• Title/Summary/Keyword: Low temperature phase

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재결정제어압연용 저탄소강의 연속냉각 상변태거동에 미치는 Nb 첨가효과 (Effect of Nb Addition on Phase Transformation Behavior during Continuous Cooling in Low Carbon Steels for Recrystallization Control Rolling)

  • 이상우;주웅용
    • 열처리공학회지
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    • 제13권5호
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    • pp.346-354
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    • 2000
  • Effect of Nb addition on the phase transformation behavior was studied through continuous cooling transformation tests after reheating(reheating CCT) and deforming(deforming CCT) the 0.07%C-1.3%Mn-0.015%Ti-(0~0.08)% Nb steels. Transformation temperatures for deforming CCT were lower than those for reheating CCT, and the critical cooling rate for bainite transformation during deforming CCT was lower than that during reheating CCT. These enhanced hardenability for deforming CCT was considered to come from the sufficient solid solution of Nb in austenite during high temperature reheating before deformation. With Nb addition, the phase transformation temperature decreased, the bainite formation was enhanced, and the hardness of steel increased. Furthermore, these phenomena were more remarkable for deforming CCT than for reheating CCT. From the results, Nb-Ti bearing low carbon steel was considered to be a very favorable alloy system with good strength/toughness balance by recrystallization control rolling process.

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UV중합성 수지와 알키드 수지 혼합물의 경화특성 및 상분리 구조에 관한 연구 (A Study on Curing Properties and Structures of Phase Separation for UV-Curable Resing and Alkyd Resin Blends)

  • 최정병
    • 한국인쇄학회지
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    • 제18권1호
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    • pp.13-24
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    • 2000
  • UV-curable resin has the properties of quick-drying, high productivity at low temperature, energy, space saving, solventless, non-polluting and low-stinking, and thus, UV-curing system has been widely used in the fields of printing inks, adhesives, paints and coating agents. This study has been executed to develop a new functionnal material by the polymerization induced phase separation. The results obtained were as follows. As for the curing properties of the monomer/prepolymer/alkyd resin blends, it was found out that there was a peak by the polymerization induced phase separation when measuring the changes of viscosity and elasticity. It was also found out that such polymerization phase separation occurred in case that the alkyd resin contents were 20wt% and 30wt% and not found at the contents of 40wt%. Therefore, it would be desirable to maintain the contents of alkyd resin at less than 30wt% in order to use the polymerization induced phase separation.

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압축성 이상(二相) 충격파관 문제에 대한 엄밀 리만해법 (EXACT RIEMANN SOLVERS FOR COMPRESSIBLE TWO-PHASE SHOCK TUBE PROBLEMS)

  • 염금수;장근식
    • 한국전산유체공학회지
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    • 제15권3호
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    • pp.73-80
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    • 2010
  • In this paper, we present the exact Riemann solver for the compressible liquid-gas two-phase shock tube problems. We hereby consider both isentropic and non-isentropic two-phase flows. The shock tube has a diaphragm in the mid-section which separates the liquid medium on the left and the gas medium on the right. By rupturing the diaphragm, various waves are observed on the phasic field variables such as pressure, density, temperature and void fraction in the form of rarefaction wave, shock wave and material interface (contact discontinuity). Both phases are treated as compressible fluids using the linearized equation of state or the stiffened-gas equation of state. We solve several shock tube problems made of a high/low pressure in the liquid and a low/high pressure in the gas. The wave propagations are well resolved by the exact Riemann solutions.

