• 한국재료학회지
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• 제22권9호
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• pp.454-458
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• 2012

Various adhesive materials are used in flip chip packaging for electrical interconnection and structural reinforcement. In cases of COF(chip on film) packages, low temperature bonding adhesive is currently needed for the utilization of low thermal resistance substrate films, such as PEN(polyethylene naphthalate) and PET(polyethylene terephthalate). In this study, the effects of anhydride and dihydrazide hardeners on the low-temperature snap cure behavior of epoxy based non-conductive pastes(NCPs) were investigated to reduce flip chip bonding temperature. Dynamic DSC(differential scanning calorimetry) and isothermal DEA(dielectric analysis) results showed that the curing rate of MHHPA(hexahydro-4-methylphthalic anhydride) at $160^{\circ}C$ was faster than that of ADH(adipic dihydrazide) when considering the onset and peak curing temperatures. In a die shear test performed after flip chip bonding, however, ADH-containing formulations indicated faster trends in reaching saturated bond strength values due to the post curing effect. More enhanced HAST(highly accelerated stress test) reliability could be achieved in an assembly having a higher initial bond strength and, thus, MHHPA is considered to be a more effective hardener than ADH for low temperature snap cure NCPs.

• Journal of the Korean Wood Science and Technology
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• 제10권3호
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• pp.118-131
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• 1982

1. 이 연구(硏究)는 Yale대학교(大學校) 임과대학목재이학교실(林料大學木材利學敎室)에서 최근(最近) 새로히 쓰기 시작(始作)한 phenolic resin의 일종(一種)과 soy-bean glue 1auxein 10-B에 대(對)하여 assembly time의 변동(變動)이 제작(製作)된 합판(合板) shear strength에 어떠한 영향을 주는가를 알고 또한 그의 비교적(比較的) 적당(適當)한 실질적(實質的)인 assembly time의 범위를 결정(決定)하기 위하여 실시(實施)된 것이다. 2. 이 연구(硏究)에서 쓴 단판은 동실험실(同實驗室)에 실험용재료(實驗用材料)로 비치(備置)된 1/22in. 너도 밤나무(beech) 단판을 사용(使用)하였으며 수지는 phenolic resin U.S.P. low temperature liguid resorcinol type 와 Lauxein No. 10-B cold press water - resistant soygule 등으로 실험용(實驗用) sample을 구입(購入)하여 사용(使用)하였다. 3. 실험용(實驗用) ply-wood는 삼합식(三合式)으로 실험(實驗)을 하게 된 assembly time의 variation은 일분(一分)에서 시작(始作)하여 5, 10. 15, 25, 35, 50, 70분(分)등으로 8개(個)의 variation이 있게 하고 assembly 법(法)으로는 open assembly와 closed assembly의 2법(法)으로 하였으며 제작(製作)된 ply-wood의 성질비교(性質比較)는 dry test와 wet test의 shear strength test를 통(通)하여 나타나는 shear strength와 목파율을 가지고 하였다. 4. assembly time의 variation에 따른 합판의 shear strength와 목파율은 Table 1. 2. 3. 4에 표시(表示)된 바와 같은 결과(結果)를 보였으며 phenolic resin을 갖이고 closed assembly 법(法)으로 제작(製作)된 합판의 wet test를 제외하고는 모두 assembly time이 증가(增加)됨에 따라 shear strength와 목파율은 감소(減少)되여 가는 경향(傾向)을 보이고 있다. 그리고 실질적(實質的)으로 유효(有效)한 assembly time의 범위는 다음 표(表)(8)과 같다. 5. 이 실험(實驗)을 하는 동안 친절(親切)한 충고(忠告)와 지도편달(指導鞭達)를 애끼지 않고 도와주신 Yale 대학교(大學校) 목재이용학교수(木材利用學敎授) Dr. F.F.Wangaard씨(氏)와 Prof. Hess a. 그리고 실험실(實驗室) 담임자(擔任者)인 Mr. Clanch씨(氏)에게 충심(衷心)으로 사의(謝意)를 표시(表示)한다.

