• Title/Summary/Keyword: Long-term characterization

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Fabrication and Characterization of Alumina Sol for Coating by a Method of the Mechanical Milling (기계적 분쇄방법을 통한 코팅용 알루미나 졸의 제조 및 평가)

  • Yu, Jeong-Hwan;Jung, Seung-Hwa;Jo, Bum-Rae;Hong, Gyung-Pyo;Mun, Jong-Soo;Kang, Jong-Bong
    • Korean Journal of Materials Research
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    • v.18 no.8
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    • pp.417-421
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    • 2008
  • $Al_2O_3$ sol with long-term stability was prepared by mechanical milling. Thin films were evaluated and created for use as coating materials. The particle size of the manufactured sol was 98 nm when 2 wt% of nitric acid was added. This indicates that the viscosity of the sol is 12 cps and that it has long-term stability. The thickness of the thin films, which varied from 100 nm to 500 nm, could be managed by adjusting the draw rate and the amount of an organic additive. A thin film heated to $500^{\circ}C$ indicated a hydrophilic property against water and excellent permeability against a visible ray.

Development of Portable Measurement Unit with Wireless Transmission by Wireless LAN for Long-term Monitoring (장기간 소자 모니터링이 용이한 소형 무선랜 무선송신 계측장치 개발)

  • Park, So Jeong;Park, Il-Hoo;Moon, Young-Sun;Lee, Kook Jin;Kim, Gyu-Tae
    • Journal of the Semiconductor & Display Technology
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    • v.17 no.1
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    • pp.45-49
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    • 2018
  • Portable microcontroller based measurement unit is demonstrated using digital-to-analog convertor module, analog-to-digital convertor module and additional preamplifier circuit with low-budget but excellent performances. Using the designed measurement unit, the measurement of current below 1 nA with applying voltage up to 5 V is successfully carried out. With the WiFi module in microcontroller, measured data is transferred to the user's computer. To evaluate the performance of the measurement unit, the transfer curve of a commercial N-type field effect transistor was measured with the measurement unit and the results is well consistent with that measured using commercial characterization system.

A comprehensive study of the effects of long-term thermal aging on the fracture resistance of cast austenitic stainless steels

  • Collins, David A.;Carter, Emily L.;Lach, Timothy G.;Byun, Thak Sang
    • Nuclear Engineering and Technology
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    • v.54 no.2
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    • pp.709-731
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    • 2022
  • Loss of fracture resistance due to thermal aging degradation is a potential limiting factor affecting the long-term (80+ year) viability of nuclear reactors. To evaluate the effects of decades of aging in a practical time frame, accelerated aging must be employed prior to mechanical characterization. In this study, a variety of chemically and microstructurally diverse austenitic stainless steels were aged between 0 and 30,000 h at 290-400 ℃ to simulate 0-80+ years of operation. Over 600 static fracture tests were carried out between room temperature and 400 ℃. The results presented include selected J-R curves of each material as well as K0.2mm fracture toughness values mapped against aging condition and ferrite content in order to display any trends related to those variables. Results regarding differences in processing, optimal ferrite content under light aging, and the relationship between test temperature and Mo content were observed. Overall, it was found that both the ferrite volume fraction and molybdenum content had significant effects on thermal degradation susceptibility. It was determined that materials with >25 vol% ferrite are unlikely to be viable for 80 years, particularly if they have high Mo contents (>2 wt%), while materials less than 15 vol% ferrite are viable regardless of Mo content.

Synthesis, Characterization and Identification of In Vitro and In Vivo DNA adducts of 1- and 2-Bromopropane

  • Moon, Yoon-Soo;Basnet, Arjun;Zhao, Long-Xuan;Kim, Eun-Kyung;Lim, Hyun-Tae;Chae, Whi-Gun;Jeong, Tae-Cheon;Lee, Eung-Seok
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.246.2-247
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    • 2003
  • It has been reported that 2-bromopropane might be a causative agent for reproductive toxicity and have immunotoxic effects. 1-Bromopropane known as an alternative to ozone depleting solvents, which has structural similarity to 2-bromopropane, has been reported to be neurotoxic to rats in long-term inhalation exposure. (omitted)

