• Title/Summary/Keyword: Liquid-solid

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The High-throughput Solid-Phase Extraction in the Field of Synthetic Biology: Applications for the Food Industry and Food Managements

  • Hyeri SEONG;Min-Kyu KWAK
    • The Korean Journal of Food & Health Convergence
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    • v.10 no.3
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    • pp.19-22
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    • 2024
  • The field of synthetic biology has emerged in response to the ongoing progress in the life sciences. Advances have been made in medicine, farming, eating, making materials, and more. Synthetic biology is the exploration of using living organisms to create new organisms. By manipulating specific genes to express targeted proteins, proteins can be created that are both productive and cost-effective. Solid-phase extraction (SPE) and liquid-liquid extraction (LLE) are employed for protein separation during the production process involving microorganisms. This study centers on Scanning Probe Microscopy (SPM) to showcase its utility in the food industry and food management. SPE is predominantly utilized as a pretreatment method to eliminate impurities from samples. In comparison to LLE, this method presents benefits such as decreased time and labor requirements, streamlined solvent extraction, automation capabilities, and compatibility with various other analytical instruments. Anion exchange chromatography (AEC) utilizes a similar methodology. Pharmaceutical companies utilize these technologies to improve the purity of biopharmaceuticals, thereby guaranteeing their quality. Used in the food and beverage industry to test chemical properties of raw materials and finished products. This exemplifies the potential of these technologies to enhance industrial development and broaden the scope of applications in synthetic biology.

Review of Combustion Instability in Liquid Propellant Rocket Engines (액체로켓엔진의 연소불안정 현상)

  • Khil, Tae-Ock;Im, Ji-Hyuk;Yoon, Young-Bin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.11 no.1
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    • pp.71-84
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    • 2007
  • The review of the liquid propellant rocket engine is presented. The combustion instabilities which were discovered on solid and liquid propellant rocket engines in 1930, have occurred on propulsion devices, such as gas turbine, ramjet, scramjet and rocket, and thus a study on the combustion instability became necessary. However, this problem has not been solved yet. Therefore, we investigated causes and mechanisms of the combustion instability and surveyed the efforts of solving combustion instability in various countries for developing stable liquid propellant rocket engines.

Recent Progress in Nanoparticle Synthesis via Liquid Medium Sputtering and its Applications

  • Cha, In Young;Yoo, Sung Jong;Jang, Jong Hyun
    • Journal of Electrochemical Science and Technology
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    • v.7 no.1
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    • pp.13-26
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    • 2016
  • Nanoparticles (NPs), which have been investigated intensively as electrocatalysts, are usually synthesized by chemical methods that allow precise size and shape control. However, it is difficult to control the components and compositions of alloy NPs. On the other hand, the conventional physical method, sputtering with solid substrates, allows for facile composition control but size control is difficult. Recently, “liquid medium sputtering” has been suggested as an alternative method that is capable of combining the advantages of the chemical and conventional physical methods. In this review, we will discuss NP synthesis via the liquid medium sputtering technique using ionic liquid and low-volatile polymer media. In addition, potential applications of the technique, including the generation of oxygen reduction reaction electrocatalysts, will be discussed.

Ultrasonic Extraction of Phenolic Compounds from Laminaria japonica Aresch Using Ionic Liquid as Extraction Solvent

  • Han, Dandan;Zhu, Tao;Row, Kyung-Ho
    • Bulletin of the Korean Chemical Society
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    • v.32 no.7
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    • pp.2212-2216
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    • 2011
  • An ionic liquid-based ultrasonic-assisted extraction method has been successfully applied to the effective extraction of phenolic compounds from Laminaria japonica Aresch. Three kinds of 1-alkyl-3-methyl-imidazolium with different cations and anions were evaluated for extraction efficiency. The results showed that both the characteristics of anions and cations have remarkable effects on the extraction efficiency. In addition, the ionic liquid-based ultrasonic-assisted extraction procedure was also optimized on some extraction parameters, such as ultrasonic power, extraction time and solid-liquid ratio. Compared with the conventional solvent, the optimum approach gained the highest extraction efficiency within the shortest extraction time. Average recoveries of phenolic compounds were from 75.5% to 88.3% at three concentration levels.

A Study of Heat Storage System with Phase Change Material - Inward Melting and Solidification in a Horizontal Cylinder - (상변화물질을 이용한 잠열축열조에 관한 기초 연구 - 수평원관내에서의 내향용융 및 응고열전달 실험 -)

  • Kim, I.G.;Cho, N.C.;Kim, J.G.;Lee, C.M.;Yim, C.S.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.1 no.4
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    • pp.319-329
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    • 1989
  • Heat transfer phenomena during inward melting and solidification process of the phase change material were studied expertimentally. The phase change medium was 99% pure n-docosane paraffin ($C_{22}H_{46}$). The solid-liquid interface motion during phase change was recorded photographically. Measurements were made on the temperature, the solid-liquid interface, the melted or frozen mass and the various energy components stored or extracted from the cylinder wall. For melting, the experimental results reaffirmed the dominant role played by the conduction at an early stage, by the natural convection at longer time. For solidification, natural convection effects in the superheated liquid were modest and were confined to short freezing time. Although the latent energy is the largest contributor to the total stored or extracted energy, the aggregate sensible energies can make a significant contribution, especially at large cylinder wall superheating or subcooling, large initial phase change material subcooling or superheating.

