• 제목/요약/키워드: MICRO-VOID

검색결과 101건 처리시간 0.022초

Micro X-ray CT를 이용한 글라스 비드의 3차원 간극 구조 정량화 (Quantification of 3D Pore Structure in Glass Bead Using Micro X-ray CT)

  • 정연종;윤태섭
    • 한국지반공학회논문집
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    • 제27권11호
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    • pp.83-92
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    • 2011
  • 무질서하고 불균질한 형상을 갖는 지반 재료 내 간극 구조는 하중에 의한 재료의 변형 및 간극 내 유체의 흐름 등 물리 역학적 거동에 중요한 영향 인자이다. 최근 들어 X-ray CT에 의한 비파괴 검사를 통해 지반 재료의 내부 구조를 마이크로미터 단위의 높은 해상도를 통해 평가하는 기법이 사용되고 있다. CT 이미지는 재료의 많은 정보를 포함하고 있음에도 그에 따른 이미지 해석 기법의 개발이 다소 미흡하여 2, 3차원 이미지의 정성적 관찰 및 간극비와 같은 거시적인 물성치 획득만이 이루어지고 있다. 본 연구에서는 연속적으로 획득된 글라스 비드의 2차원 CT 이미지에 기반하여 3차원 입자 및 간극 구조를 형성하고, 복잡한 간극구조를 간극셀과 간극채널로 정량적 분리를 실시하였다. 이를 위해 좌표 변환법, 이진화, 들로네 삼각망, 그리고 유클리디안 거리변환법과 같은 이미지 프로세싱 기법을 3차원 CT 이미지에 적용하였고 불균질한 글라스 비드의 간극구조에 대해 정량적으로 간극셀의 분포 및 간극간의 연결도 평가가 가능함을 확인하였다.

A micro-computed tomographic evaluation of root canal filling with a single gutta-percha cone and calcium silicate sealer

  • Kim, Jong Cheon;Moe, Maung Maung Kyaw;Kim, Sung Kyo
    • Restorative Dentistry and Endodontics
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    • 제45권2호
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    • pp.18.1-18.9
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    • 2020
  • Objectives: The purpose of this study was to evaluate the void of root canal filling over time when a calcium silicate sealer was used in the single gutta-percha cone technique. Materials and Methods: Twenty-four J-shaped simulated root canals and twenty-four palatal root canals from extracted human maxillary molars were instrumented with ProFile Ni-Ti rotary instruments up to size 35/0.06 or size 40/0.06, respectively. Half of the canals were filled with Endoseal MTA and the other half were with AH Plus Jet using the single gutta-percha cone technique. Immediately after and 4 weeks after the root canal filling, the samples were scanned using micro-computed tomography at a resolution of 12.8 ㎛. The scanned images were reconstructed using the NRecon software and the void percentages were calculated using the CTan software, and statistically analyzed by 1-way analysis of variance, paired t-test and Tukey post hoc test. Results: After 4 weeks, there were no significant changes in the void percentages at all levels in both material groups (p > 0.05), except at the apical level of the AH Plus Jet group (p < 0.05) in the simulated root canal showing more void percentage compared to other groups. Immediately after filling the extracted human root canals, the Endoseal MTA group showed significantly less void percentage compared to the AH Plus Jet group (p < 0.05). Conclusions: Under the limitations of this study, the Endoseal MTA does not seem to reduce the voids over time.

고온히터 솔더접합부의 신뢰성 평가 및 예측 (Reliability Assessment and Prediction of Solder Joints in High Temperature Heaters)

