• Title/Summary/Keyword: Lead determination

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Determination of Adequate Solder Volume using 3D Solder Joint Configuration in SMT (3차원 납 접합부 형상을 이용한 표면실장기술의 적정 납량 결정)

  • 최동필;김성관;유중돈
    • Journal of Welding and Joining
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    • v.14 no.2
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    • pp.71-78
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    • 1996
  • In order to rpovide proper SMT design criteria in a systematic way, a mathematical formulation has been developed to predict the configuration of the solder fillet formed between the gullwing type lead and rectangular pad. Effects of SMT design parameters such as the solder volume and pad dimension on the solder profile are investigated using the FEM that calculates the 3D configuration by minimizing the energy due to surface tension and gravity in the equilibrium state. Design criteria of QFP and SOP are illustrated by plotting the acceptable range of the solder volume with respect to the length and width ratios of the pad and lead. The results show that the acceptable design range increases with increase in the pad length and width. The pad length has more significant effects on design criteria compared with the pad width, and Bond number can be utilized to predict the joint quality.

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Implementation of Finite Capacity-Driven MRP-C System (한정된 제조자원능력을 고려한 MRP-C 시스템 적용)

  • 김동규;박재현;강경식
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.22 no.51
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    • pp.117-127
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    • 1999
  • Modern production control systems based on MRPⅡ (Manufacturing Resource planning) didn't solved about the capacity and lead time problems. In the past, It solved that problems under deterministic. Therefore, the problem about determination of correct lead time and finite capacity are studied continuously by researchers. Now, we need to a integrated method that is from low level to high level instead of top-down in MRP. In this research uses the MRP-C(Capacitated Material Requirement Planning) concept that is more efficient then MRP system for capacity and flexible lead time , and shows the MRP-C algorithm and the prototype.

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Stress Determination in Epitaxial Lead Titanate Films by Asymmetric X-ray Diffraction Method

  • Uchida, Hiroshi;Kiguchi, Takanori;Wakiya, Naoki;Shinozaki, Kazuo;Mizutani, Nobuyasu
    • The Korean Journal of Ceramics
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    • v.6 no.4
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    • pp.385-389
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    • 2000
  • Residual stresses in epitaxial films were measured by X-ray diffraction method. Lattice strains of the (hkl) planes measured along particular Ψ-angles were converted to the in-plane stress according to the equation of stress-strain tensor conversion. Residual tensile stresses were observed in epitaxial PbTiO$_3$ films deposited on (100) SrTiO$_3$ substrate. Tensile stresses approximately 0.9 GPa were measured in Pb-rich films, while it increased to approximately 2.0 GPa with the decreasing of Pb content in the case of Pb-poor films, which ascribed to the formation of lead and oxygen vacancies (expressed as x in Pb$_1-x$TiO$_3-x$).

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Batch Unscented Transformation for Satellite Orbit Determination Using A Satellite Laser Ranging (SLR)

  • Seo, Kyoung-Seok;Park, Sang-Young;Park, Eun-Seo;Kim, Young-Rok;Choi, Kyu-Hong
    • Bulletin of the Korean Space Science Society
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    • 2008.10a
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    • pp.34.2-34.2
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    • 2008
  • The batch least square filter is widely used for ground estimations. However, in orbit determination (OD) under inaccurate initial conditions and few measurement data the performance by the batch least square filter can lead an unstable results. To complement weak part of the batch filter, the batch unscented transformation without any linearization process is developed by ACL (Astrodynamics and Control Laboratory) in YONSEI University. In this paper, the batch unscented transformation is introduced and applied to satellite orbit determination using Satellite Laser Ranging (SLR) data. Only range of the satellite measured from ground tracking stations is used for measurement data. The results of simulation test are compared with those of the weighted batch least square filter for various initial states errors (position and velocity). Simulation results show that the batch unscented transformation is comparable or slightly superior to batch least square filter in the orbit determination.

