• Fashion & Textile Research Journal
• /
• v.1 no.4
• /
• pp.363-369
• /
• 1999

Artemisia princeps was used for the natural dye stuff extraction and concentration to produce the condensed dye liquid. Using this liquid, the silk and the cotton fabrics were dyed. And then the K/S value, color difference were measured in order to determine the dyeability and the antimicrobial activity. The K/S value of silk were much higher than those of cotton. In terms of the silk fabric, the premordanting method was most efficient of the mordanting method. The various surface colors on the dyed fabric were resulted according to used mordants and mordanting methods. The dye fastness was significantly improved when mordants were added. Among them, Cr-mordant improved more than 1 level. The Cu-mordant showed the greatest antimicrobial activity on both of mordant treated silk and cotton.

• Journal of radiological science and technology
• /
• v.13 no.2
• /
• pp.43-49
• /
• 1990

[ $^{111}$ ]In has wide applications in nuclear medicine for labelling and in-vivo distribution studies. A method is developed for the production of carrier free $^{111}$In using the reaction $^{nat.}Cd(p,\;xn)$ $^{111}$In with MC-50 cyclotron. Carrier free $^{111}$In was separated from the irradiated metallic cadmium by liquid-liquid extraction and cation exchange chromatography. The yield of $^{111}$In at EOB is $0.8mCi/{mu}\;Ahr$ and the nuclidic purity is over 99%. $^{111}In-DTPA\;and\;^{111}In-bleomycin$ were prepared for medical study.

• Bulletin of the Korean Chemical Society
• /
• v.23 no.3
• /
• pp.432-436
• /
• 2002

Benomyl, one of the known endocrine disrupting chemicals, was analyzed to understand the fate in the nature. Water, sediment and biota samples are acidified to hydrolyze benomyl into carbendazim then followed by extraction and concentration. The concentrations of carbendazim in the samples were determined by liquid chromatography/time-of-flight mass spectrometer. Analysis data showed that certain amount of carbendazim was accumulated in sediment. On the contrary, no sign of accumulation in biota was observed probably due to the increased degradation rate in vivo. It is, however, that no one can claim carbendazim is not harmful to biota, since carbendazim may give a negative effect against organisms at the point of intaking.

• Proceedings of the Membrane Society of Korea Conference
• /
• 1995.10a
• /
• pp.43-44
• /
• 1995

The diffusion behavior of liquid into polymer has been described by Fick's law, but the departure from Fickian diffusion is frequently found. In this study, 'noble' expressions for the rates of relaxation and sorption are introduced to eliminate these limitations. The ralaxation-sorption coupled mechanism model are based on the possibility of contacting liquid molecule and the active site which has the numerical concept of free volume. The concept has an analogy of reaction rate expressed by the possibility of collision with molecules and used in adsorption and reactive extraction etc. The new model simulated by Rungc-Kutta method for initial-value problem and Fickian diffusion is caompared with experimental data. The results show that the ralaxation-sorption coupled mechanism is able to account well for Fickian and non-Fickian sorption behavior including sigmoid and two-stage. In addition, this model has a chance of expansion to multi-component sorption with ease.

• Journal of Energy Engineering
• /
• v.10 no.2
• /
• pp.83-89
• /
• 2001

This paper studies the possibility of applying the EIT(Electrical Impedance Tomography) technique for investigating the formation and movement of dispersed phase droplets as they stream through a Direct Contact Heat Exchanger(DCHX). In most direct contact liquid-liquid heat exchangers, oil or hydro-carbon with a density different (lighter or heavier) from water is normally used as dispersed working fluid. The main difficulty that arises with arrangement lies in the extraction of performance parameters and visualization of dispersed phase fluids if required. In order to delve into these problems, this paper introduces a number of cases regarding the operation and principle of DCHXs and investigates the possibility of applying the EIT technique whose results are given for several examples.

