• Transactions of Materials Processing
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• v.5 no.4
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• pp.327-336
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• 1996

The effect of dynamic strain aging on high temperature deformation behaviour of the A-Mg alloy was investigated by strain rate change tests and stress relaxation tests between 20$0^{\circ}C$and 50$0^{\circ}C$. Yield point, short stress transient and periodic discontinuities on the stress-strain curve were considered as an evidence of the effect of dynamic strain aging. With this criterion two distinct strain rate-temperature regimes could be manifested. Dynamic strain aging was considered to be effective in the high temperature-low strain rate regime, whereas dynamic recovery was a dominant deformation mechanism in the low temperature-high strain rate regime. It was found that dynamic strain aging in the high temperature deformation was governed by the mechcanism of diffusion-controlled, viscous dislocation movement.

• The Journal of Advanced Prosthodontics
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• v.1 no.3
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• pp.113-117
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• 2009

STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad $S\ddot{a}ckingen$, Germany) were prepared in 40 mm (length) $\times$ 4 mm (width) $\times$ 3 mm (height) samples. Specimens were artificially aged in distilled water by heat-treatment at a temperature of 75, 100, 125, 150, 175, 200, and $225^{\circ}C$ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences ($\alpha$= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below $125^{\circ}C$ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above $150^{\circ}C$, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above $100^{\circ}C$. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above $175^{\circ}C$. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%.

• Journal of the Korean Ceramic Society
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• v.27 no.8
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• pp.971-978
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• 1990

The ifluence of transformability and stabilized effects in tetragonal phase on the isothermal phase transformation of Y-TZP at low temperature were investigated. The transformability of Y-TZP powders were gradually increased with calcination temeprature and reached maximum at critical temperature, but when the Y-TZP powders were calcined above critical temperature, transformability of Y-TZP were gradually decreased with increasing calcination temperature. It was concluded that maximum transformability was appeared because particle size effects decreased and constrain effects increased with calcined temperature. The isothermal phase transformation during aging at 25$0^{\circ}C$ only observed in Y-TZP stabilized by constrain effects and the amounts of transformation during aging at 25$0^{\circ}C$ only observed in Y-TZP stabilized by constrain effects and the amount of transformed monoclinic phase during aging decreased with increasing constrain effects. From these results, the mechanism of isothermal phase transformation and degradation behaviors at low temperature in Y-TZP was concluded that occurred by decreasing of constrain effects due to stress relaxation at grian boundary.

• Journal of Welding and Joining
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• v.26 no.5
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• pp.60-65
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• 2008

Ferritic stainless steels of the 400 series have been available for automotive exhaust system, heat exchanger, radiater etc. in various industrial because heat resistance, corrosion resistance and strength are excellent. Especially, automotive exhaust system is required good heat resistance because typical temperature of exhaust system exposed during operation of engine is reach up to $800^{\circ}C$. However, research for effect of high temperature in ferritic stainless steels is not enough. In this study, high temperature tensile properties of lap weld of ferritic stainless steels(STS 429) were investigated. In accordance with heat input, lap welds had been produced and were evaluated at high temperature($800^{\circ}C$) to compare high temperature tensile properties. In addition, room temperature tensile tests were carried out for non-aging and aging specimens. As a result of R.T tensile test, non-aging specimens were fractured in base metal except for low heat input specimen and aging specimens were fractured in weld metal. Also high temperature tensile test were carried out by aging specimen. After high temperature tensile test, fracture of aged specimen was occurred in base metal except for low heat input specimen. Fracture surface of low heat input specimen in weld metal was confirmed as brittle fracture with observation using scanning electron microscope(SEM). Significant decrease in ultimate tensile strength (between 82 and 85%) was observed for aged ferritic stainless steels(STS 429) when tested at high temperature.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2017.05a
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• pp.915-922
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• 2017

The study on the thermal and oil resistance rubber composite, 2016. [6] predicted the lifetime of Fluorocarbon Rubber by accelerating aging at high temperature ($150^{\circ}C$, $175^{\circ}C$, $200^{\circ}C$). general rubber products are likely to exhibit different properties depending on the degradation factors such as temperature, humidity, ozone, light, emulsion, mechanical and electrical stress. To solve these problems, We compared the rate of change about tensile strength, elongation rate, volume change rate, weight change rate, thickness change rate, thermal conductivity in low temperature promoting aging on the basis of predictive lifetime of high temperature promoting aging. As a result of the review, the required life expectancy was satisfied, but there was a slight difference in the rate of change between the high-temperature promoted aging life result and the low temperature promoted aging life result. The cause was a reduction in "tensile strength / elongation" and an increase in "volume / weight / thickness" caused by the main chain decomposition of fluorine rubber due to aging at high temperature promoting aging. However, the low temperature promoting aging was caused by the curing reaction of fluorine rubber at $80^{\circ}C$. The tensile strength / elongation and volume / weight / thickness changes were small.

