• Korean Journal of Materials Research
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• v.27 no.11
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• pp.609-616
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• 2017

We investigated a Leidenfrost effect in the growth of ZnO nanostructures on silicon substrates by ultrasonic-assisted spray pyrolysis deposition(SPD). Structural and optical properties of the ZnO nanostructures grown by varying the growth parameters, such as substrate temperature, source concentration, and suction rate of the mist in the chambers, were investigated using field-emission scanning electron microscopy, X-ray diffraction, and photoluminescence spectrum analysis. Structural investigations of the ZnO nanostructures showed abnormal evolution of the morphologies with variation of the substrate temperatures. The shape of the ZnO nanostructures transformed from nanoplate, nanorod, nanopencil, and nanoprism shapes with increasing of the substrate temperature from 250 to $450^{\circ}C$; these shapes were significantly different from those seen for the conventional growth mechanisms in SPD. The observed growth behavior showed that a Leidenfrost effect dominantly affected the growth mechanism of the ZnO nanostructures.

• Proceedings of the Korean Vacuum Society Conference
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• 2015.08a
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• pp.126.1-126.1
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• 2015

A quantitative relationship between Leidenfrost point and surface characteristics such as surface material and roughness is investigated. Based on the relationship, we have fabricated the surfaces with their Leidenfrost points (LFP) tuned by controlling surface coating and structures. As discovered by Leidenfrost, liquids placed on a hot plate levitate on the gas phase-air gap formed by the vaporization of liquids. This phenomenon is called 'Leidenfrost effect'. A change of LFP has attracted many researchers for several years but the ability to tune LFP is still a remaining issue. Many of previous work has progressed for various conditions so the systematic approach and analysis are needed to clearly correlate the LFP and the surface conditions. In this report, we investigate a relation of surface energy and LFP using various coating materials such as Octadecyltrichlorosilane (OTS) and 1H, 1H, 2H, 2H-Perfluorooctyltrichlorosilane (FOTS). Also, we analyze how surface roughness affects LFP via surface micro structuring with ICP-RIE fabrication process. The improved understanding can have potential applications such as the control of liquid droplet behavior at elevated temperatures for efficient cooling system.

• Journal of the Korean Society of Visualization
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• v.18 no.1
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• pp.18-25
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• 2020

The droplet impact behavior is dominated by some parameters such as surface temperature, We number, surface and fluid property. Especially, Leidenfrost effect which prevents the contact between surface and droplet is very powerful phenomenon for determining droplet impact behavior. Due to this effect, the impact regime is divided into contact boiling regime and film boiling regime whether the droplet contact with the surface. Many studies have found that surface micro-structures which processed by surface processing are effective to overcome the Leidenfrost effect. In this study, droplet impact behaviors were compared using ethanol both on flat and laser-ablated Al surface. On the flat surface, impact regime was mainly divided by surface temperature. And there is key dominant parameter for each regime. On the laser-ablated surface, we could see changed impact regime and different impact behavior such as jetting and ejection of tiny droplets despite of same impact conditions.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.39 no.7
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• pp.567-578
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• 2015

Single droplet-wall collision heat transfer characteristics on a heated plate above Leidenfrost temperature were experimentally investigated considering the effects of impact velocity. The collision characteristics of the droplet impinged on the heated wall and the changes in temperature distribution were simultaneously measured using synchronized high-speed video and infrared cameras. The surface heat flux distribution was obtained by solving the three-dimensional transient heat conduction equation for the heated substrate using the measured surface temperature data as the boundary condition for the collision surface. As the normal impact velocity increased, heat transfer effectiveness increased because of an increase in the maximum spreading diameter and a decrease in the vapor film thickness between the droplet and heated wall. For We < 30, droplets stably rebounded from a heated wall without breakup. However, the droplets broke up into small droplets for We > 30. The tendency of the heat transfer to increase with increasing impact velocity was degraded by the transition from the rebounding region to the breakup region; this was resulted from the reduction in the effective heat transfer area enlargement due to the breakup phenomenon.

• Plant Journal
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• v.16 no.3
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• pp.42-46
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• 2020

In the large LNG process in FLNG or FSRU, sudden temperature drops of the steel in the event of LNG leaks may cause brittle fracture of the structure. In this paper, we investigate the principle and process of forming a cryogenic fluid on a steel plate through a cryogenic spillage experiment, and analyze the correlation of the temperature distribution of the steel plate according to the distance from the nozzle and exposure time. Two types of cryogenic fluids were used: LN2 and LNG. The cyogenic liquid was released on the steel plate at 1.6L/min for LN2 and 1.5L/min for LNG. For the steel, DH was used and the temperature was measured at 10 points in total. The Leidenfrost effect was observed on the steel plate, and the temperature distribution of the steel was varied according the flow path and the heat of evaporation of the fluid.