  • 박은주;권대일;사윤기
    • 마이크로전자및패키징학회지
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    • 제24권2호
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    • pp.23-27
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    • 2017
  • 본 논문에서는 고온히터의 주 고장 원인이 되는 단자대 솔더 접합부의 손상 원인을 파악하여 사용 수명을 예측하는 방법을 제시하였다. 고온 히터 사용에 따르는 온도 스트레스로 인한 단자대 솔더 접합부의 영향을 알아보기 위해 동일한 부하 조건을 재현할 수 있는 고온히터 시편을 제작하였다. 고온히터 단자대의 단락은 주로 솔더접합부 내의 금속간 화합물이나 void로 인한 crack발생에서 기인한다. 가속시험을 통한 고장 재현을 위해 고온히터 시편을 $170^{\circ}C$의 오븐에서 장시간 동안 노출시키며 솔더 내부의 금속간 화합물 조성과 void의 변화를 측정하였다. 솔더 내의 금속간 화합물 층의 변화를 확인하기 위해서 주사전자현미경을 이용한 단면 분석을 시행하였고, 시편의 온도 스트레스로 인한 void 변화를 측정하기 위해 저항분광법을 이용한 특정 기준 주파수와 위상에 대한 신호를 실시간으로 측정하는 동시에 microCT를 이용하여 void 분율을 간헐적으로 관찰하였다. 시험결과 고온 노출 시간이 증가함에 따라 솔더 내부의 void의 분율이 증가하는 것을 확인하였으며 위상차 변화와 높은 상관관계가 있음을 확인하였다. 이 상관관계를 통해 온도 스트레스에 노출된 고온히터의 수명을 비파괴적으로 예측할 수 있음을 제시하였다.

원통형 셀 구조를 갖는 한방향 CFRP 적층 복합재료의 정적인장파괴거동 (Mechanical Properties and Fracture Behavior of Cylindrical Shell Type for Unidirectional CFRP Composite Material under Tension Load)

  • 오환섭
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 1998년도 추계학술대회 논문집
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    • pp.273-278
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    • 1998
  • In this paper, basic micro-mechanical properties of unidirectional CFRP composite shell such as bonding strength, fiber volume fraction and void fraction are measured and tensile strength test is performed with a fixture. And then fracture surfaces are observed by SEM. In case of basic micro-mechanical properties, bonding strength is reduce with decreasing of radius of each ply in a shell for the effect of residual stress, fiber volume fraction is smaller than plate, and void fraction is vise versa. For these reason, tensile strength of shell is smaller than plate fabricated with same prepreg. For failure mode shell has many splitted part along its length, and it is assumed that this phenomenon is caused by the difference of bonding strength for residual stress.

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자유단조 공정 시 내부 기공 거동 예측을 위한 멀티스케일 유한요소해석 연구 (A Study of Multiple Scale FEM Modeling for Prediction of Inner Void Closing Behavior in Open Die Forging Process)

  • 곽은정;강경필;이경훈
    • 소성∙가공
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    • 제21권5호
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    • pp.319-323
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    • 2012
  • In order to predict the internal void closing behavior in open die forging process, multiple scale modeling has been developed and applied. The huge size difference between ingot and inner void makes it almost impossible to simultaneously model the actual loading conditions and the void shape. Multiple scale modeling is designed to integrate macro- and micro- models effectively and efficiently. The void closing behavior was simulated at 39 different locations in a large ingot during upsetting and cogging. The correlation between the closing behavior and variables such as effective plastic strain and maximum compressive strain was studied in order to find an efficient measure for predicting the soundness of the forging.

Ti-6Al-4V합금의 고상 확산접합에 관한 연구 (A Study on the Solid State Diffusion Bonding of Ti-6Al-4V Alloy)

  • 강호정;강춘식
    • Journal of Welding and Joining
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    • 제15권6호
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    • pp.32-40
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    • 1997
  • Solid state diffusion bonding is the joining process performed by creep and diffusion, which is accelerated by heating below melting temperature and proper pressing, in vacuum or shielding gas atmosphere. By this process we can obtain sufficient joint which can't be expected from the fusion welding. For Ti-6Al-4V alloy, the optimum solid state diffusion bonding condition and mechanical properties of the joint were found, and micro void morphology at bond interface was observed by SEM. The results of tensile test showed sufficient joint, whose mechanical properties are similar to that of base metal. 850$^{\circ}$C, 3MPa is considered as the optimum bonding condition. Void morphology at interface is long and flat at the initial stage. As the percentage of bonded area increases, however, small and round voids are found. Variation of void shape can be explained as follows. As for the void shrinkage mechanism, at the initial stage, power law creep is the dominant, but diffusion mechanism is dominant when the percentage of bonded area is increased.