저온소결 (Ba0.86Ca0.14)(Ti0.85Zr0.12Sn0.03)O3계 세라믹스의 미세구조와 유전 특성 (Microstructure and Dielectric Properties of Low Temperature Sintering (Ba0.86Ca0.14)(Ti0.85Zr0.12Sn0.03)O3 System Ceramics)

  • 류주현
    • 한국전기전자재료학회논문지
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    • 제29권7호
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    • pp.404-407
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    • 2016
  • In this study, to develop low temperature sintering capacitor composition ceramics with the good dielectric properties, $(Ba_{0.86}Ca_{0.14})(Ti_{0.85}Zr_{0.12}Sn_{0.03})O_3$ (BCTZ) ceramics were prepared by the conventional solid-state reaction method. The effects of $B_2O_3$ addition on the dielectric properties and microstructure was investigated. The XRD patterns demonstrated that all the specimens showed Perovskite phase, and secondary phases are indicated in the measurement range of XRD. And also, temperature coefficient of capacitance(TCC) of all the specimen sintered at $1,180^{\circ}C$ showed +3~-56% except for x=0.006. For all the specimens, observed one peak was tetragonal cubic difuse phase transition temperature(Tc), which is located in the vicinity of room temperature.

GroEL/ES Chaperone and Low Culture Temperature Synergistically Enhanced the Soluble Expression of CGTase in E. coli

  • Park, So-Lim;Kwon, Mi-Jung;Kim, Sung-Koo;Nam, Soo-Wan
    • Journal of Microbiology and Biotechnology
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    • 제14권1호
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    • pp.216-219
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    • 2004
  • The effect of culture temperature on the production of soluble form of B. macerans cyclodextrin glucanotransferase (CGTase) in recombinant E. coli was investigated. E. coli cell was cotransformed with two plasmids (pTCGT1 and pGroll) in which the cgt and groEL/ES genes are under the control of T7 promoter and pzt-1 promoter, respectively. When tetracycline (10 ng/ml) and IPTG (l mM) were added as inducers at the early-exponential phase (2 h) and mid-exponential phase (3h), respectively, the solubilization of the inclusion body CGTase was greatly dependent on the temperature of the culture. At low culture temperature of $25^\circ{C}$, 2- or 3-fold higher activity and specific activity were obtained over $37^\circ{C}$. SDS-PAGE analysis revealed that about 62% of CGTase in the total CGTase protein was found in the soluble fraction by applying overexpression of GroEL/ES chaperone and by cultivation of E. coli at $25^\circ{C}$, whereas 33% of CGTase was detected in the soluble fraction at $37^\circ{C}$. Therefore, the expression of GroEL/ES and cultivation at $25^\circ{C}$ greatly enhanced the soluble production of CGTase in E. coli.

Circadian Rhythms of Melatonin, Thyroid-Stimulating Hormone and Body Temperature: Relationships among those Rhythms and Effect of Sleep-Wake Cycle

  • Kim, Mi-Seung;Lee, Hyun J.;Im, Wook-Bin
    • Animal cells and systems
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    • 제6권3호
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    • pp.239-245
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    • 2002
  • Plasma melatonin, thyroid-stimulating hormone (TSH) and body temperature were measured simultaneously and continuously before and after the sleep-wake cycle was shifted in 4 healthy males and changes in the circadian rhythm itself and in the phase relationship among these circadian rhythms were determined. Normal sleep-wake cycle (sleep hours: 2300-0700) was delayed by 10 h (sleep hours: 0900-1700) during the experiment. Even after this shift the typical melatonin rhythm was maintained: low during daytime and high during night. The melatonin rhythm was gradually delayed day by day. The TSH rhythm was also maintained fundamentally during 3 consecutive days of altered sleep-wake cycle. The phase was also delayed gradually but remarkably. The daily rhythm of body temperature was changed by the alteration of sleep-wake cycle. The body temperature began to decrease at the similar clock time as in the control but the decline during night awake period was less steep and the lowered body temperature persisted during sleep. The hormonal profiles during the days of shifted sleep/wake cycle suggest that plasma melatonin and TSH rhythms are basically regulated by an endogenous biological clock. The parallel phase shift of melatonin and TSH upon the change in sleep-wake cycle suggests that a common unitary pacemaker probably regulates these two rhythms. The reversal phase relationship between body temperature and melatonin suggests that melatonin may have a hypothermic effect on body temperature. The altered body temperature rhythm suggests that the awake status during night may inhibit the circadian decrease in body temperature and that sleep sustains the lowered body temperature. It is probable but uncertain that there ave causal relationships among sleep, melatonin, TSH, and body temperature.