• Composites Research
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• v.30 no.1
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• pp.7-14
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• 2017

In this paper, the inter-lamina shear strength (ILSS) of multi-wall carbon nanotube (MWNT) reinforced carbon fiber reinforced plastics (CFRP) and thin-ply composites were verified under low earth orbit (LEO) space environment. CFRP, MWNT reinforced CFRP, thin-ply CFRP and MWNT reinforced thin-ply CFRP were tested after aging by using accelerated ground simulation equipment. The used ground simulation equipment can simulate high vacuum ($2.5{\times}10^{-6}torr$), atomic oxygen (AO, $9.15{\times}10^{14}atoms/cm^2{\cdot}s$), ultraviolet light (UV, 200 nm wave length) and thermal cycling ($-70{\sim}100^{\circ}C$) simultaneously. The duration of aging experiment was twenty hours, which is an equivalent duration to that of STS-4 space shuttle condition. After the aging experiment, ILSS were measured at room temperature ($27^{\circ}C$), high temperature ($100^{\circ}C$) and low temperature ($-100^{\circ}C$) to verify the effect of operation temperature. The MWNT and thin-ply shows good improvement of ILSS at ground condition especially with the thin-ply. And after LEO exposure large degradation of ILSS was observed at MWNT added composite due to the thermal cycle. And the degradation rate was much higher under the high temperature condition. But, at the low temperature condition, the ILSS was largely recovered due to the matrix toughening effect.

• Korean Journal of Food Science and Technology
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• v.21 no.4
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• pp.549-555
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• 1989

The effect of high temperature aging on the meat tenderness improvement was studied, and also the effect of salt, pyrophosphate and succinic anhydride on binding characteristics of restructed beef were compared. At high temperature aging, shear force value decreased and myofibrillar fragmentation index increased as the aging progressed. From the electronic microscopic observation, the morphological change of myofibril appeared much faster when the meat was aged at high temperature. Added salt increased TBA values and rupture strength while reducing cooking loss. Increase in pyrophosphate decreased rooking loss and Increased rupture strength and TBA value. When salt and pyrophosphate were combined, the effects were somewhat additive. Added succinic anhydride increased cooking loss and hardness and decreased color rating, acceptability rating and adhesiveness, but cohessiveness was not significantly different from control group containing salt and pyrophosphate. The results suggest that high temperature aging have greater improving effect of meat tenderness of Korean native male cattle compared to low temperature aging and addition of succinic ahydride in combination with salt and pyrophosphate reduce binding ability of restructured beef.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.28 no.12
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• pp.1968-1973
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• 2004

Structural degradations are often experienced on the components of nuclear power plants in reactor pressure vessels (RPV) and steam generators (SG) when these components are exposed to high temperature and high pressure for a long period of time. Such conditions result in the change of microstructures and of mechanical properties of materials, which requires an evaluation of the safeguards related to structural integrity. In a primary reactor cooling system (RCS), a dissimilar weld zone exists between cast stainless steel (CF8M) in a pipe and low-alloy steel (SA508 cl.3) in a nozzle. Thermal aging is observed in CF8M as the RCS is exposed for a long period of time under the operating temperature between 290 and 33$0^{\circ}C$. Under the same conditions, it is well known that degradation is not observed in low alloy steel. An investigation of the effect of thermal aging on the various mechanical properties of the dissimilar weld zone is required. The purpose of the present investigation is to find the effect of thermal aging on the dissimilar weld zone. The specimens are prepared by an artificially accelerated aging technique maintained for various times at 43$0^{\circ}C$, respectively. Then, The various mechanical test for the dissimilar welds are performed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.203-206
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• 2008

Transformation of austenite to martensite during cold rolling has been widely used to strengthen metastable austenitic stainless steel grades. Aging treatment of cold worked metastable austenitic stainless steels, including ${\alpha}'$-martensite phase, results in the further increase of strength, when aging is performed in $200^{\circ}C$ to $450^{\circ}C$ temperature range. The purpose of the present study was to evaluate the effect of time and temperature on the stress-strain behavior of cold worked austenitic stainless steels. The amount of ${\alpha}'$-martensite during cold working and aging was examined by ferrite scope and X-ray diffraction (XRD). During aging at $450^{\circ}C$ for 1hr, tensile strength dramatically increased by 150MPa. Deformed metastable austenitic steels containing the "body-centered" ${\alpha}'$-martensite are strengthened by the diffusion of interstitial solute atoms during aging at low temperature.

• Journal of the Korean Society for Heat Treatment
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• v.13 no.1
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• pp.1-9
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• 2000

The microstructural characteristics and low temperature tensile properties between $25^{\circ}C$ and $-196^{\circ}C$ for as-welded and age hardened specimen by using Al 5083-H321 for base metal, 5083-5356 and 5083-4043 weldments have been investigated. The hardness of 5083-5356 weldment decreases with aging treatment, whereas the weld region of 5083-4043 weldment shows remarkable increase in hardness after aging due to the precipitation of fine Si particle at the grain boundaries and interiors. Low temperature tensile properties of 5083 AI base metal, 5083-5356 and 5083-4043 weldments appear to be the increment of tensile strengths and elongations at the room temperature and $-196^{\circ}C$, while the decrement of tensile properties around $-50^{\circ}C$ is shown. Through the observation of fine serration to fracture in the stress-strain curve and tensile fractography, the increment of localized deformation leading to promote the neck initiation and the increment of the dimple size cause to decrease in tensile strengths and elongations around $-50^{\circ}C$. For the tensile specimen of the 5083 base metal, 5083-5356 and 5083-4043 weldments, the reason to increase in elongation after solution and aging treatment is the diminishment of fine pit, the resolution of Mg into the matrix and the spheridization of the eutectic Si.