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Development of Analytical Method and Monitoring of Organophosphorus Pesticides in the Raw Water and Clean Water by Liquid Chromatography-Tandem Mass Spectrometry (LC/MS/MS를 이용한 유기인계 농약류의 최적 분석법 정립과 원·정수에서의 모니터링)

  • Kim, Gyung-A;Song, Mi-Jeong;Yeom, Hoon-Sik;Son, Hee-Jong;Lee, Sang-Won;Choi, Jin-Tack
    • Journal of Environmental Science International
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    • v.24 no.12
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    • pp.1569-1582
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    • 2015
  • The analytical method for 16 organophosphorus pesticides was developed in this study. The 16 organophosphorus pesticides were analyzed by liquid chromatography-tandem mass spectrometry (LC/MS/MS) using on-line solid phase extraction (on-line SPE) with PLRP- S cartridge. Analysis of all analytes in the MS/MS was processed in the electrospray ioni-zation (ESI) positive mode. They are Azinphos ethyl, Chlorfenvinphos, Ethion, Famphur, Phosmet, Phosphamidon, Terbufos, Aspon, Chlorpyrifos-methyl, Crotoxyphos, Dichlofenthi-on, Dicrotophos, Fonofos, Thionazin, Dimethoate and Iprobenfos. Limits of detection (LODs) and Limits of quantification(LOQs) were obtained as 0.8~2.0 ng/L and 2.6~6.4 ng/L, respectively. All compounds were not detected at the 8 sampling points of the raw water and clean water.

The Study on the Two-Phase Flow in the Microchannel Using DSMC(Direct Simulation Monte Carlo) Method (DSMC(Direct Simulation Monte Carlo)방법을 이용한 마이크로관 내에서의 2 상유동에 관한 연구)

  • Lee, Jin-Ho;Ryu, Dong-Hun;Lee, Tae-Hong
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.27 no.12
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    • pp.1667-1672
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    • 2003
  • In contrast to the high demand for MEMS devices, microflow analysis is not feasible even for single-phase flow with conventional Navier-Stokes equation because of non-continuum effect when characteristic dimension is comparable with local mean free path. DSMC is one of particle based DNS(Direct Numerical Simulation) methods that uses no continuum assumption. In this paper, gas flow in microchannel is studied using DSMC. Interfacial shear and flow characteristics are observed and compared with the results of gas flow that is in contact with liquid case and solid wall case. The simulation is limited to the case of equilibrium steady state and evaporation/condensation coefficient is assumed to be the same and unity. System temperature remains constant and the interfacial shear appears to be small compared to the result with solid wall. This is because particles evaporated and reflected from the liquid surface form high density layer near the interface with liquid flow.

Predicting Micro-Thickness of Phase Fronts in Propellants (추진제의 마이크로 스케일 상면 두께 예측)

  • Yoh Jai-Ick
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2005.11a
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    • pp.13-21
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    • 2005
  • I consider the structure of steady wave system which is admitted by the continuum equations for materials that undergo phase transformations with exothermic chemical reaction. In particular, the dynamic phase front structures between liquid and gas phases, and solid and liquid phases are computationally investigated. Based on the one-dimensional continuum shock structure analysis, the present approach can estimate the nano-width of waves that are present in combustion. For illustration purpose, n-heptane is used in the evaporation and condensation analysis and HMX is used in the melting and freezing analysis of energetic materials of interest. On-going effort includes extension of this idea to include broad range of liquid and solid fuels, such as rocket propellants.

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A Study on the Hot Cracking Phenomena of Cu-Ni Bearing Hot Rolled Steels (Cu-Ni 첨가형 열연강판의 열간균열현상에 관한 연구)

  • Yun, In-Taek;Jo, Yeol-Rae;Kim, Sun-Ho;Kim, In-Bae
    • Korean Journal of Materials Research
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    • v.9 no.4
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    • pp.335-340
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    • 1999
  • The hot cracking phenomena and phase behaviors during hot working process of Cu-Ni bearing hot rolled steels were investigated by a $90^{\circ}$bending tests, BSE image analysis and EDS analysis. For aNi-free 1.2% Cu bearing steel, the surface hot cracking occurred about $1100^{\circ}C$ due to a liquid state Cu-enriched phase formed continuously at the interface between oxide scale and matrix. The liquid Cu-enriched phase penetrated into austenite grain boundaries and caused surface cracking during the hot working. In case of 0.6% Ni containing 1.2% Cu-Ni bearing steel, solid state Cu-Ni-riched phase existed at the scale/matrix interface as a discontinuous type. But the higher addition of 1.2% Ni, solid state Ni-Cu-riched phase was formed dominantly in the oxide scale. It was found that the addition of Ni suppressed the surface cracking of 1.2% Cu bearing steel by eliminating the liquid state Cu-enriched phase.

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Development of Treatment Process for Residual Coal from Biosolubilization

  • Rifella, Archi;Shaur, Ahmad;Chun, Dong Hyuk;Kim, Sangdo;Rhim, Young Joon;Yoo, Jiho;Choi, Hokyung;Lim, Jeonghwan;Lee, Sihyun;Rhee, Youngwoo
    • Clean Technology
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    • v.24 no.2
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    • pp.119-126
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    • 2018
  • This study introduced a treatment process that was developed to treat Indonesian low-rank coal with high-ash content, which has the same characteristics as residual coal from the biosolubilization process. The treatment process includes separation of ash, solid-liquid separation, pelletizing, and drying. To reduce the ash content, flotation was performed using 4-methyl-2-pentanol (MIBC) as frother, and kerosene, waste oil, and cashew nut shell liquid (CNSL) as collectors. The increasing amount of collector had an effect on combustible coal recovery and ash reduction. After flotation, a filter press, extruder, and an oven drier were used to make a dried coal pellet. Then another coal pellet was made using asphalt as a binder. The compressive strength and friability of the coal pellets were tested and compared.