• Title/Summary/Keyword: Lab Scale 실험

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Recovery of Iron-Nickel Alloy Etching Waste Solution in Pilot Scale (파일럿 규모에서 철-니켈 합금 에칭폐액 재생)

  • Chae, Byungman;Kim, Dae-Weon;Hwang, Sung-Ok;Kim, Deukhyeon;Lee, Sangwoo
    • Clean Technology
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    • v.23 no.4
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    • pp.393-400
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    • 2017
  • In this study, we have developed a process for separating and recovering Ni and Fe in solution through a new solvent instead of TBP and Alamine336, which are solvents used in the conventional solvent extraction method. Experimental conditions were optimized through lab test and a $10L\;h^{-1}$ pilot plant was constructed for commercialization. In addition, the process data for mass production were obtained through pilot experiment and it was confirmed that there is no problem in product quality that can be used through the corrosion test of ferric chloride.

Attrition Characteristics of Korean Antracite Ash in Fluidized Bed Combustors (유동층 연소로에서 국내탄 회재의 마모 특성)

  • Lee, See Hoon;Kim, Sang Done;Kim, Jae Sung;Lee, Jong Min
    • Applied Chemistry for Engineering
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    • v.17 no.5
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    • pp.547-551
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    • 2006
  • In the reactor following the American standard test method (ASTM) D5757-95 and lab-scale fluidized bed combustor, the attrition characteristics of sand and ash of Korean anthracite were investigated. The attrition characteristics, such as particle size distribution of fly ash, attrition rate, and attrition ratio etc, were studied with variation of gas velocities. The particle attrition of ash was more active than sand which was generally used as a fluidized material and also the attrition index of ash taken by ASTM D5757-95 was 5 times higher than that of sand. The formation of fine particles continuously occurred due to particle attrition with increasing gas velocities. The following equation has been suggested for attrition rate of ash. $$\frac{dW}{dt}=-3.18{\times}10^{-7}(U-U_{mf})W$$.

Optimization and Scale-up of Fish Skin Peptide Loaded Liposome Preparation and Its Storage Stability (어피 펩타이드 리포좀 대량생산 최적 조건 및 저장 안정성)

  • Lee, JungGyu;Lee, YunJung;Bai, JingJing;Kim, Soojin;Cho, Youngjae;Choi, Mi-Jung
    • Food Engineering Progress
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    • v.21 no.4
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    • pp.360-366
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    • 2017
  • Fish skin peptide-loaded liposomes were prepared in 100 mL and 1 L solution as lab scales, and 10 L solution as a prototype scale. The particle size and zeta potential were measured to determine the optimal conditions for the production of fish skin peptide-loaded liposome. The liposome was manufactured by the following conditions: (1) primary homogenization at 4,000 rpm, 8,000 rpm, and 12,000 rpm for 3 minutes; (2) secondary homogenization at 40 watt (W), 60 W, and 80 W for 3 minutes. From this experimental design, the optimal conditions of homogenization were selected as 4,000 rpm and 60 W. For the next step, fish peptides were prepared as the concentrations of 3, 6, and 12% at the optimum manufacturing conditions of liposome and stored at $4^{\circ}C$. Particle size, polydispersion index (pdI), and zeta potential of peptide-loaded liposome were measured for its stability. Particle size increased significantly as manufacture scale and peptide concentration increased, and decreased over storage time. The zeta potential results increased as storage time increased at 10 L scale. In addition, 12% peptide showed the formation of a sediment layer after 3 weeks, and 6% peptide was considered to be the most suitable for industrial application.