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열간 판재단조시 강괴 내부의 기공폐쇄에 관한 연구 (Study on Internal Void Closure in Slab ingot during Hot Plate Forging)

  • 조종래;김동권;김영득;이부윤
    • 소성∙가공
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    • 제5권1호
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    • pp.18-26
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    • 1996
  • In order to investigate the effect of pre-cooling of ingot on void closure in hot plate forging the internal strain and stress distributions are examined quantitatively by using ABAQUS. Simula-tions are carried out on a large slab ingot having the same temperature and the temperature gradient induced by air-cooling. It is shown that pre-cooling produces little effect on the strain behavior but remarkable effect on the hydrostatic stress at the central zone of ingot. The main factors for crushing micro-voids are the effective strain and the time integral of hydrostatic stress in the region surrounding the voids. Based on regression analysis it was found that the distortion of void can be expressed as a polynomial function of the two factors.

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In vitro Estimation of The Hounsfield Units and The Volume and Void of Canine Struvite Stones as Predictors of Fragility in Extracorporeal Shock Wave Lithotripsy

  • Wang, Ji-hwan;Hwang, Tae-sung;Jung, Dong-in;Yeon, Seong-chan;Lee, Hee-chun
    • 한국임상수의학회지
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    • 제34권3호
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    • pp.178-184
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    • 2017
  • The aim of this study was to determine whether Hounsfield units (HUs), volume, and various void parameters can predict stone fragility in extracorporeal shock wave lithotripsy (ESWL). HU, volume, porosity, number of voids/stone volume, and void distribution of 30 struvite stones were estimated using helical computed tomography (CT) and micro-CT. The number of shock waves necessary for full fragmentation was accepted as a measure of the stone fragility in ESWL. The correlations between the number of shock waves and the HU, volume, porosity, and number of voids/stone volume were examined. The number of shock waves of the two groups according to the void distribution was also compared. Stone volume correlated with the number of shock waves. Shell-patterned struvite stones were significantly less susceptible to fragmentation in ESWL than non-shell-patterned struvite stones. Stone volume and void distribution may be predictors of the outcome of ESWL treatment.

콘크리트 중의 염소이온 확산 특성에 관한 실험적 연구 (A Experimental Study on the Chloride Diffusion Properties in Concrete)

  • 박승범;김도겸
    • 콘크리트학회논문집
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    • 제12권1호
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    • pp.33-44
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    • 2000
  • Since the mechanism of chloride diffusion and its ratio in concrete depend on structural conditions and concrete as a micro-structure, if these are analyzed quantitatively, the long-term ageing of structures can be predicted. Although, a quantitative analysis of concrete micro-structure, in which the results are affected by various parameters, is very difficult, this can be done indirectly by the durability test of concrete. In this study, the compressive strength, void ratio and air permeability of concrete. In this study, the compressive strength, void ratio and air permeability of concrete are chosen as the parameters in concrete durability test, and these effects on test results are analysed according to changes of mixing properties. The relationships between parameters and chloride diffusion velocity is used for prediction models of chloride diffusion. The developed prediction models for the chloride diffusion according to mixing and physical properties, can be used to estimate the service life and corrosion initiation of reinforcing bars in marine structures.

LIPCA에 공급되는 전기장의 변화가 PZT 특성과 적층배향에 미치는 영향 (The Effect of Variable Electric Fields on the PZT Characteristic and Laminate Configuration in LIPCA)

  • 김철웅;남인창;윤광준
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.397-398
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    • 2006
  • The advanced piezoelectric ceramic composite actuator, which is called LIPCA with the FRP and the optimization of the laminate configuration, was performed to maximize the stress transfer and the fiber bridging effect. This study evaluated the effect of variable electric fields on the PZT characteristic, laminate configuration and fatigue characteristics under the resonance frequency, which meant the largest performance range and the changes of its interlaminar phase were also evaluated by stages. In conclusions, Comparing with the fatigue lift of intact LIPCA, the fatigue life of LIPCA embedded by the artificial delamination was decreased up to 50%. The micro void growth and the coalescence of epoxy were actively made at the interlaminar phase subject to the large tensile stress.

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