• 한국재료학회지
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• 제26권11호
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• pp.590-597
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• 2016

In this study, six kinds of low-carbon steel specimens with different ferrite-pearlite microstructures were fabricated by varying the Nb content and the transformation temperature. The microstructural factors of ferrite grain size, pearlite fraction, interlamellar spacing, and cementite thickness were quantitatively measured based on optical and scanning electron micrographs; then, Charpy impact tests were conducted in order to investigate the correlation of the microstructural factors with the impact toughness and the ductile-brittle transition temperature (DBTT). The microstructural analysis results showed that the Nb4 specimens had ferrite grain size smaller than that of the Nb0 specimens due to the pinning effect resulting from the formation of carbonitrides. The pearlite interlamellar spacing and the cementite thickness also decreased as the transformation temperature decreased. The Charpy impact test results indicated that the impact-absorbed energy increased and the ductile-brittle transition temperature decreased with addition of Nb content and decreasing transformation temperature, although all specimens showed ductile-brittle transition behaviour.

• Korean Chemical Engineering Research
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• 제50권1호
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• pp.6-10
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• 2012

본 연구의 목적은 styrene-butadiene-styrene(SBS) 블록공중합체와 폐타이어 고무분말(crumb rubber, CR)로 개질한 아스팔트의 저온접착특성에 대해 파라핀오일 가소제의 영향에 대한 것이다. SBS/CR로 개질한 아스팔트 블렌드와 파라핀오일/SBS/CR 아스팔트 블렌드의 온도 민감성을 침입도와 연화점으로 측정하였다. 형광현미경으로 파라핀오일/SBS/CR 아스팔트 블렌드에 대한 개질제들의 분산 상태와 만능시험기로 저온에서 접착성질을 각각 측정하였다. 저온접착시험에서 SBS 함량의 증가와 파라핀오일 함량 5 wt % 및 10 wt %에서 접착강도와 변형률이 증가하였다. $-20^{\circ}C$에서 측정한 접착강도와 강인성은 파라핀오일이 10 wt %와 SBS 공중합체의 양이 6 wt %인 조성에서 최대값을 얻었다. SBS/CR/아스팔트 블렌드에서 파라핀오일의 첨가는 유연성을 부여하는 효과를 나타내고, 저온에서 강인성의 증가를 가져오는 것을 확인하였다.

• 열처리공학회지
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• 제27권5호
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• pp.235-241
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• 2014

Effects of rolling and cooling conditions on microstructures and mechanical properties of high-deformable pipeline steels were investigated in this study. Six kinds of pipeline steels were fabricated by varying rolling and cooling conditions, and their microstructures were analyzed by scanning electron microscopy, electron back-scattered diffraction, and transmission electron microscopy. Tensile and Charpy impact tests were conducted on the steels in order to examine the mechanical properties. The steels rolled in the two-phase region showed better low-temperature toughness than those in the single-phase region due to the larger amount of ferrites having high-angle boundaries, although they have lower strength and absorbed energy. The steel rolled in single-phase and finish-cooled at higher temperature showed a good combination of high strength and good low-temperature toughness as well as excellent deformability of the lowest yield ratio and the highest uniform elongation because of the presence of fine ferrite and a mixture of various low-temperature transformation phases.

• 대한기계학회논문집A
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• 제30권8호
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• pp.965-975
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• 2006

High pressure turbine blades are one of the key components in fossil power plants operated at high temperature. The blade is usually made of 12Cr steel and its operating temperature is above $500^{\circ}C$. Long term service at this temperature causes material degradation accompanied by changes in microstructures and mechanical properties such as strength and toughness. Quantitative assessment of reduction of strength and toughness due to high temperature material degradation is required for residual life assessment of the blade components. Nondestructive technique is preferred. So far most of the research of this kind was conducted with low alloy steels such as carbon steel, 1.25Cr0.5Mo steel or 2.25Cr1Mo steel. High alloy steel was not investigated. In this study one of the high Cr steel, 12Cr steel, was selected for high temperature material degradation. Electrochemical polarization method was employed to measure degradation. Strength reduction of the 12Cr steel was represented by hardness and toughness reduction was represented by change of transition temperature, FATT. Empirical relationships between the electrochemical polarization parameter and significance of material degradation were established. These relationship can be used for assessing the strength and toughness on the aged high pressure blade components indirectly by using the electrochemical method.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.583-588
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• 2002

The purpose of the study is to evaluate fracture toughness on the Laser and the electron beam welded joints of high tensile steels (HT500, HT550, HT650) by using 3-point bend CTOD and Charpy impact test. WM (weld metal) CTOD tests have been carried out using two kinds of CTOD specimen, the Laser beam welding (108mm length, and 24mm width, and 12mm thickness) and the electron beam welding (l71mm length, and 38mm width, and 19mm thickness). WM Charpy impact specimen is a standard V-notch type, and the temperature of the experiment is changed from -45 to 20 degree of centigrade. FE-analysis is also performed in order to investigate the effect of stress-strain fields on fracture characteristics. Results of the standard V-notch Charpy test are influenced by strength mis-match effect and the absorbed energy vE depends on crack path, and The transition temperature of Laser beam welded joints is more higher than that of electron beam welded joints. Results of the 3-point bend test give low critical CTOD and the crack path is in the weld metal of al specimens. These results indicate fracture toughness characteristics of the welded joints and transition temperature of HT500 are similar both a Laser beam welded joint and an electron beam welded joint. But the fracture toughness and the transition temperature of the electron beam welded joints of HT550 and HT650 are higher than those o the Laser beam welded joints.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2000년도 춘계학술대회 논문집 전자세라믹스 센서 및 박막재료 반도체재료 일렉트렛트 및 응용기술
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• pp.72-75
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• 2000