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Rayleigh-Ritz procedure for determination of the critical load of tapered columns

  • Marques, Liliana;Da Silva, Luis Simoes;Rebelo, Carlos
    • Steel and Composite Structures
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    • v.16 no.1
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    • pp.45-58
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    • 2014
  • EC3 provides several methodologies for the stability verification of members and frames. However, when dealing with the verification of non-uniform members in general, with tapered cross-section, irregular distribution of restraints, non-linear axis, castellated, etc., several difficulties are noted. Because there are yet no guidelines to overcome any of these issues, safety verification is conservative. In recent research from the authors of this paper, an Ayrton-Perry based procedure was proposed for the flexural buckling verification of web-tapered columns. However, in order to apply this procedure, Linear Buckling Analysis (LBA) of the tapered column must be performed for determination of the critical load. Because tapered members should lead to efficient structural solutions, it is therefore of major importance to provide simple and accurate formula for determination of the critical axial force of tapered columns. In this paper, firstly, the fourth order differential equation for non-uniform columns is derived. For the particular case of simply supported web-tapered columns subject to in-plane buckling, the Rayleigh-Ritz method is applied. Finally, and followed by a numerical parametric study, a formula for determination of the critical axial force of simply supported linearly web-tapered columns buckling in plane is proposed leading to differences up to 8% relatively to the LBA model.

Precision orbit determination with SLR observations considering range bias estimation

  • Kim, Young-Rok;Park, Sang-Young;Park, Eun-Seo;Park, Jong-Uk;Jo, Jung-Hyun;Park, Jang-Hyun
    • Bulletin of the Korean Space Science Society
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    • 2010.04a
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    • pp.27.5-28
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    • 2010
  • The unexpected observation condition or insufficient measurement modeling can lead to uncertain measurement errors. The uncertain measurement error of orbit determination problem typically consists of noise, bias and drift. It must be removed by using a proper estimation process for better orbit accuracy. The estimation of noise and drift is not easy because of their random or unpredictable variation. On the other hand, bias is a constant difference between the mean of the measured values and the true value, so it can be simply removed. In this study, precision orbit determination with SLR observations considering range bias estimation is presented. The Yonsei Laser-ranging Precision Orbit Determination System (YLPODS) and SLR NP (Normal Point) observations of CHAMP satellite are used for this work. The SLR residual test is performed to estimate the range bias of each arc. The result shows that we can get better orbit accuracy through range bias estimation.

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Study on Determination of Seven Transition Metal Ions in Water and Food by Microcolumn High-Performance Liquid Chromatography

  • Hu, Qiufen;Yang, Guangyu;Li, Haitao;Tai, Xi;Yin, Jiayuan
    • Bulletin of the Korean Chemical Society
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    • v.25 no.5
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    • pp.694-698
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    • 2004
  • A new method for the simultaneous determination of seven transition metal ions in water and food by microcolumn high-performance liquid chromatography has been developed. The lead, cadmium, mercury, nickel, cobalt, silver and tin ions were pre-column derivatized with tetra-(4-aminophenyl)-porphyrin ($T_4$-APP) to form the colored chelates which were then enriched by solid phase extraction with $C_{18}$ cartridge. The enrichment factor of 50 was achieved by eluted the retained chelates from the cartridge with tetrahydrofuran (THF). The chelates were separated on a ZORBAX Stable Bound microcolumn ($2.0{\times}50\;mm,\;1.8\;{\mu}m$)with methanol-tetrahydrofuran (95 : 5, v/v, containing 0.05 mol/L pyrrolidine-acetic acid buffer salt, pH = 10.0) as mobile phase at a flow rate of 0.5 mL/min and detected with a photodiode array detector from 350-600 nm. The seven chelates were separated completely within 2.0 min. The detection limits of lead, cadmium, mercury, nickel, cobalt, silver and tin are 4 ng/L, 3 ng/L, 6 ng/L, 5 ng/L, 5 ng/L, 6 ng/L, 4 ng/L respectively in the original samples. This method was applied to the determination of the seven transition metal in water and food samples with good results.

Effectiveness of the Sensor using Lead Dioxide Electrodes for the Electrochemical Oxygen Demand (전기화학적 산소요구량 측정용 이산화납 전극 센서의 유효성)