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Synthesis and Characterization of Degradable Polycationic Polymers as Gene Delivery Carriers

  • Kim, Hyun-Jin;Kwon, Min-Sung;Choi, Joon-Sig;Kim, Bo-Hye;Yoon, Jae-Keun;Kim, Kwan;Park, Jong-Sang
    • Bulletin of the Korean Chemical Society
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    • v.28 no.1
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    • pp.63-67
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    • 2007
  • Biodegradable cationic poly(ester-amide) polymers were synthesized by double-monomer method, that showed excellent solubility in many organic solvents and water. Different degradation patterns were obtained by the regulation of monomer ratios and overall long period of time of DNA protection up to 12 days was shown by PicoGreen reagent assay. Good transfection profiles in the presence of serum and very low toxicity on mammalian cells may allow these polymers to become suitable for long-term gene delivery systems and therapeutic applications.

Preparation and characterization of the primary gas standards for isoprene (아이소프렌 일차표준가스의 제조 및 특성 평가)

  • Kim, Taesu;Kang, Chul-Ho;Kim, Yong Doo;Lee, Seungho;Kim, Dalho
    • Analytical Science and Technology
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    • v.27 no.6
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    • pp.357-363
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    • 2014
  • Isoprene is a one of the biogenic volatile organic compounds (BVOCs) and it is known as a source of the tropospheric ozone and formaldehyde. In addition, isoprene is a trace component of the exhaled breath and it is a potential biomarker for the diagnosis of diseases such as lung cancer. In these regards, isoprene gas standards are required for the accurate measurement of isoprene in air samples. To establish a standard for isoprene gas, gravimetric preparation and characterization of primary gas standards were studied. The primary gas standards were produced independently in 4 aluminum cylinders and concentrations were examined by GC-FID. As a result, the uncertainty of the gravimetric preparations including purity of the raw material was 0.01% and reproducibility of the preparation of independent 4 cylinders was 0.08%. The primary gas standards for isoprene showed 14 months of long-term stability. The relative expended uncertainty of 2.8% (95% of confidence level, k=1.96) was assigned to the certified value of 10 ${\mu}mol$/mol level of isoprene based on the quantitative evaluation of the purity, weighing, reproducibility, adsorption and long-term stability.

Research on Approaches to revitalize KKU Design Venture (건국 디자인 벤처(KKU)의 활성화에 관한 연구)

  • 김인경
    • Journal of the Korea Fashion and Costume Design Association
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    • v.5 no.2
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    • pp.93-102
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    • 2003
  • With respect to this research, the College of Arts and Design, Kon Kuk University founded Design Venture of KKU(Kon Kuk University) in July 2001 as an approach to tackle the issue on how to accept and respond to the waves of changes in paradigms of the 21st century represented by information revolution. Such move is to cope more effectively with the changes in the current educational environment with an aim to secure the competitive edges compatible with the conditions of each college under the uniform and standardized educational systems. Even the professionals in the design fields of this country try to find the significance in bringing out in the open the latent creative talents of the students by improving the quality of our daily necessities and putting the students through more practical training, and in creating international competitiveness of our design field by encouraging the students to gain more diverse experiences. Therefore, the purpose of this research is to present the approaches to revitalize Design Venture of Kon Kuk University which has been managed as part of the efforts to establish the new identity for the design of this country in the 21st century, and to present the new model for an enterprise which, rooted in the College, can grow into a high value-added business. The methodology for this research is based on the case study of Design Venture of Kon Kuk University and investigation into the literature. The contents of this research include the following three steps. Firstly, initial research is made into the background for founding the College of Arts and Design which had been promoted as a differentiated strategy for the long-term and short-term development plan of the College of Arts and Design, in Chungju Campus of Kon Kuk University. Secondly, the basic strategy for Vonchi, brand of Design Venture of KKU and the brand launching process are examined. Thirdly, Various approaches to revitalize the Vonchi brand recognition are collected and analyzed to present the conclusion and the alternative. Such research findings as given above on Design Venture of KKU may satisfy diverse consumer-oriented requirements on the strength of the characterization and differentiation of the college and may enhance the competitive edge of the college.