Effect of Internal Flow Guide in Pintle Tip on Pintle Injector Thruster Combustion (핀틀 인젝터의 팁 내부 유동 가이드가 연소 성능에 미치는 영향)

  • Lee, Keonwoong;Nam, Jeonsoo;Radhakrishnan, Kanmaniraja;Koo, Jaye
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.48 no.9
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    • pp.703-709
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    • 2020
  • Pintle injector is known to have been adopted as injector of Lunar Module Descent Engine (LMDE) and contributed to success of the Apollo program and recently used in merlin engine. In this study, 500N Lab-Scale pintle injector thruster was manufactured and the combustion experiment with LOx/GCH4 was conducted. However, the proto-type thruster was showed some problems, such as low combustion efficiency and melting of pintle tip. To solve these problems, the flow guide in pintle tip was suggested through the CFD simulation. After addition of flow guide module, the combustion efficiency increased and pintle tip did not melt until the end of combustion.

In-situ Bioremediation of Total Petroleum Hydrocarbons-Contaminated Soil by Pseudomonas Species (토양 내 TPH(Total Petroleum Hydrocarbons)의 생물학적 분해 연구)

  • Kim, Jee-Young;Lee, Sang-Seob
    • Microbiology and Biotechnology Letters
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    • v.39 no.2
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    • pp.161-167
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    • 2011
  • We previously showed that five strains belonging to Pseudomonas could remove TPH (Total Petroleum Hydrocarbons) efficiently when they are applied to TPH-contaminated soil. We optimized the bioremediation condition using different hydrocarbons and nutrients conditions to improve the efficiency. We setup lab-scale column bioreactor to monitor TPH and diesel removal efficiency. When we applied five Pseudomonas sp. mixtures to 25,000 $mg{\cdot}kg^{-1}$ TPH-contaminated soil (diesel 10,000 $mg{\cdot}kg^{-1}$, kerosene 10,000 $mg{\cdot}kg^{-1}$, gasoline 5,000 $mg{\cdot}kg^{-1}$) with the optimum condition, 76.3% of TPH removal efficiency was shown for 25 days. Meanwhile, in the application of five Pseudomonas sp. mixtures to 20,000 $mg{\cdot}kg^{-1}$ diesel-contaminated soil with the optimum condition, 99.2% of diesel removal efficiency was shown for 40 days. In the application to lab-scale bioreactor with five high efficiency bacteria, 88.5% of TPH removal efficiency was shown for 45 days. Based on the results from this study, we confirmed that this mixed Pseudomonas sp. consortium might improve the bioremediation of TPH in contaminated soil, the efficacy can be controlled by improving the nutrients. We also confirmed that the nutrients and oxygen for biodegradation of TPH could contribute on the management and control of applications of these strains for the study of bioremediation of TPH-contaminated soil.

Computational Fluid Dynamics(CFD) Simulation for a Pilot-scale Selective Non-catalytic Reduction(SNCR) Process Using Urea Solution (요소용액을 이용한 파일럿규모 SNCR 공정에 대한 CFD 모델링 및 모사)

  • Nguyen, Thanh D.B.;Kang, Tae-Ho;Lim, Young-Il;Kim, Seong-Joon;Eom, Won-Hyeon;Yoo, Kyung-Seun
    • Korean Chemical Engineering Research
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    • v.46 no.5
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    • pp.922-930
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    • 2008
  • The selective non-catalytic reduction(SNCR) performance is sensitive to the process parameters such as flow velocity, reaction temperature and mixing of reagent(ammonia or urea) with the flue gases. Therefore, the knowledge of the velocity field, temperature field and species concentration distribution is crucial for the design and operation of an effective SNCR injection system. In this work, a full-scale two-dimensional computational fluid dynamics(CFD)-based reacting model involving a droplet model is built and validated with the data obtained from a pilot-scale urea-based SNCR reactor installed with a 150 kW LPG burner. The kinetic mechanism with seven reactions for nitrogen oxides($NO_x$) reduction by urea-water solution is used to predict $NO_x$ reduction and ammonia slip. Using the turbulent reacting flow CFD model involving the discrete droplet phase, the CFD simulation results show maximum 20% difference from the experimental data for NO reduction. For $NH_3$ slip, the simulation results have a similar tendency with the experimental data with regard to the temperature and the normalized stoichiometric ratio(NSR).