  • Kim, Hong-Won;Chung, Nam-Yong
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.21 no.4
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    • pp.575-581
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    • 2012
  • The electrochemical oxygen demand (ECOD) is an additional sum parameter, which has not yet found the attention it deserves. It is defined as the oxygen equivalent of the charge consumed during an electrochemical oxidation of the solution. Only one company has yet developed an instrument to determine the ECOD. This instrument uses $PbO_2$-electrodes for the oxidation and has been successfully implemented in an automatic on-line monitor. A general problem of the ECOD determination is the high overpotential of electrochemical oxidations of most organic compounds at conventional electrodes. Here we present a new approach for the ECOD determination, which is based on the use of a solid composite electrodes with highly efficient electro-catalysts for the oxidation of a broad spectrum of different organic compounds. Lead dioxide as an anode material has found commercial application in processes such as the manufacture of sodium per chlorate and chromium regeneration where adsorbed hydroxyl radicals from the electro-oxidation of water are believed to serve as the oxidizing agent. The ECOD sensors based on the Au/$PbO_2$ electrode were operated at an optimized applied potential, +1.6 V vs. Ag/AgCl/sat. KCl, in 0.01 M $Na_2SO_4$ solution, and reduced the effect of interference ($Cl^-$ and $Fe^{2-}$) and an expended lifetime (more than 6 months). The ECOD sensors were installed in on-line auto-analyzers, and used to analyze real samples.

Determination of Metals of Coal and Respirable Coal Dust in Gangneung and Taebaek Coal Mines (강릉·태백지역 석탄광산의 탄 및 호흡성 탄분진중 금속 농도 비교에 관한 연구)

  • Kim, Hae Jeong;Choi, Ho Chun;Chung, Ho Keun
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.1 no.1
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    • pp.82-88
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    • 1991
  • Determination of Cu, Fe, Ni, Pb, and Zn concentrations in coal and respirable coal dust were performed by atomic absorption spectrophotometry. The coal samples of 18 coal mines in Gangneung area were collected and 25 coal mines in Taebaek area. Crushed coal samples were divided into three mesh sizes. The results were as follows : 1. Metal concentrations of coals in Gangneung area by sieve sizes( -100/+200 mesh, -200/+325 mesh, -325 mesh) were as follows: Cu ; 20, 18, 19, Fe ; 1,830, 1,765, 1,107, Pb ; 6, 8, 14, Ni ; 17, 17, 14, Zn ; 4, 2, $4{\mu}g/g$, respectively. Metal concentrations in coals in Taebaek area by sieve sizes(-100/+200 mesh, -200/+325 mesh, -325 mesh) were as follows: Cu ; 30, 32, 26, Fe ; 1,741, 1,822, 1,773, Pb ; 8, 9, 7, Ni ; 13, 13, 13, Zn ; 8, 5, $4{\mu}g/g$, respectively. There were not significant differences of Cu, Fe, Ni, Pb, and Zn concentrations of coals statistically in Gangneung and Taebaek area by sieve size. 2. Metal concentrations of coals in Gangneung and Taeback area were as follows : Cu ; 19, 30, Fe ; 1,514, 1,778, Pb ; 9, 8, Ni ; 16, 13, Zn ; 3, $6{\mu}g/g$, respectively. Differences of copper and zinc concentrations of coal samples were significant between Gangneung and Taebaek area, but those of iron, nickel and lead concentrations were not significant. 3. Copper, iron, lead, nickel and zinc concentrations of coals and respirable coal dust were as follows : Cu ; 30, 6, Fe ; 1,779, 5,075, Pb ; 8, 7,814, Ni ; 13, 5,681, Zn ; 5, $134{\mu}g/g$, respectively. Differences of nickel, lead and zinc concentrations were significant between coals and respirable coal dust but those of copper and iron concentrations were not significant.

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The role of matrix modifier for the determination of Lead (Pb) in blood by graphite furnace atomic absorption spectrometry (흑연로 원자흡수분광법에 의한 혈중 납분석시 매트릭스 변형제의 역할)

  • Yoo, Kwang-Sik;Kwon, Jin-Kee
    • Analytical Science and Technology
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    • v.5 no.4
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    • pp.349-358
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    • 1992
  • The direct determination of lead in the whole-blood by graphite furnace atomic absorption spectrometric analysis was carried out by using the sample which was diluted five-fold with 1% Triton X-100. Matrix modification was tried to remove the interferences of blood matrix and also to get the optimum analytical condition. Good agreement with certificated values in reference materials(bovine blood) supplied by comparison program in Japan was obstained when 1% $(NH_4)_2HPO_4$ as matrix modifier and ashing temperature, $700^{\circ}C$ were used or 1% $(NH_4)_2HPO_4$ and 0.1% $PdCl_2$ as matrix modifier and ashed at $700^{\circ}C$. Standard deviations were appeared as 2.2~6.3% for 1% $(NH_4)_2HPO_4$ and 3.1~9.1% for 1% $(NH_4)_2HPO_4$ and 0.1% $PdCl_2$ in the range of $31{\sim}624{\mu}gPb/l$.

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