures such as grain size (or particle size), internal strain and crystal structure. Thus, it is necessary to study the synthesis of nanostructured materials to make significant improvements in their magnetic properties. In this study, nanostructured Fe-20at.%Co and Fe-50at.%Co alloy powders were prepared by hydrogen reduction from the two oxide powder mixtures, $Fe_2O_3$ and $Co_3O_4$. Furthermore, the effect of microstructure on the magnetic properties of hydrogen reduced Fe-Co alloy powders was examined using XRD, SEM, TEM, and VSM.

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ICOSAHEDRAL CLUSTERS AND MAGNETIC PROPERTIES OF $LaCo_{13}$ AMORPHOUS AND CRYSTALLINE ALLOYS

  • Fukamichi, K.;Fujita, A.;Ohashi, N.;Hashimoto, M.;Matsubara, E.;Waseda, Y.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.767-771
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    • 1995
  • The atomic structure and magnetic properties of $LaCo_{13}$ amorphous alloy have been investigated and compared with those of its crystalline counterpart. It has been confirmed that the amorphous alloy is composed of the icosahedral clusters with a $NaZn_{13}$-type structure. The magnetic moment and the spin- wave stiffness constant obtained from the magnetic measurements in the amorphous state are larger than those in the crystalline state. The Curie temperature estimated from the reduced magnetization curve for the former is much higher than the value for the latter. The localized magnetic moment character in the amorphous state is stronger than that in the crystalline state.

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Microstructure and Magnetic Properties of Au-doped Finemet-type Alloy

  • Le, Anh-Tuan;Kim, Chong-Oh;Ha Nguyen Duy;Chau Nguyen;Tho Nguyen Duc;Lee, Hee-Bok
    • Journal of Magnetics
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    • v.11 no.1
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    • pp.36-42
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    • 2006
  • In this report, we demonstrate a comprehensive analysis of the effects of Au addition on the microstructure and magnetic properties of $Fe_{73.5}Si_{13.5}B_{9}Nb_{3}Au_1$ Finemet-type alloy. It was found that the as-quenched alloys were the amorphous state and turned into nanocrystalline state under heat treatments. The DSC analysis indicates that the sharply exothermal peak corresponding to the crystallization of the $\alpha-Fe(Si)$ was observed at $547-579^{\circ}C$ depending on the heating rates, which is little higher than that of original Finemet (542-$570{^{\circ}C}$, respectively). Besides, the thermomagnetic result confirmed that the full substitution of Cu by Au with the single phase structure in the M(T) curve along cooling cycle. Ultrasoft magnetic properties of the nanocrystallized samples were significantly enhanced by the proper annealing such as the increase of permeability and the decrease of the coercivity. The optimum annealing condition was found at the annealing temperature of $540^{\circ}C$ and the increase of the annealing time up to 90 min.

CORROSION PHENOMENA OF MAGNETIC ATTACHMENT USED IN ORAL ENVIRONMENT (구강 환경에서 사용된 자성 Dyna 어태치먼트의 부식현상)

  • Kwak Jong-Ha;Chung Chae-Heon;Choe Han-Cheol
    • The Journal of Korean Academy of Prosthodontics
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    • v.40 no.5
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    • pp.470-483
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    • 2002
  • The purpose of this study was to investigate further the mechanics of failure of magnets used for denture retention. Dyna magnets were retrived from denture that had failed after 34 months of clinical use. The magnets were observed and sectioned in order to analyse with high resolution scanning electron microscope. From this study, corrosion behaviors of used magnetic attachment were analysed. The results were as follows ; 1. In Nd-Fe-B based magnetic materials, the erosion-corrosion was started at ununiformed part of stainless steel cover. 2. Corrosion was initiated at weared stainless steel surface and then magnetic materials were spalled by corrosive solution. 3. Spatting was occurred in Nd-Fe-B magnet materials due to corrosion products and then corrosion rate was increased drastically. 4. Corrosion started from ununiformed stainless steel surface as well as welded zone. In conclusion, the failure of magnets may occur by either breakdown of the welding or breakdown of the encapsulating material. So, it is considered that the corrosion problem of dental magnetic materials could be solved to some extent with surface treatment of dental magnetic materials.