Shipboard sewage treatment using Membrane Sequence Batch Reactor (MSBR을 이용한 크루즈선 오.폐수 처리 장치)

  • Kim, In-Soo;Lee, Eon-Sung;Oh, Yeom-Jae;Kim, Eog-Jo
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2010.04a
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    • pp.395-396
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    • 2010
  • Lab scale experiment study was carried out for biological process development on cruise. SBR(Sequence Bath Reactor), MBR(Membrane Bioreactor), and MSBR(Membrane Sequence Bath Reactor) system were investigated for practical application on shipboard sewage treatment. From the results it was suggested that MSBR system might be suitable process for cruise in terms of pollutant removal efficiency, maintenance and special environmental conditions of cruise. Based on Res. MEPC.159(55) the MSBR system was qualified for the required regulations.

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Estimation of Propellant Consumption during Thrust Control of GOx/PC Hybrid Rocket (GOx/PC 하이브리드 로켓의 추력제어 환경에서 후퇴거리 예측)

  • Kang, Wan-Kyu;Huh, Hwan-Il
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2009.11a
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    • pp.526-529
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    • 2009
  • In this study, we analyze the characteristic of burning classified by a propellant according to a flux of an oxidizer to analyze propellant regression distance in accordance with a thrust control and burning time of hybrid rocket using hybrid combustor of Lab-Scale. To control a flux of an oxidizer, we design flow control system to regulate the mount of opening and shutting of a needle valve by a driving of stepping motor by a combination the needle valve with stepping motor. We derive the relationships between mass flow rate and regression rate according to a propellant through the oxidizer flux change. While doing the thrust control, we estimate regression distance through the oxidizer flux in accordance with thrust and confirm the creditability through the actual thrust control burning experimentation.

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Control of Turbid Water Transport with Filamentous Mat (섬모상 매트에 의한 탁수이동차단에 관한 실험적 연구)

  • Yu, Jianghua;Yi, Qitao;Kim, Youngchul
    • Journal of Korean Society on Water Environment
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    • v.26 no.1
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    • pp.44-51
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    • 2010
  • A lab-scale apparatus for turbid water transport control was tested and examined. The channel had a dimension of $100cm{\times}30cm{\times}15cm$ (length${\times}$hight${\times}$width). And the turbidity water was prepared using two types of particles, bentonite and loess. The channel equipped with filamentous mat was operated under various shock load conditions. In the control channel, instantly, turbid water mixed with the clean water inside the channel and turbidity prevails the entire channel. While in the mat-equipped channel, it increases only at the bottom. Overall, the filamentous mat gave capture efficiency of 70~90% compared with the control group. The capture efficiency of turbid particles decreased with increased input turbidity flux. The result of experimental run on how turbid particles are separated in the mat channel shows that settling, filtration and attachment are the main processes. Meanwhile, turbidity was diffused from the channel bottom due to turbidity gradient before and after mat zone. The particle size before mat zone was lightly coarser than that after mat zone.

Multiphase Simulation of a Liquid Jet in a Lab-scale Ramjet Combustor (모형 램젯 연소기에서 액체제트의 다상유동 해석)

  • Oh, Jeong-Seog;Lee, Won-Nam;Lee, Jong-Geun;Santavicca, Dominique A.
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2010.11a
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    • pp.386-392
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    • 2010
  • The multiphase simulation of a liquid jet in a lab-scale ramjet combustor with a plain orifice type injector was studied with a commercial CFD tool, a FLUENT program. The objectives of the current study are to analysis the breakup characteristics of a hexane liquid jet in a cross flow and to derive the correlation between flow conditions and drag force coefficients in a test section. From the result of a numerical simulation, we concluded that a DPM and Realizable $k-{\varepsilon}$ model with an enhanced wall treatment were available to simulate the multiphase flow simulation. And the calculated distribution of a hexane vapor concentration was well-matched with experimental results.

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