• 한국방사선학회논문지
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• 제11권5호
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• pp.353-359
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• 2017

대표적인 저강도 초음파 자극 기술인 음파영동은 초음파의 물리적 진동과 온열 효과를 이용하여 약물을 인체 표피 내부로 전달시키는 기법이다. 음파영동법은 치료 약물 전달의 효율을 높일 수 있으며, 인슐린이나 지질 등 분자 크기가 비교적 큰 약물의 전달에도 효과적이라는 장점을 갖는다. 본 연구에서는 효율적인 음파영동 치료를 위하여 대면적 단일 진동소자와 치료 부위에 약물 이송 기능을 갖는 복합 구조 초음파 변환기 어셈블리를 제안하였다. 또한, 치료 부위의 온도를 상승 및 유지시킬 수 있는 변환기 어셈블리 구조를 제안하고 유효성을 평가하였다. 본 연구에서 제안된 변환기 어셈블리는 지속적으로 정량의 약물을 제공하고, 가온을 통하여 약물 전달을 보조함으로써 초음파를 이용한 음파영동 시술의 효율을 향상시킬 수 있을 것으로 사료된다.

• Nuclear Engineering and Technology
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• 제23권3호
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• pp.352-362
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• 1991

가압 경수로의 노심 설계에 있어서 제한된 우라늄 자원의 효율적인 이용을 위한 다양한 방안으로 장주기 운전, 고연소도 및 저누출 장전 모형 통을 강구하고 있는 추세이다. 이러한 노심들은 원자로 운전 주기 전반에 걸친 공간적 출력 분포 제어와 잉여 반응도 제어를 위해 가연성 독물질을 사용하고 있다. 이와 관련하여 가연성 독물질 관리의 최적화 연구가 다각도로 진행되고 있다. 본 연구에서는 1990년도부터 국내 가압 경수로에 국산 핵연료가 장전되기 시작하면서 가도리니아 독봉을 사용하고 있으며 장차 주된 가연성 독물질로 쓰일 예정이므로 이에 대해서 분석을 수행하였다. 분석 결과 가도리니아 독봉은 열중성자 흡수 단면적이 매우 큰데서 기인한 특이한 연소 특성을 보이고 있다. 특히 집합체 내에서의 가도리니아 독봉의 위치에 따라 매우 다양한 출력 분포를 보이고 있다. 이러한 다양한 출력 분포 중에서 노심의 반경 방향 첨두 출력을 가능한 낮게하는 집합체 내에서의 가도리니아봉 위치 최적 선정을 위한 방법론을 제시하였다.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2009년도 추계학술대회 논문집
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• pp.149-149
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• 2009

Generally, Nafion ionomer is used in the polymer electrolyte fuel cell (PEFC) electrodes to achieve high power density. At the high temperature operation of PEFC, however, ionic conductivity of Nafion remarkably decreased due to the evaporation of water in Nafion polymer. Recently, many researchers have focused on using the Ionic Liquids(ILs) instead of water in Nafion polymer. ILs have intrinsic properties such as good electrochemical stability, high ionic conductivity, and non-flammability. Especially, ILs play a crucial role in proton conduction by the Grottuss mechanism and act as water in water-free Nafion polymer. However, it was found that the ILs was leached out of the polymer matrix easily. In this study, we prepared membrane electrode assemblies with various contents of ILs. The effect of ILs in the electrode of each designed was investigated by a cyclic voltammetry measurement and the cell performance obtained through a single cell test using H2/Air gases. Electrodes with different contents of ILs in catalyst layer were examined at high temperature and low humidified condition.

• 대한기계학회논문집A
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• 제30권4호
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• pp.373-378
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• 2006

We present the design, fabrication, and characterization of a multi-chip microelectrofluidic bench, achieving both electrical and fluidic interconnections with a simple, low-loss and low-temperature electrofluidic interconnection method. We design 4-chip microelectrofluidic bench, having three electrical pads and two fluidic I/O ports. Each device chip, having three electrical interconnections and a pair of two fluidic I/O interconnections, can be assembled to the microelectofluidic bench with electrical and fluidic interconnections. In the fluidic and electrical characterization, we measure the average pressure drop of $13.6{\sim}125.4$ Pa/mm with the nonlinearity of 3.1 % for the flow-rates of $10{\sim}100{\mu}l/min$ in the fluidic line. The pressure drop per fluidic interconnection is measured as 0.19kPa. Experimentally, there are no significant differences in pressure drops between straight channels and elbow channels. The measured average electrical resistance is $0.26{\Omega}/mm$ in the electrical line. The electrical resistance per each electrical interconnection is measured as $0.64{\Omega}$. Mechanically, the maximum pressure, where the microelectrofluidic bench endures, reaches up to $115{\pm}11kPa$.