Dielectric/Magnetic Nanowires Synthesized by the Electrospinning Method for Use as High Frequency Electromagnetic Wave Absorber

  • Jwa, Yong-Ho
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.11a
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    • pp.14-14
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    • 2009
  • High frequency electromagnetic(EM) waves are increasingly being applied in industries because of saturationat lower frequency bands as a result of huge demand. However, electromagneticinterference (EMI) has become a serious problem, and as a result, highfrequency EM absorbers are now being extensively studied. Also, recentdevelopments in absorber technology have focused on producing absorbers thatare thin, flexible, and strong. Hence, one-dimension ferrous nano-materials area potential research field, because of their interesting electronic andmagnetic properties. Commercially, EM wave absorbing products are made ofcomposites, which blend the insulating polymer with magnetic fillers. Inparticular, the shape of the magnetic fillers, such flaky, acicular, or fibrousmagnetic metal particles, rather than spherical, is essential for synthesizingthin and lightweight EM wave absorbers with higher permeability. High aspectratio materials exhibit a higher permeability value and therefore betterabsorption of the EM wave, because of electromagnetic anisotropy. Nanowires areusually fabricated by drawing, template synthesis, phase separation, selfassembly, and electrospinning with a thermal treatment and reduction process.Producing nanowires by the electrospinning method involves a conventionalsol-gel process that is simple, unique, and cost-effective. In thispresentation, Magnetic nanowire and dielectric materials coated magneticnanowire with a high aspect ratio were successfully synthesized by theelectrospinning process with heat treatment and reduction. In addition toestimating the EM wave absorption ability of the synthesized magnetic anddielectric materials coated magnetic nanowire with a network analyzer, weinvestigated the possibility of using these nanowires as high-frequency EM waveabsorbers. Furthermore, a wide variety of topics will be discussed such as thetransparent conducting nanowire and semiconducting nanowire/tube with theelectrospinning process.

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Investigating the fatigue failure characteristics of A283 Grade C steel using magnetic flux detection

  • Arifin, A.;Jusoh, W.Z.W.;Abdullah, S.;Jamaluddin, N.;Ariffin, A.K.
    • Steel and Composite Structures
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    • v.19 no.3
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    • pp.601-614
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    • 2015
  • The Metal Magnetic Memory (MMM) method is a non-destructive testing method based on an analysis of the self-magnetic leakage field distribution on the surface of a component. It is used for determining the stress concentration zones or any irregularities on the surface or inside the components fabricated from ferrous-based materials. Thus, this paper presents the MMM signal behaviour due to the application of fatigue loading. A series of MMM data measurements were performed to obtain the magnetic leakage signal characteristics at the elastic, pre-crack and crack propagation regions that might be caused by residual stresses when cyclic loadings were applied onto the A283 Grade C steel specimens. It was found that the MMM method was able to detect the defects that occurred in the specimens. In addition, a justification of the Self Magnetic Flux Leakage patterns is discussed for demonstrating the effectiveness of this method in assessing the A283 Grade C steel under cyclic loadings.