Novel deposition technology for nano-crystalline silicon thin film at low temperature by hyper-thermal neutral beam assisted CVD system

  • Jang, Jin-Nyoung;Song, Byoung-Chul;Oh, Kyoung-Suk;Yoo, Suk-Jae;Lee, Bon-Ju;Choi, Soung-Woong;Park, Young-Chun;Hong, Mun-Pyo
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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    • pp.1025-1027
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    • 2009
  • Novel low temperature deposition process for nano-crystalline Si thin film is developed with the hyper-thermal neutral beam (HNB) technology. By our HNB assisted CVD system, the reactive particles can induce crystalline phase in Si thin films and effectively combine with heating effect on substrate. At low deposition temperature under $80^{\circ}C$, the HNB with proper incident energy controlled by the reflector bias can effectively enhance the nano-crystalline formation in Si thin film without any additional process. The electrical properties of Si thin films can be varied from a-Si to nc-Si according to change of HNB energy and substrate temperature. Characterization of these thin films with conductivity reveal that crystalline of Si thin film can increase by assist of HNB with appropriate energy during low temperature deposition. And low temperature prcoessed nc-Si TFT performance has on-off ratio as order 5.

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전력반도체 패키징을 위한 Transient liquid phase 접합 기술 (Trasient Liquid Phase bonding for Power Semiconductor)

  • 노명훈;;정재필;김원중
    • 마이크로전자및패키징학회지
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    • 제24권1호
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    • pp.27-34
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    • 2017
  • Recently, a demand in sustainable green technologies is requiring the lead free bonding for high power module packaging due to the environmental pollution. The Transient-liquid phase (TLP) bonding can be a good alternative to a high Pb-bearing soldering. Basically, TLP bonding is known as the combination of soldering and diffusion bonding. Since the low melting temperature material is fully consumed after TLP bonding, the remelting temperature of joint layer becomes higher than the operating temperature of the power module. Also, TLP bonding is cost-effective process than metal nanopaste bonding such as Ag. In this paper, various TLP bonding techniques for power semiconductor were described.

Characteristics of Sticking Coefficient in BSCCO Thin Film

  • 조춘남;안준호;오재한;최운식;박용필
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 제2회 학술대회 논문집 일렉트렛트 및 응용기술전문연구회
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    • pp.59-63
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    • 2000
  • BSCCO thin films are fabricated via a co-deposition process by an ion beam sputtering with an ultra-low growth rate, and sticking coefficients of the respective elements are evaluated. The sticking coefficient of Bi element exhibits a characteristic temperature dependence : almost a constant value of 0.49 below $730^{\circ}C$ and decreases linearly with temperature over $730^{\circ}C$ This temperature dependence can be elucidated from the evaporation and sublimation rates of bismuth oxide, $Bi_2O_3$, from the film surface. It is considered that the liquid phase of the bismuth oxide plays an important role in the Bi(2212) phase formation in the co-deposition process.

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Magnetic and magneto-optical properties of two metallic phase magnet Co/Co$_2$TiSn films

  • Kim, T. W.;Lee, J. W.;S. C. Shin
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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    • pp.375-377
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    • 1998
  • The magneto-optical properties of Co/Co$_2$TiSn two-phase magnet films were studied. These films show that relatively large Kerr rotations which are -0.4 deg. at the wavelength of 400 nm, compared to that of pure Co. It is conceivable that the magneto-optical effects may be due to both contributions of ferromagnetic Co matrix and ferromagnetic Co$_2$TiSn Heusler alloy precipitate. The perpendicular magnetization curve domonstrates a typical bubble domain hysteresis loop. the saturation magnetization change of the annealed film is less sensitive to temperature in the low temperature region and the Curie temperature of Co$_2$TiSn Heusler alloy precipitate is a little higher in the annealed film. These can be explained by the increase of the number of Co-Co exchange interaction in Heusler alloy structure resulting from the change of chemical ordering by annealing.

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