• Computers and Concrete
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• v.16 no.2
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• pp.261-274
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• 2015

This study established the standard recommended values and expansion fracture threshold values for the content of steel slag in controlled low-strength materials (CLSM) to ensure the appropriate use of steel slag aggregates and the prevention of abnormal expansion. The steel slags used in this study included basic oxygen furnace (BOF) slag and desulfurization slag (DS), which replaced 5-50% of natural river sand by weight in cement mixtures. The steel slag mortars were tested by high-temperature ($100^{\circ}C$) curing for 96 h and autoclave expansion. The results showed that the effects of the steel slag content varied based on the free lime (f-CaO) content. No more than 30% of the natural river sand should be replaced with steel slag to avoid fracture failure. The expansion fracture threshold value was 0.10%, above which there was a risk of potential failure. Based on the scanning electron microscopy (SEM) analysis, the high-temperature catalysis resulted in the immediate extrusion of peripheral hydration products from the calcium hydroxide crystals, leading to a local stress concentration and, eventually, deformation and cracking.

• Journal of the Korean Ceramic Society
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• v.49 no.6
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• pp.575-580
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• 2012

Geopolymers were synthesized using raw materials produced from two different areas: one was from Indonesia and the other was from Habcheon, Korea. The constituting phases of the Indonesian raw material were quartz and kaolinite, while those of the Habcheon sample were quartz, halloysite and albite. They were both calcined at $750^{\circ}C$ for 6 hours, and solution of NaOH and water glass was added to activate the geopolymeric reaction. The compressive strength of geopolymer synthesized from the Indonesian raw material showed a low value of $151\;kgf/cm^2$ after curing for 28 days. However, it could be greatly increased by adding blast furnace slag powders of $1188\;kgf/cm^2$ and $1969\;kgf/cm^2$ at 20 wt% and 40 wt% additions, respectively. The compressive strength of the geopolymer synthesized from the Habcheon raw material was high, at $557\;kgf/cm^2$, after 28 days, and the very high early-stage (3 days) strength of $556\;kgf/cm^2$ for this sample was remarkable. Commercially available Habcheon metastate raw material, of which composition showed low CaO and $Na_2O$ contents compared to the calcined Habcheon raw material, was also examined. It was found that the compressive strength of the commercial metastate type was nearly identical to that of the calcined Habcheon raw material except for the relatively low value at an early curing stage and at a high curing temperature of $60^{\circ}C$.

• Computers and Concrete
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• v.17 no.2
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• pp.271-280
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• 2016

This study examined the mechanical properties and adiabatic temperature rise of low-heat concrete developed based on ternary blended cement using ASTM type IV (LHC) cement, ground fly ash (GFA) and limestone powder (LSP). To enhance reactivity of fly ash, especially at an early age, the grassy membrane was scratched through the additional vibrator milling process. The targeted 28-day strength of concrete was selected to be 42 MPa for application to high-strength mass concrete including nuclear plant structures. The concrete mixes prepared were cured under the isothermal conditions of $5^{\circ}C$, $20^{\circ}C$, and $40^{\circ}C$. Most concrete specimens gained a relatively high strength exceeding 10 MPa at an early age, achieving the targeted 28-day strength. All concrete specimens had higher moduli of elasticity and rupture than the predictions using ACI 318-11 equations, regardless of the curing temperature. The peak temperature rise and the ascending rate of the adiabatic temperature curve measured from the prepared concrete mixes were lower by 12% and 32%, respectively, in average than those of the control specimen made using 80% ordinary Portland cement and 20% conventional fly ash.

• Journal of the Korea Institute of Building Construction
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• v.16 no.1
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• pp.67-76
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• 2016

Concrete exposed to severely low temperature below $-20^{\circ}C$ should be provided with proper heat supplying curing to protect the concrete from early frost damage at the time of pouring.meanwhile, so far, effective heat curingmethods of the concrete under severely low temperature are not well established in Korea. For this reason, the objective of this paper is to provide effective heat curingmethod of concrete exposed to severely low temperature to protect early frost damage by varying the combination of heat curingmaterial combinations. Temperature history,maturity development and core strength results are investigated. Fourmock-up specimens simulating slab, wall and column were prepared and heat insulation, heat supplying and both were applied. Test results indicate that the combination of quadruple layer bubble sheet(4BS) and embedding of heating cable has desirable performance for a slab, and heat supplying curing inside heat enclosure and heat generationmat also shows desirable performance for a wall, and for a column, use of EPS heat insulation has proper performance against early frost damage, which reaches $45^{\circ}D{\cdot}D$ and helps the concretemaintain above $0^{\circ}C$ within 3 days. Themethodsmentioned above are believed to be optimum protection from early frost damage of the concrete under $-20^{\circ}C$.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.04a
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• pp.53-58
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• 2000