Influence of multiple holes on the magnetic properties of YBCO superconductor

  • Oh, W.S.;Oh, S.K.;Jang, G.E.;Kim, C.J.;Han, Y.H.;Jung, S.Y.;Sung, T.H.
    • Progress in Superconductivity and Cryogenics
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    • v.11 no.2
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    • pp.15-19
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    • 2009
  • Bulk $YBa_2Cu_3O_{7-{\delta}}$ (YBCO) superconductor was manufactured with the top-seeded melt grown method. The 9, 16, and 25 holes, as small as 0.7mm in diameter, parallel to the c-axis were mechanically drilled. Magnetic flux mapping and levitation force were measured and compared to estimate the influence of multiple holes on the magnetic properties of YBCO superconductor at 77K. According to the measurements, the maximum magnetic flux density obtained from the plain sample was 2.48kG, while the maximum magnetic flux density of the sample with 25 holes was low as around 2.29kG. The levitation force measured on the sample with 9 holes increased from 91N to 105N. The levitation force measured on the samples with 9 holes is relatively higher than the plain sample without any holes. In this case, increase of the levitation force in the perforated samples could be explained by enhancement of the cooling efficiency more effectively. We investigated that the magnetic properties of YBCO superconductor were strongly influenced by the artificial holes.

Magnetic Sensor-Based Detection of Picoliter Volumes of Magnetic Nanoparticle Droplets in a Microfluidic Chip

  • Jeong, Ilgyo;Eu, Young-Jae;Kim, Kun Woo;Hu, XingHao;Sinha, Brajalal;Kim, CheolGi
    • Journal of Magnetics
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    • v.17 no.4
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    • pp.302-307
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    • 2012
  • We have designed, fabricated and tested an integrated microfluidic chip with a Planar Hall Effect (PHE) sensor. The sensor was constructed by sequentially sputtering Ta/NiFe/Cu/NiFe/IrMn/Ta onto glass. The microfluidic channel was fabricated with poly(dimethylsiloxane) (PDMS) using soft lithography. Magnetic nanoparticles suspended in hexadecane were used as ferrofluid, of which the saturation magnetisation was 3.4 emu/cc. Droplets of ferrofluid were generated in a T-junction of a microfluidic channel after hydrophilic modification of the PDMS. The size and interval of the droplets were regulated by pressure on the ferrofluid channel inlet. The PHE sensor detected the flowing droplets of ferrofluid, as expected from simulation results. The shape of the signal was dependent on both the distance of the magnetic droplet from the sensor and the droplet length. The sensor was able to detect a magnetic moment of $2{\times}10^{-10}$ emu at a distance of 10 ${\mu}m$. This study provides an enhanced understanding of the magnetic parameters of ferrofluid in a microfluidic channel using a PHE sensor and will be used for a sample inlet module inside of integrated magnetic lab-on-a-chip systems for the analysis of biomolecules.

Analysis of charge and magnetic characteristics of brake wear particles (브레이크 마모입자의 하전 및 자성 특성 분석)

  • Chaeyeon Jo;Dongho Shin;Gunhee Lee;Sang-Hee Woo;Seokhwan Lee;Bangwoo Han;Jungho Hwang
    • Particle and aerosol research
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    • v.19 no.2
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    • pp.31-42
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    • 2023
  • The charge and magnetic characteristics of LM (Low-metallic) and NAO (Non-asbestos-organic) brake wear particles were analyzed. The ratio of charged particles from total particles is about 86% of the LM pad and about 92% of the NAO pad. Number of charge per particle from the NAO pad is also higher than that of the LM pad. The ratio of magnetic particles from total particles increases with the particle size. The ratio of magnetic particles from the LM pad is about 15% for the particles with the size of 1 ㎛, and about 74% for ones with 5 ㎛. The ratio from the NAO pad is about 5% for the particles with the size from 0.5 ㎛ to 2 ㎛, and about 80% for the particles with 5 ㎛. Through the analysis of the components of the two pads with SEM-EDS (Scanning Electron Microscopy - Energy Dispersive X-ray Spectroscopy), it was found that the LM pad was occupied with more iron fraction than the NAO pad and that PM2.5-10 was occupied with more iron fraction than PM2.5. The particles smaller than 10 ㎛ (i.e. PM10) from the LM pad contained about 83% of charged particles, about 43% of magnetic particles, and about 93% of charged or magnetic particles. PM10 from the NAO pad contained about 88% of charged particles, about 15% of magnetic particles, and about 89% of charged or magnetic particles.