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Preparation and Characterization of Polymer Lubricating Bearings (고온용 폴리머 윤활 베어링의 특성 연구)

  • Han, Jong-Dae;Kim, Sang-Keun;Kim, Byung-Kwan
    • Tribology and Lubricants
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    • v.24 no.4
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    • pp.179-185
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    • 2008
  • Microporous polymer lubricants(MPLs) are solid polymer materials containing micropores which are filled with liquid lubricants, and which are molded or formed to suit rolling bearings or other machine parts requiring lubrication. MPLs can be effectively applied to provide long-term, maintenance-free lubrication of a variety of machine elements without fully replacing of oils and greases. The application of rolling bearings packed fully with an MPL could reduce or eliminate the problems such as grease deterioration, leakage, under-lubrication caused by insertion of water or foreign matters under severe operation conditions. This paper discuss the application of MPLs for lubrication of rolling ball bearings. Two different MPLs were synthesized and the features of MPLs were tested. Characteristics of the bearings which are packed fully with synthesized MPLs were investigated using SEM, TG/DSC, extents of oil leakage, OIT, and life time test. After these preliminary tests twelve MPLs were synthesized and evaluated by measuring extents of oil leakage and OIT values. Then synthesis conditions for the optimum MPL were selected by SSRED(Six Sigma Robust Engineering Design) pro gram using extents of oil leakage and OIT values respectively. The optimum MPL by means of OIT value showed higher performance such as long life time and application at higher temperature of $140^{\circ}C$ than previous temperature of $100^{\circ}C$.

Structural health monitoring of the Jiangyin Bridge: system upgrade and data analysis

  • Zhou, H.F.;Ni, Y.Q.;Ko, J.M.
    • Smart Structures and Systems
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    • v.11 no.6
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    • pp.637-662
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    • 2013
  • The Jiangyin Bridge is a suspension bridge with a main span of 1385 m over the Yangtze River in Jiangsu Province, China. Being the first bridge with a main span exceeding 1 km in Chinese mainland, it had been instrumented with a structural health monitoring (SHM) system when completed in 1999. After operation for several years, it was found with malfunction in sensors and data acquisition units, and insufficient sensors to provide necessary information for structural health evaluation. This study reports the SHM system upgrade project on the Jiangyin Bridge. Although implementations of SHM system have been reported worldwide, few studies are available on the upgrade of SHM system so far. Recognizing this, the upgrade of original SHM system for the bridge is first discussed in detail. Especially, lessons learned from the original SHM system are applied to the design of upgraded SHM system right away. Then, performance assessment of the bridge, including: (i) characterization of temperature profiles and effects; (ii) recognition of wind characteristics and effects; and (iii) identification of modal properties, is carried out by making use of the long-term monitoring data obtained from the upgraded SHM system. Emphasis is placed on the verification of design assumptions and prediction of bridge behavior or extreme responses. The results may provide the baseline for structural health evaluation.

A Study on the Soluble Salt and Deterioration of Ceramics from Taean Shipwreck (태안 마도 출토 도자기의 염에 의한 손상상태 연구)

  • Jang, Sung-Yoon;Nam, Byeong-Jik;Park, Dae-Woo;Kang, Hyun-Mi;Jung, Yong-Hwa
    • 보존과학연구
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    • s.30
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    • pp.189-202
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    • 2009
  • Ceramics from Taean shipwreck were studied to investigate the deterioration by soluble salts and desalination pattern according to each ceramic characterization. NaCl crystals were found as a crystal growth on the ceramic microstructure and deteriorated to push off the glaze layer of some Puncheong ware sample. As a result of monitoring the desalination pattern of ceramics for 74days, the earthenware sample with big pores and no glaze removed soluble salts so fast, but Puncheong ware and Whiteware samples removed lots of soluble salts slowly and continuously. Generally, it takes long time to remove soluble salts from porcelains, due to small pores and glaze, but the long-term desalination probably can cause the damage on the surface layer such like glaze. As some soluble salts still remains in the ceramic microstructures after desalination, it is very important to control and keep the relative humidity stable through the proper storage. There are various ceramic deterioration patterns by soluble salts. Therefore, it needs to select the desalination method of ceramics from shipwreck, considering the material characteristics and the production techniques.

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