• Title/Summary/Keyword: Mag H

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The Change of Ginsenoside Composition in American Ginseng (Panax quinquefolium) Extract by the Microwave and Vinegar Process (서양삼 추출물의 초단파 및 식초 처리에 의한 인삼 사포닌 성분 변화)

  • Jo, Hee Kyung;Gwak, Hyeon Hui;Im, Byung Ok;Cho, Soon Hyun;Ko, Sung Kwon
    • Korean Journal of Pharmacognosy
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    • v.45 no.2
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    • pp.107-112
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    • 2014
  • The purpose of this study is to develop a new preparation process of American ginseng (Panax quinquefolium) extract featuring high concentration of ginsenoside $Rg_3$, $Rg_5$, and $Rk_1$, Red ginseng special components. Chemical transformation from ginseng saponin glycosides to prosapogenin was analyzed by the HPLC. Extracts of American ginseng were processed under several treatment conditions of microwave and vinegar (about 14% acidity). The results showed that the quantity of ginsenoside $Rg_3$ increased by over 0.9% at the 20 minutes of the pH 2~4 vinegar and microwave American ginseng ethanol extract compared with other process times. The result of MAG-20 indicates that the American ginseng microwave and vinegar-processed American ginseng extracts (about 14% acidity) treated for 20 minutes produced the highest amount of ginsenoside $Rg_3$ (0.969%), $Rg_5$ (1.071%), and $Rk_1$ (0.247%). Besides, MAG-15 indicates that the microwave - and vinegar-processed American ginseng extracts (about 14% acidity) treated for 15 minutes produced the highest amount of ginsenoside $Rg_3$ (0.772%), $Rg_5$ (1.330%), and $Rk_1$ (0.386%). This indicates that American ginseng treated with microwave and vinegar had the quantity of the ginsenoside $Rg_3$ over 32 times the amount of the ginsenoside $Rg_3$ (which was not found in raw and American ginsengs) in the average commercial Red ginseng.

Preparation, characterization and comparison of antibacterial property of polyethersulfone composite membrane containing zerovalent iron or magnetite nanoparticles

  • Dizge, Nadir;Ozay, Yasin;Simsek, U. Bulut;Gulsen, H. Elif;Akarsu, Ceyhun;Turabik, Meral;Unyayar, Ali;Ocakoglu, Kasim
    • Membrane and Water Treatment
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    • v.8 no.1
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    • pp.51-71
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    • 2017
  • Antimicrobial polyethersulfone ultrafiltration membranes containing zerovalent iron ($Fe^0$) and magnetite ($Fe_3O_4$) nanoparticles were synthesized via phase inversion method using polyethersulfone (PES) as membrane material and nano-iron as nanoparticle materials. Zerovalent iron nanoparticles (nZVI) were prepared by the reduction of iron ions with borohydride applying an inert atmosphere by using $N_2$ gases. The magnetite nanoparticles (nMag) were prepared via co-precipitation method by adding a base to an aqueous mixture of $Fe^{3+}$ and $Fe^{2+}$ salts. The synthesized nanoparticles were characterized by scanning electron microscopy, X-ray powder diffraction, and dynamic light scattering analysis. Moreover, the properties of the synthesized membranes were characterized by scanning electron microscopy energy dispersive X-ray spectroscopy and atomic force microscopy. The PES membranes containing the nZVI or nMag were examined for antimicrobial characteristics. Moreover, amount of iron run away from the PES composite membranes during the dead-end filtration were tested. The results showed that the permeation flux of the composite membranes was higher than the pristine PES membrane. The membranes containing nano-iron showed good antibacterial activity against gram-negative bacteria (Escherichia coli). The composite membranes can be successfully used for the domestic wastewater filtration to reduce membrane biofouling.

Stability of Sputtered Hf-Silicate Films in Poly Si/Hf-Silicate Gate Stack Under the Chemical Vapor Deposition of Poly Si and by Annealing

  • Kang, Sung-Kwan;Sinclair, Robert;Ko, Dae-Hong
    • Journal of the Korean Ceramic Society
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    • v.41 no.9
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    • pp.637-641
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    • 2004
  • We investigated the effects of SiH$_4$ gas on the surface of Hf-silicate films during the deposition of polycrystalline (poly) Si films and the thermal stability of sputtered Hf-silicate films in poly Si/Hf-silicate structure by using High Resolution Transmission Electron Microscopy (HR-TEM) and X-ray Photoelectron Spectroscopy (XPS). Hf-silicate films were deposited by using DC-mag-netron sputtering with Hf target and Si target and poly Si films were deposited at 600$^{\circ}C$ by using Low Pressure Chemical Vapor Deposition (LPCVD) with SiH$_4$ gas. After poly Si film deposition at 600$^{\circ}C$, Hf silicide layer was observed between poly Si and Hf-silicate films due to the reaction between active SiH$_4$ gas and Hf-silicate films. After annealing at 900$^{\circ}C$, Hf silicide, formed during the deposition of poly Si, changed to Hf-silicate and the phase separation of the silicate was not observed. In addition, the Hf-silicate films remain amorphous phase.

