• 제목/요약/키워드: Low Temperature Bonding

검색결과 303건 처리시간 0.028초

Sr-Ferrite를 이용한 자기 연마재에 관한 연구 (A Study on Magnetic Abrasive Using Sr-Ferrite)

  • 김희남;김동욱
    • 동굴
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    • 제79호
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    • pp.77-81
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    • 2007
  • In this paper deals with behavior of the magnetic abrasive using Sr-Ferrite on polishing charateristiccs in a internal finishing of staninless steel pipe a tying magnetic abrasive polishing. The magnetic polishing is the useful method to finish some machinery fabrications by using magnetic power. This method is one of the precision techniques and has in aim for clean technology in the transportation of the pure gas in the clean pipes. The magnetic abrasive polishing method is not so common in the field of machine that it is not known to widely. There are rarely researcher in this field because of non-effectiveness of magnetic abrasive. Therefore, in this paper we deals with the development of the magnetic abrasive with the use of Sr-Ferrite. In this development, abrasive grain SiC has been made by using the resin bond fabricated at low temperature. And magnetic abrasive powder was fabricated from the Sr-Ferrite which was crushed into 200 mesh. The XRD analysis result shows that only SiC abrasive and Sr-Ferrite crystal peaks were detected, explaining that resin bond was not any more to contribute chemical reaction. From MACRO analysis, we found that SiC abrasive and Sr-Ferrite were strongly bonding with each other.

고막 패각의 콘크리트 잔골재로 재활용 방안에 관한 연구 (A Study Properties of concrete Recycling Cockle Shells as Fine Aggregate)

  • 김정섭;김광섭;김판선
    • 한국건축시공학회지
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    • 제4권1호
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    • pp.141-146
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    • 2004
  • 1) As a result of compressive strength experiment, rupture compressive strength showed more increases in specimens of 15% and 20% of Cockle shells in those of non-mixture. Comparing compressive strength between no-mixed Specimens and Specimens of containing Cockle shells, Specimens containing Cockle shells showed higher strength in 60 days and 90 days of age, and as ark Cockle is contained and age is elapsed, compressive strength is also increased In addition, estimation of compressive strength by reactive hardness in concrete using Cockle shells as aggregate shows low reliability. 2) As a result of experimenting compressive strength after heating, Specimens containing Cockle shells and non-mixed Specimens showed similar strength at $200^{\circ}C$, but compressive strength was lowered as content of Cockle shells increased at over $400^{\circ}C$ and heating temperature was higher. It is because Cockle shells was fired by heat and then its adhesion and bonding capacity were lost. 3) To sum up the above experimental results, it is found that using splitted Cockle shells as aggregate for concrete by 10%~20% showed the same or higher compressive strength and shear strength as concretes using general aggregate and it can be used as substitute aggregate of concrete. It is considered that for future use of splitted Cockle shells as substitute concrete aggregate, continuous researches of its durability, applicability and economy are needed.

Ba-Ferrite와 GC, CBN을 이용한 자기 연마재 개발 (Development of The Magnetic Abrasive Using Ba-Ferrite and GC, CBN)

  • 김희남;윤여권
    • 한국안전학회지
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    • 제23권5호
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    • pp.43-48
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    • 2008
  • The magnetic polishing is the useful method to finish some machinery fabrications by using magnetic power. This method is one of the precision polishing techniques and has an aim for clean technology in the transportation of the pure gas in the clean pipes. The magnetic abrasive polishing method is not so common in the field of machine that it is not known to widely. There are only few researchers in this field because of non-effectiveness of magnetic abrasive. Therefore, in this paper deals with development of the magnetic abrasive using Ba-Ferrite. In this development, abrasive grain GC and CBN has been made by using the resin bond fabricated at low temperature. And magnetic abrasive powder was fabricated from the Ba-Ferrite which was crushed into 200 mesh. The XRD analysis result shows that only GC, CBN and Ba-Ferrite crystal peaks were detected, explaining that resin bond was not any more to contribute chemical reaction. From SEM analysis, we found that GC, CBN abrasive and Ba-Ferrite were strongly bonding with each other.