• Journal of Electrochemical Science and Technology
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• 제10권1호
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• pp.22-28
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• 2019

To maximize the oxygen evolution reaction (OER) in the electrolysis of water, nano-grade $IrO_2$ powder with a low specific surface was prepared as a catalyst for a solid polymer electrolyte (SPE) system, and a membrane electrode assembly (MEA) was prepared with a catalyst loading as low as $2mg\;cm^{-2}$ or less. The $IrO_2$ catalyst was composed of heterogeneous particles with particle sizes ranging from 20 to 70 nm, having a specific surface area of $3.8m^2g^{-1}$. The anode catalyst layer of about $5{\mu}m$ thickness was coated on the membrane (Nafion 117) for the MEA by the decal method. Scanning electron microscopy (SEM) and electrochemical impedance spectroscopy (EIS) confirmed strong adhesion at the interface between the membrane and the catalyst electrode. Although the loading of the $IrO_2$ catalyst was as low as $1.1-1.7mg\;cm^{-2}$, the SPE cell delivered a voltage of 1.88-1.93 V at a current density of $1A\;cm^{-2}$ and operating temperature of $80^{\circ}C$. That is, it was observed that the over-potential of the cell for the oxygen evolution reaction (OER) decreased with increasing $IrO_2$ catalyst loading. The electrochemical stability of the MEA was investigated in the electrolysis of water at a current density of $1A\;cm^{-2}$ for a short time. A voltage of ~2.0 V was maintained without any remarkable deterioration of the MEA characteristics.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제45회 하계 정기학술대회 초록집
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• pp.252.2-252.2
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• 2013

ZnO nanostructures have a lot of interest for decades due to its varied applications such as light-emitting devices, power generators, solar cells, and sensing devices etc. To get the high performance of these devices, the factors of nanostructure geometry, spacing, and alignment are important. So, Patterning of vertically- aligned ZnO nanowires are currently attractive. However, many of ZnO nanowire or nanorod fabrication methods are needs high temperature, such vapor phase transport process, metal-organic chemical vapor deposition (MOCVD), metal-organic vapor phase epitaxy, thermal evaporation, pulse laser deposition and thermal chemical vapor deposition. While hydrothermal process has great advantages-low temperature (less than $100^{\circ}C$), simple steps, short time consuming, without catalyst, and relatively ease to control than as mentioned various methods. In this work, we investigate the dependence of ZnO nanowire alignment and morphology on si substrate using of nanosphere template with various precursor concentration and components via hydrothermal process. The brief experimental scheme is as follow. First synthesized ZnO seed solution was spun coated on to cleaned Si substrate, and then annealed $350^{\circ}C$ for 1h in the furnace. Second, 200nm sized close-packed nanospheres were formed on the seed layer-coated substrate by using of gas-liquid-solid interfacial self-assembly method and drying in vaccum desicator for about a day to enhance the adhesion between seed layer and nanospheres. After that, zinc oxide nanowires were synthesized using a low temperature hydrothermal method based on alkali solution. The specimens were immersed upside down in the autoclave bath to prevent some precipitates which formed and covered on the surface. The hydrothermal conditions such as growth temperature, growth time, solution concentration, and additives are variously performed to optimize the morphologies of nanowire. To characterize the crystal structure of seed layer and nanowires, morphology, and optical properties, X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), Raman spectroscopy, and photoluminescence (PL) studies were investigated.

• 한국기계가공학회지
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• 제16권1호
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• pp.9-16
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• 2017

This study describes the development of a 1-inch cryogenic glove valve for an LNG pumping system and localization development achieved through the performance test. The cryogenic valve used in the LNG pumping system plays an important role in maintaining a flow rate by LNG transportation. This trial manufactured goods, which was achieved through reverse engineering and developing the assembly process. The result of the leak test satisfied the internal pressure condition using the 78-bar normal temperature test and maintained the anti-leakage condition. Also, the result of the cryogenic leak test (BS 6364: low temperature test procedure) maintained anti-leakage at -196 and 52 bar, which satisfied the test standards.

• 한국자동차공학회논문집
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• 제25권3호
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• pp.350-359
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• 2017

This paper presents a new holistic development approach for the carbon continuous-fiber composite frame of an automotive sunroof assembly. The original steel frame has been designed to get higher bending stiffness with its corrugated cross-sectional shape. The new approach uses the prepregs of a fast cure epoxy and PCM manufacturing processing. For higher productivity, the new frames feature a very simple plat cross sectional shape but achieve high bending stiffness through the laminate design. The sandwich structure with a PET foam core was presented. The frames were made of carbon UD laminae covered single carbon fabric on the outer surfaces. The fabrics provide torsional stiffness and also hold the carbon UD fibers floating in the low viscous epoxy resin of prepregs at the curing temperature during processing. The final product yields approximately 18 % savings in weight compared with the original.