The Young Open Cluster NGC 1893 in the Outer Galaxy

  • Lim, Beomdu;Sung, Hwankyung
    • The Bulletin of The Korean Astronomical Society
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    • v.38 no.2
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    • pp.72.2-72.2
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    • 2013
  • We present a UBVI and $H{\alpha}$ photometric study of the young open cluster NGC 1893 in the outer Galaxy as part of "Sejong Open cluster Survey (SOS)" project. Using the properties of early-type stars in the photometric diagrams 65 early-type members were selected. More than 120 $H{\alpha}$ emission stars and candidates were found by $H{\alpha}$ photometry. Together with the published young stellar object catalogue and X-ray source list for this cluster, a total of 837 pre-main sequence (PMS) stars were identified in our photometric data. We obtained the mean reddening of < E(B-V) > = $0.56{\pm}0.08$ mag from the (U-B, B-V) diagram and confirmed the normal reddening law ($R_V=3.1$) toward NGC 1893 based on color excess ratios from optical to mid-infrared wavelengths. The zero-age main sequence fitting to the reddening-corrected color-magnitude diagrams gives a distance modulus of $V_0-M_V=12.8{\pm}0.1$. The age of the cluster inferred from stellar evolution models is about 1-2 Myr. We also found the Salpeter/Kroupa type initial mass function for this cluster. Finally, the mass accretion rate of 80 PMS stars with UV excess emission was estimated for the stars with masses from $0.6M_{\odot}$ to $5M_{\odot}$.

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Application of Fast Atom Bombardment Collision-induced Dissociation Tandem Mass Spectrometry for Structural identification of Glycerolipids Isolated From Marine Sponge

  • Lee, Sun-Young;Hong, Joo-Yeon;Jung, Jee-H.;Hong, Jong-Ki
    • Mass Spectrometry Letters
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    • v.2 no.1
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    • pp.8-11
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    • 2011
  • Two types of glycerolipids [monoacylglycerols (MAG) and cyclitols] were isolated by reversed phase high-performance liquid chromatography from the methanol extracts of a marine sponge, and analyzed by fast atom bombardment mass spectrometry (FAB-MS) in positive-ion mode. FAB mass spectra of these compounds yielded protonated molecules $[M + H]^+$ and abundant sodiated molecules $[M + Na]^+$ from a mixture of 3-nitrobenzyl alcohol and NaI. The structures of these compounds were elucidated by FAB-collisional-induced dissociation (CID)-tandem mass spectrometry. We carried out collision-indused dissociation (CID) of these lipids in B/E-linked scan mode. The CID B/E-linked scan of $[M + H]^+$ and $[M + Na]^+$ precursor ions resulted in the formation of numerous characteristic product ions through a series of dissociative processes. The product ions formed by charge-remote fragmentation (CRF) provided important information for the identification of the acyl chain structure substituted at the glycerol backbone. Some of the product the ions were diagnostic for the presence of a glycerol backbone or acyl chain structure.

Physicochemical Properties of Organic Liquid Fertilizer with Oil Cake and Rice Bran as Affected by Microorganism and the Ratio of Molasses

  • An, Nan-Hee;Kim, Yong-Ki;Cho, Jung-Rai;Jee, Hyeong-Jin;Lee, Byung-Mo;Yoon, Jong-Chul;Choi, Ji-Won
    • Korean Journal of Soil Science and Fertilizer
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    • v.46 no.6
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    • pp.579-584
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    • 2013
  • The study was conducted to investigate changes in the characteristics of inorganic components during fermenting process of organic liquid fertilizers according to the type and ratio of microorganism and the amount of molasses when producing organic liquid fertilizers using sesame oil cake and rice bran. To select appropriate microorganisms, liquid fertilizers were produced through a 90-day fermentation process by adding mag-ggeo-li, yogurt, dried yeast, and leaf mold. The pH in liquid fertilizer was decreased, and then increased in all microorganism samples except the mag-ggeo-li sample. The EC was rapidly increased in all samples until the $10^{th}$ days after production, and showed no changes after the $60^{th}$ days in dried yeast and after the $30^{th}$ days in the other samples. The concentration of $NH_4$-N was generally increased with time. The concentration of $P_2O_5$ was rapidly increased until the $10^{th}$ days after production and was maintained at about 1% regardless of the type of microorganism. In terms of the characteristics of liquid fertilizers according to the ratio of selected dried yeast, the pH was decreased until the $30^{th}$ days after producing the liquid fertilizers, and then was increased regardless of the ratio of dried yeast. The EC was increased with time and showed no differences depending on the amount of dried yeast. The concentration of $NH_4$-N was increased with time and in proportion to the amount of dried yeast. In terms of the characteristics of liquid fertilizers according to the ratio of molasses, the pH was decreased with increasing the molasses. The EC and concentration of $P_2O_5$ were no differences according to the amount of molasses. When 3% molasses was added, the content of $NH_4$-N was 2.6 mg $L^{-1}$ at the beginning and was at 3,025 mg $L^{-1}$ on the $90^{th}$ days.