• Mass Spectrometry Letters
• /
• v.5 no.1
• /
• pp.1-11
• /
• 2014

Lipids play important roles in biological systems; they store energy, play a structural role in the cell membrane, and are involved in cell growth, signal transduction, and apoptosis. Phospholipids (PLs) in particular have received attention in the medical and lipidomics research fields because of their involvement in human diseases such as diabetes, obesity, atherosclerosis, and many cancers associated with lipid metabolic disorders. Here I review experimental strategies for PL analysis based on nanoflow liquid chromatography-electrospray ionization-tandem mass spectrometry (nLC-ESI-MSn). In particular, discussed are lipid extraction methods, nanoflow LC separation of PLs, effect of ionization modifiers on the ESI of PLs, influence of chain lengths and unsaturation degree of acyl chains of PLs on MS intensity, structural determination of the molecular structure of PLs and their oxidized products, and quantitative profiling of PLs from biological samples such as tissue, urine, and plasma in relation to cancer and coronary artery disease.

• Journal of the Korean Home Economics Association
• /
• v.38 no.3
• /
• pp.1-9
• /
• 2000

Saururus-chinensis was used for the natural due stuff extraction and concentration to produce the condensed dye liquid. Using this liquid, the silk and the cotton fabrics were dyed. And then the K/S value, color difference were measured in order to determine the dye ability and the antimicrobial activity. The K/S values of silk were much higher than those of cotton. In terms of the silk fabric, the Al, Cr-premordanting and Fe, Cu-simmordanting method was most efficient of the mordanting method. The various suface colors on the dyed fabric were resulted according to used mordants and mordanting methods. The dye fastness was significantly improved when mordants were added. Among them, Al-mordant improved more than 1 level. The Cu, Fe-mordants showed the greatest antimicrobial activity on both of mordant treat silk and cotton.

• Macromolecular Research
• /
• v.12 no.4
• /
• pp.427-430
• /
• 2004

Calix[4]crown-6-2,4-bis(2-hydroxyethyl ether) (2), which has crown-6 moieties at the 1- and 3-positions and hydroxyethyl functions at the 2- and 4-positions, was prepared for the syntheses of polyester 3 and polyurethane 4 by reactions with adipoyl chloride and hexamethylene diisocyanate, respectively. The ion binding characteristics of monomer 2 and polymers 3 and 4 toward alkali and alkali earth metal ions were measured by liquid-liquid extraction from the aqueous phase into the organic phase. We observed that the polyurethane 4 has a higher binding affinity toward various metal cations when compared to polyester 3, which exhibits cesium ion selectivity.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
• /
• v.11 no.3
• /
• pp.384-390
• /
• 1999

A vibrating U-Tube decimeter has been evaluated as a sensor for measuring the concentration of oil in the liquid line of a refrigeration system. Calibration and performance tests were conducted under simulated liquid-line conditions for R-407C/POE oil and R-410A/POE oil mixtures in oil concentration from 0 to 15 weight percent. Test temperatures ranged from 20 to 5$0^{\circ}C$. As a result of test, oil concentration correlations are presented in terms of specific gravity at each constant temperature. These equations enable to predict the oil concentration without any extraction of the mixture, and can be applied for R-407C/POE oil and R-410A/POE oil mixtures.

• Archives of Pharmacal Research
• /
• v.29 no.1
• /
• pp.108-111
• /
• 2006

The economic and effective method for preparation of R-(-)-ibuprofen by diastereomer crystallization was developed. R-(-)-ibuprofen was resolved from racemic ibuprofen by forming R-(-)ibuprofen-R-(+)-$\alpha$-methylbenzylamine diastereomeric salt with R-(+)-$\alpha$-methylbenzylamine and crystallization. The purity of R-(-)-ibuprofen-R-(+)-$\alpha$-methylbenzylamine diastereomeric salt was tested and confirmed using HPLC and $^1H-NMR$ method. The pure diastereomeric salt collected from repeated recrystallization was further fractionated by liquid-liquid extraction to the pure enantiomer without racemization. R-(-)-ibuprofen was recovered producing overall yield of 2.4% with the purity more than 99.97%.