• Nuclear Engineering and Technology
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• v.52 no.3
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• pp.508-519
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• 2020

During transients or accidents, the reactor core is uncovered, and droplets entrained above the quench front collides with the uncovered fuel rod surface. Droplet impact cooling can reduce the peak cladding temperature. Besides zirconium-based cladding, versatile accidental tolerant fuel (ATF) claddings, including FeCrAl, have been proposed to increase the accident coping time. In order to investigate the effect of surface properties on droplet impact cooling of cladding surfaces, the droplet impact phenomena are photographed on the FeCrAl and zircaloy-4 (Zr-4) surfaces under different conditions. On the oxidized FeCrAl surface, the Leidenfrost phenomenon is not observed even when the surface temperature is as high as 550 ℃ with We > 30. Comparison of the impact behaviors observed on different materials shows that nucleate and transition boiling is more intensive on surfaces with larger thermal conductivity. The Leidenfrost point temperature (LPT) decreases with the solid thermal effusivity (${\sqrt{k{\rho}C_p}}$). However, the CHF temperature is relatively insensitive to the surface oxidation and Weber number. Droplet spreading diameter is analyzed quantitatively in the film boiling stage. Based on the energy balance a correlation is proposed for droplet maximum spreading factor. A mechanistic model is also developed for the LPT based on homogeneous nucleation theory.

• Journal of computational fluids engineering
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• v.21 no.4
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• pp.90-95
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• 2016

Leidenfrost drops with ellipsoidal shaping can control the bouncing height by adjusting the aspect ratio(AR) of the shape at the moment of impact. In this work, we focus on the effect of the AR and the impact Weber number(We) on the non-axisymmetrical spreading dynamics of the drop, which plays an important role in the control of bouncing. To understand the impact dynamics, the numerical simulation is conducted for the ellipsoidal drop impact upon the perfect non-wetting solid surface by using volume of fluid method, which shows the characteristics of the spreading behavior in each principal axis. As the AR increases, the drop has a high degree of the alignment into one principal axis, which leads to the consequent suppression of bouncing height with shape oscillation. As the We increases, the maximum spreading diameters in the principal axes both increase whereas the contact time on the solid surface rarely depends on the impact velocity at the same AR. The comprehensive understanding of the ellipsoidal drop impact upon non-wetting surface will provide the way to control of drop deposition in applications, such as surface cleaning and spray cooling.

• Nuclear Engineering and Technology
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• v.35 no.4
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• pp.274-285
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• 2003

Film boiling heat transfer coefficients for a downward-facing hemispherical surface are measured from the quenching tests in DELTA (Downward-boiling Experimental Loop for Transient Analysis). Two test sections are made of copper to maintain Bi below 0.1. The outer diameters of the hemispheres are 120 mm and 294 mm, respectively. The thickness of both the test sections is 30 mm. The effect of diameter on film boiling heat transfer is quantified utilizing results obtained from the two test sections. The measured heat transfer coefficients for the test section with diameter 120 mm lie within the bounding values from the laminar film boiling analysis, while those for diameter 294 mm are found to be greater than the numerical results on account of the Helmholtz instability. There is little difference observed between the film boiling heat transfer coefficients measured from the two test sections. In addition, the higher thermal conductivity of copper results in the higher minimum heat flux in the tests. For the test section of diameter 120 mm, the Leidenfrost point is lower than that for the test section of diameter 294 mm. Destabilization of film boiling propagates radially inward for the 294 mm test section versus radially outward for the 120 mm Test Section.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.37 no.5
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• pp.459-465
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• 2013

In the manufacturing process of steel plates, materials at high temperatures above $800^{\circ}C$ are rapidly cooled by using a circular impinging water jet to determine their strength and toughness. In this study, the basic heat and fluid flow is solved by using the existing numerical model for boiling heat transfer. Actually, steel undergoes a phase change from austenite to ferrite or bainite during the cooling process. The phase change induces changes in its thermal properties. Instead of directly solving the phase change and the material cooling together, we solve the heat transfer only by applying the thermal properties that vary with temperature, which is already known from other studies. The effects of the changes in the thermal properties on the cooling of steel and the necessity of calculating the phase change are discussed.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.38 no.12
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• pp.1051-1056
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• 2014

After hot rolling, a high-temperature steel plate with a temperature higher than $800^{\circ}C$ is rapidly cooled by multiple circular water jets. In this cooling process, because the temperature of the steel plate is much higher than the boiling point of the cooling water, film-boiling heat transfer occurs and a very thin steam layer forms between the plate surface and the cooling water. The steam layer acts as a thermal resistance that prevents heat transfer between the cooling water and the steel plate. In addition to the film-boiling heat transfer, complex physical phenomena such as the free-surface flow of residual water that accumulated on the material and the material's high-speed motion also occur in the cooling process. In this study, the simultaneous cooling process of the upper and lower sides of a running hot steel strip is investigated using a three-dimensional numerical model and the cooling performances and characteristics of the upper-side cooling and lower-side cooling are compared.