The effect of $Al_2O_3+Y_2O_3$ additives on fracture toughness of ${\beta}-SiC-TiB_2$ composites by hot-pressed sintering were investigated, The ${\beta}-SiC-TiB_2$ ceramic composites were hot-presse sintered and annealed by adding 4, 8, 12wt% $Al_2O_3+Y_2O_3$(6 : 4wt%) powder as a liquid forming additives at low temperature($1800^{\circ}C$) for 4h. In this microstructures, the relative density is over 97% of the theoretical density and the porosity increased with increasing $Al_2O_3+Y_2O_3$ contents because of the increasing tendency of pore formation. But the fracture toughness showed the highest of $7.0MPa{\cdot}m^{1/2}$ for composites added with 12wt% $Al_2O_3+Y_2O_3$ additives at room temperature. The electrical resistivity showed the lowest of $1.59\times10^{-3}\Omega{\cdot}cm$ for composite added with 8wt% $Al_2O_3+Y_2O_3$ additives at room temperature and is all positive temperature coefficient resistance(PTCR} against temperature up to $700^{\circ}C$.

• 대한기계학회논문집A
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• 제39권5호
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• pp.491-497
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• 2015

본 논문은 필라멘트 와인딩 공법으로 제작된 구배 단면을 갖는 돔 분리형 복합재 압력용기 접착체결부의 온도영향에 따른 층간파괴인성 평가를 위해 모드 I, II 그리고 혼합모드의 시험적 평가를 수행하였다. 모드 I과 혼합모드 층간파괴인성은 DCB 시편을 사용하였으며, 모드 II 층간파괴인성은 ENF 시편을 사용하여 평가하였다. 와인딩 각도는 $[{\pm}10^{\circ}]_6$, $[{\pm}27^{\circ}]_6$ 그리고 ($[{\pm}10^{\circ}]_3/FM73/[{\pm}10^{\circ}]_3$)이며 곡면 단면을 고려하였다. 시험 평가에 적용된 온도 환경은 환경 챔버와 전기로를 이용하여 $-30^{\circ}C$에서 $60^{\circ}C$로 조성하였다. 층간파괴인성에 온도가 미치는 영향을 평가한 결과, 층간파괴인성은 저온에서 높게 나타났으며, 온도가 증가함에 따라 감소하는 경향을 확인하였다. 시편 종류별 결과에서는, 돔부와 헬리컬부가 접착체결된 $[{\pm}10^{\circ}]_3/FM73/[{\pm}10^{\circ}]_3$ 와인딩 시편이 가장 높은 층간파괴인성을 가짐을 확인하였다.

• 한국가스학회지
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• 제2권3호
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• pp.78-87
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• 1998

액화천연가스 저장용 소재로 널리 사용되고 있는 Ni 함유 페라이트 강은 $2-3\%,\;5.5\%,\;9\%$ 그리고 $13\%$ Ni 강으로 크게 분류되고 그 중에서도 경제성이 있으며 $-196^{\circ}C$까지의 온도에서 파괴인성과 용접성이 매우 우수한 $9\%$ Ni강이 가장 많이 사용되고 있다. 저온에서의 우수한 파괴인성은 Ni 첨가에 의한 잔류 오스테나이트 및 페라이트의 안정화 그리고 열처리효과에 기인한다. 최근 액화천연가스 저장탱크의 대형화에 따라 보다 두껍고 인성이 큰 소재가 요구되며, 따라서 이에 부응하는 저온용 Ni 함유 페라이트 강의 개발동향을 소개하였다.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2004년도 학술대회지
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• pp.355-361
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• 2004

Ceramic femoral heads in the total hip replacement have been developed to reduce the polyethylene liner wear, Alumina and zirconia (3Y-TZP) having the excellent tribological properties are coupled against acetabular cups of polyethylene and are used in clinical application worldwide. However, alumina has a risk of catastrophic failure, and zirconia has the low temperature degradation in spite of enhanced fracture toughness. Recently, novel zirconia/alumina composite is very attractive due to the low temperature degradation (LTD)-free character and high fracture toughness. In the present study, we focus on the wear of ceramic on ceramic, which are able to be used as femoral heads and acetabular cups. Therefore, LTD-free zirconia/alumina composites with three compositions are made in a form of disk and cylinder, and the wear of the composites is performed on pin-on-disk type wear tester. The wear is conducted with or without lubricant. All the composites fabricated with the different composition show the good wear resistance.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2001년도 추계학술발표대회 개요집
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• pp.247-251
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• 2001