During the curing process of thick glass/epoxy laminates, a substantial amount of temperature lag and overshoot at the center of the laminates is usually experienced due to the large thickness and low thermal conductivity of the glass/epoxy composites. Also, it requires a longer time for full and uniform consolidation. In this work, temperature, degree of cure and consolidation of a 20mm thick unidirectional glass/epoxy laminate were investigated using an experiment and a 3-dimentional numerical analysis considering the exothermic reaction. From the experimental and numerical results, it was found that the experimentally obtained temperature profile agreed well with the numerical one and the cure cycle recommended by the prepreg manufacturer should be modified to prevent a temperature overshoot and to obtain full consolidation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.11
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• pp.2853-2865
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• 2000

During the curing process of thick glass/epoxy laminates, a substantial amount of temperature lag and overshoot at the center of the laminates is usually experienced due to the large thickness and low thermal conductivity of the glass/epoxy composites. Also, it takes a longer time for full and uniform consolidation. In this work, temperature, degree of cure and consolidation of a 20 mm thick unidirectional glass/epoxy laminate were investigated using an experiment and a 3-dimentional numerical analysis. From the experimental and numerical results, it was found that the experimentally obtained temperature profile agreed well with the numerical one, and the cure cycle recommended by the prepreg manufacturer should be modified to prevent a temperature overshoot and to obtain full consolidation.

• Proceedings of the Korea Concrete Institute Conference
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• 2002.10a
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• pp.33-38
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• 2002

Concrete placed under cold weather has some defects such as the decrease of initial strength by hydration delay, strength unrecovery at unhardened concrete freezing, and structural failure and crack by expansion pressure. So, in this study, we tried to evaluate the JIS mortar which was made under cold weather using de-icing agency. In mortar test, the do-icing agency increased compressive strength under standard curing, and the de-icing agency made by NaNO$_2$ gave the highest strength. However, as pre-curing time under 21$^{\circ}C$ was short, the de-icing agency made by NaNO$_2$ and Ca[NO$_3$]$_2$ had the highest strength.

• Proceedings of the Korea Concrete Institute Conference
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• 1998.04b
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• pp.755-760
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• 1998

In the present, we have developed high strength concrete for the sleepers of high speed rail and verified its applicability by in-situ applications. Concrete for sleepers is manufactured by steam curing at low temperature(below 55$^{\circ}C$), and should be finished its manufacturing process such as placing, curing, demolding and prestressing in 24 hours. The sleepers need its compressive strength above 350kg/$\textrm{cm}^2$ in 15 hours, air-entrainment for durability and nominal design strength of 600kg/$\textrm{cm}^2$, considering its quality variation at factory. We performed the optimum mix design of concrete and verified the rightness of the use of TYPE III cement. Finally, we have confirmed the manufactured sleepers satisfy the required material properties through in-situ application.

• Fashion & Textile Research Journal
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• v.2 no.2
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• pp.123-131
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• 2000

Diphenyl-2-ethanolamidophosphate (DPEOAP) was synthesized to treat polyester fabrics in order to improve its flame retardancy. The flame retardancy and physical properties of DPEOAP-treated polyester fabrics were investigated. The results were as follows: 1) polyester fabrics can be treated with DPEOAP by means of Pad-Dry-Cure method, because DPEOAP was easily soluble in benzene. 2) The most economic conditions of treatment were determined as 10% of DPEOAP cocentration, $140^{\circ}C$ of curing temperature, and 2 minutes of curing time. 3) Though the washablity of DPEOAP is low in comparison with the other products which are purchasable in a market, it has an excellent flame retardment effect 3 times more than in number of flame contact just with 0.66% add-on. 4) The physical properties of DPEOAP treated polyester fabrics were little changed as compared with non-treated fabric.

• 한국신재생에너지학회:학술대회논문집
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• 2007.06a
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• pp.146-149
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• 2007

The 2-step manufacturing method consisting of preforming and stamping processes was developed to manufacture composite bipolar plates for PEMFCs. The preform was composed of expanded graphite, graphite flake and phenol resin. Precuring conditions were optimized by checking the electrical conductivity, flexural strength and microstructure. Precuring temperature ($100^{\circ}C$) slightly above the melting point of phenol powders ($90^{\circ}C$) induced moderate curing, but also prevented excessive curing. Preforms utilizing the tangled structure of expanded graphite were easily fabricated at low pressure of 0.07-0.28MPa. The proper precuring time, 5min, was determined to fabricate the preform stably because insufficient and excessive precuring deteriorated the flexural strength of composite bipolar plates.