이온빔으로 질화처리된 사파이어기판위에 성장한 ZnO박막의 특성 (Properties of ZnO thin film grown on $Al_2O_3$ substrate pretremented by nitrogen ion beam)

  • 박병준;정연식;박종용;최두진;최원국;윤석진
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.1
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    • pp.413-416
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    • 2004
  • In this study, zinc oxide(ZnO) having large misfit(18.2%) with sapphire was tried to be grown on very thin nitride buffer layers. For the creation of various kinds of nitride buffer layer, sapphire surface was modified by an irradiation of nitrogen ion beam with low energy generated from stationary plasma thruster(SPT) at room temperature. After the irradiation of ion beam, Al-N and Al-O-N bonding was identified to be formed as nitride buffet layers. Surface morphology was measured by AFM and then ZnO growth was followed by pulsed laser deposition(PLD). Their properties are analyzed by XRD, AFM, TEM, and PL. We observed that surface morphology was improved and deep level emission related to defects was almost vanished in PL spectra from the ZnO grown on nitride buffer layer.

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4,4'-Diphenylmethane Diisocyanate (MDI)와 폴리에스테르 폴리올로부터 합성된 폴리우레탄의 모폴로지와 열적 성질에 관한 연구 (Studies on the Morphology and Thermal Properties of the Polyurethane Synthesized from 4,4'-Diphenylmethane Diisocyanate (MDI) and Polyester Polyol)

  • 정현철;강성중;김우년;김상범;이영범;홍성호
    • 한국가스학회지
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    • 제2권1호
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    • pp.59-65
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    • 1998
  • 4,4'-diphenylmethane diisocyanate (MDI)와 폴리에스테르 폴리올 그리고 1,4-butane diol로부터 폴리우레탄을 제조하고 모폴로지와 열적 특성에 대하여 연구하였다. Fourier transform infrared spectroscopy (FT-IR)를 이용한 폴리우레탄의 모폴로지 관찰에서 수소 결합된 N-H 피크와 C=O 피크는 폴리우레탄에서 하드 세그먼트(hard segment)의 함량이 증가할수록 낮은 주파수대로 전이되어 수소 결합이 증가함을 알 수 있었다. 시차 주사 열분석기(DSC)를 이용한 열적 특성에 대한 연구에서 폴리우레탄의 유리전이온도($T_g$)는 하드세그먼트의 함량이 증가함에 따라 증가하였다. 또한 소프트 세그먼트(soft segment)의 $T_g$는 관찰할 수 없었으며 이로부터 본 연구에서 제조된 폴리우레탄은 MDI의 높은 작용기로 인하여 화학 결합에 의한 경화 반응으로 균일한 망상구조를 가지고 있음을 알 수 있었다. 또한 DSC로부터 관측된 폴리우레탄의 $T_g$는 Fox 식으로부터 예측된 $T_g$와 큰 차이를 나타냈으며, 이는 경화 반응으로 인하여 폴리우레탄 사슬의 운동성이 제약되기 때문으로 생각된다. 동적 기계적 열분석(DMTA)에서도 소프트 세그먼트의 전이온도는 관찰되지 않았으며 이로부터 본 연구에서 제조된 폴리우레탄에서 하나의 상을 갖는 모폴로지를 확인할 수 있었다.