Studies on Air-bridge fabrication using thermal evaporation method and its aplication (열적 증착법을 이용한 air-bridge 제작과 그 응용에 관한 연구)

  • 이일형;김성수;윤관기;김상명;이진구
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.33A no.12
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    • pp.53-58
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    • 1996
  • In this paper, a simple fabrication technique of an air-bridge for interconnection of isolated electrodes of microwave active and passive devices and MMIC's is proposed. The proposed air-bridge proceses are mainly combinations of thermal evaporation, positive photoresist and image reversal processes for easy lift-off of up to 2.0 .mu.m thick metal. According to the resutls of air-birdge processes, it is confirmed that air-gap and thickness of theair-bridge are about 3.5.mu.m, and 2.0.mu.m, respectively. And it is also possible to make the fine air-bridge with widths of 5~60.mu.m and post-intervals of 25~200.mu.m withot collapse. finally, GaAs power MESFET's and rectangular spiral inductors are fabricatd and measured in order to confirm of feasibility of the proposed air-bridge processes. The MAG of the fabricated power MESFET's is 10dB at 10GHz, and the inductance of the (200.mu. * 6 turns) rectangular spiral inductors 4.5 nH inX-band.

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COMMON FEATURES OF SPATIAL ORIENTATION OF DISK GALAXIES IN THE COMA AND VIRGO CLUSTER

  • Hul F. X.;Wu G. X.;SU H. J.;LIU Y. Z.;YUAN Q. R.
    • Journal of The Korean Astronomical Society
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    • v.29 no.spc1
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    • pp.53-54
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    • 1996
  • Based on the database of 128 disk galaxies (66 SO, 62 S and Irr) mailnly compiled from Kent and Gunn (1982) and Doi et a1.(1995) which is complete down to m < 15.6 mag within a radius of $3^{\circ}$, the orientation of spin vectors of disk galaxies of the Coma cluster has been analyzed. The results confirm the morphological dependence of the orientation of disk galaxies found from the analsis of the Virgo cluster. Common features of orientation of disk galaxies of both clusters are outlined.

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Estimation of Rail Joint Shape Using Signals Available in a MagLev Train (자기부상열차 계측 신호를 이용한 궤도 조인트 부 형상 추정)

  • Noh, M.;Song, I.;Nam, S.;Park, Y.-W.;Kang, H.
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2014.10a
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    • pp.622-624
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    • 2014
  • A maglev train records a host of physical variables such as gaps, voltages and currents for suspension control and monitoring purposes. These data available from a maglev contains wealth of information that can be explored for various uses. One possible of such application is to use the gap data to estimate the shape of the rail, especially at the joints where rails are connected. The eddy current sensors that measure the gap between the rail and the car body produce large peaks around the joints. The suspension controller discards these peaks. Since the shape of the peaks is related to the joint, however, these peaks can be utilized to estimate the shape of the joints. In this paper, we present preliminary results on estimating the joint shape using the peak data. The results show that the approach is promising, albeit several technical difficulties to overcome.

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High-pressure NMR application for α-synuclein

  • Kim, Jin Hae
    • Journal of the Korean Magnetic Resonance Society
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    • v.26 no.2
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    • pp.21-23
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    • 2022
  • High-pressure (HP) NMR is a powerful method to elucidate various structural features of amyloidogenic proteins. Following the previous mini-review recapitulating the HP-NMR application for amyloid-β peptides of the last issue [J. H. Kim, J. Kor. Mag. Reson. Soc. 26, 17 (2022)], the recent advancements in the HP NMR application for α-synuclein (α-Syn) are briefly summarized and discussed here. Although α-Syn is a well-known intrinsically disordered protein (IDP), several studies have shown that it can also exhibit heterogeneous yet partially folded conformations, which may correlate with its amyloid-forming propensity. HP NMR has been a valuable tool for investigating the dynamic and transient structural features of α-Syn and has provided unique insights to appreciate its aggregation-prone characters.