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목분-폴리프로필렌 복합체의 상분리 및 기계적 특성에 관한 연구 (A Study on the Phase Separation and Mechanical Properties of Wood Flour-Polypropylene Composites)

  • 이경희;변성광
    • Elastomers and Composites
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    • 제48권3호
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    • pp.216-220
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    • 2013
  • 본 연구에서는 목분-고분자 복합체(Wood Flour-Polymer Composite, WPC)의 상분리 특성을 조사하고 이를 토대로 목분함량에 따른 WPC의 기계적 물성 변화에 관한 원인을 규명하였다. 이를 위해 고분자 매트릭스로 폴리프로필렌을 사용하여 서로 다른 함량의 목분을 갖는 시편을 제조하였다. 서로 다른 목분 함량을 갖는 시편들의 DSC thermogram으로부터 목분 함량에 따른 고분자 PP의 결정화 경향과 $T_m$ 경향을 분석하였다. 목분 함량이 증가함에 따라 고분자 PP의 결정량 및 $T_m$값 모두 감소하다 다시 증가하는 결과를 나타내었다. 이로부터 낮은 목분 함량에서는 목분이 매트릭스인 고분자 내에 분산되어 있으나 일정 목분 함량이상에서는 WPC의 매트릭스인 PP와 목분사이에 상분리가 일어남을 확인할 수 있었다. 한편, WPC 시편의 인장강도는 목분 함량이 증가할수록 감소하는 결과를 나타내었다. 낮은 목분 함량에서는 고분자에 분산된 목분과 고분자 사이에서의 낮은 계면 결합력과 시편내에서 강도를 높이는 역할을 하는 결정량의 감소가, 높은 목분 함량에서는 PP와 목분사이에서의 상분리로 인한 계면 결함이 WPC 시편의 인장강도를 목분함량 증가에 따라 지속적으로 감소시키는 원인이 되는 것으로 파악되었다. WPC 시편의 충격강도는 목분 함량이 증가함에 따라 증가하다가 목분 함량이 20%인 경우 최고값을 나타내며, 그 이후 다시 감소하는 경향을 나타내었는데, 낮은 목분 함량에서는 목분 함량이 증가할수록 시편의 결정량이 감소하므로 시편의 취성 감소에 의해 충격강도가 향상되나, 높은 목분 함량에서는 고분자 매트릭스와 목분 사이의 상분리로 인해 다시 충격강도가 저하되기 때문인 것으로 판단된다.

The Effects of a Thermal Annealing Process in IGZO Thin Film Transistors

  • Kim, Hyeong-Jun;Park, Hyung-Youl;Park, Jin-Hong
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.289.2-289.2
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    • 2016
  • In-Ga-Zn-O(IGZO) receive great attention as a channel material for thin film transistors(TFTs) as next-generation display panel backplanes due to its superior electrical and physical properties such as a high mobility, low off-current, high sub-threshold slope, flexibility, and optical transparency. For the purpose of fabricating high performance IGZO TFTs, a thermal recovery process above a temperature of $300^{\circ}C$ is required for recovery or rearrangement of the ionic bonding structure. However diffused metal atoms from source/drain(S/D) electrodes increase the channel conductivity through the oxidation of diffused atoms and reduction of $In_2O_3$ during the thermal recovery process. Threshold voltage ($V_{TH}$) shift, one of the electrical instability, restricts actual applications of IGZO TFTs. Therefore, additional investigation of the electrical stability of IGZO TFTs is required. In this paper, we demonstrate the effect of Ti diffusion and modulation of interface traps by carrying out an annealing process on IGZO. In order to investigate the effect of diffused Ti atoms from the S/D electrode, we use secondary ion mass spectroscopy (SIMS), X-ray photoelectron spectroscopy, HSC chemistry simulation, and electrical measurements. By thermal annealing process, we demonstrate VTH shift as a function of the channel length and the gate stress. Furthermore, we enhance the electrical stability of the IGZO TFTs through a second thermal annealing process performed at temperature $50^{\circ}C$ lower than the first annealing step to diffuse Ti atoms in the lateral direction with minimal effects on the channel conductivity.

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방열 특성에 따른 집광형 태양전지의 광전변환효율 변화에 관한 실험적 연구 (An Experimental Study on the Heat Transfer Characteristics of the Conversion Efficiency in the Concentrated Photovoltaic Cells)

  • 김강호;정상현;김영조;김창주;전동환;신현범;이재진;강호관
    • Current Photovoltaic Research
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    • 제2권4호
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    • pp.168-172
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    • 2014
  • Under concentrated illuminations, the solar cells show higher efficiencies mainly due to an increase of the open circuit voltage. In this study, InGaP/InGaAs/Ge triple-junction solar cells have been grown by a low pressure metalorganic chemical vapor deposition. Photovoltaic characteristics of the fabricated solar cells are investigated with a class A solar simulator under concentrated illuminations from 1 to 100 suns. Ideally, the open circuit voltage should increase with the current level when maintained at the same temperature. However, the fabricated solar cells show degraded open circuit voltages under high concentrations around 100 suns. This means that the heat sink design is not optimized to keep the cell temperature at $25^{\circ}C$. To demonstrate the thermal degradation, changes of the device performance are investigated with different bonding conditions and heat sink materials.

셀룰로오스 기반 Electro-Active Paper 작동기: 재료 및 응용 (Cellulose based Electro-Active Paper Actuator: Materials and Applications)

  • 장상동;양상열;고현우;김동구;문성철;강진호;정혜전;김재환
    • 한국정밀공학회지
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    • 제28권11호
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    • pp.1227-1233
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    • 2011
  • Cellulose Electro-Active Paper (EAPap) has been known as a new smart material that is attractive for a bio-mimetic actuator due to its merits in terms of lightweight, dry condition, large displacement output, low actuation voltage and low power consumption. Cellulose EAPap is made by regenerating cellulose and aligning its micro-fibrils. This paper introduces several EAPap materials, which are based on natural cellulose and its hybrid nanocomposites mixed/blended with inorganic functional materials. By chemically bonding and mixing with carbon nanotubes and inorganic nanoparticles, the cellulose EAPap can be a hybrid nanocomposite that has versatile properties and can meet material requirements for many applications. Recent research trend of the cellulose EAPap is introduced in terms of material preparations as well as application devices including actuators, temperature and humidity sensors, biosensors, chemical sensors, and so on. This paper also explains wirelessly driving technology for the cellulose EAPap, which is attractive for bio-mimetic robotics, surveillance and micro-aerial vehicles.

고기능성 복합재료의 제조와 그 특성평가에 관한 연구 (A Study on the Preocessing of high Runctional Composites and the Evaluation of Its Characteristics)

  • 김윤해
    • Journal of Advanced Marine Engineering and Technology
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    • 제22권2호
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    • pp.139-145
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    • 1998
  • Filament winding method is widely used for composite fabrications using low viscosity liquid for-mation and processing asymmetrical structures of pressure vessel pipe rocket motor case etc. The filament winding method is affected by several parameters such as pot life of process time viscosi-ty of resin filament winding temperature and schedules curing condition and post curing condi-tion of resin. To develope high functional composite materials the rotation(5, 15, 20, 30rpm) of the winding machine was controlled by D.C motor. And the wiper to give proper tension was equipped between strand and resin bath. The resin is hooked by the design wiper. The adequate cure schedule was found by DSC. NOL ring test is carried out to investigate the basic physical properties such as design technology. The void contents in filament winding is generally higher than that of the prepreg laminated plate. These high contents of void can make a crack in resin in spite of low deformation. These problem was solved by giving tension in processing. To improve the characteristics of fiber volume fraction void contents resin/fiber bonding the winding speedc is changed under constant tension. It was found that resin impregnation was not different from in fiber contents void contents at the range of 0.5~1kg tension but it was found that resin was not impregnated at the above of 1.5kg tension. In burst test a pure PE liner was failed at a nozzle part under the $14kg/\textrm{cm}^2$ pressure but a pressure vessel of CNG was failed at a cylinder part under the $200kg/\textrm{cm}^2$ pressure.

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