• 제목/요약/키워드: L3Shim

검색결과 662건 처리시간 0.026초

식용유지에 대한 붉나무 추출물의 항산화 효과 (Antioxidant Activity of Ethanol Extract from Rhus javanica $Linn\'{e}$ on Edible Oil)

  • 최웅;신동화;장영상;신재익
    • 한국식품과학회지
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    • 제24권4호
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    • pp.320-325
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    • 1992
  • 천연 항산화 물질을 분리하고자 식용 또는 한약재로 이용되는 붉나무를 75% ethyl alcohol로 항산화 성분을 추출하여 chloroform, ethyl acetate 등의 용매를 사용하여 separatory funnel, column chromatography로 분획하여 얻은 분획물의 항산화 효과를 검토하였다. 붉나무 추출물중 항산화 효과를 나타내는 유효성분은 ethyl acetate와 chloroform에 잘 용해되는 물질로, ethyl acetate로 분리한 분획물을 팜유에 600 ppm 첨가시 AI는 1.60, 돈지에서는 AI가 3.90으로 이들 용매로 분리한 분획물의 항산화 효과는 붉나무 추출 원액보다 높은 현상을 보였다. 붉나무 추출물을 팜유, 돈지 및 대두유에 농도별로 첨가하여 $60^{\circ}C$에 저장하면서 POV, AV 및 TBA가를 측정하여 이들 유지에 대한 산화안정성을 시험한 결과 Rancimat test 결과와 비슷하여 팜유에는 항산화 효과가 뚜렷하였고, 돈지에는 탁월한 결과를 보였다.

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MOCVD Multiwafer Technology for Mass Production Application

  • Hwang, D.H.;Do, L.M.;Chu, H.Y.;Zyung, T.;Lee, C.J.;Holmes, A.B.;Shim, H.K.;Protzmann, H.;Schmitz, D.;Strauch, G.;Heuken, M.;Juergensen, H.
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 1998년도 IUMRS-ICEM ABSTRACT BOOK
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    • pp.70.3-70
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    • 1998
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저압 SCR을 위한 디젤발전기 배기가스 온도 변화 (Temperature Variation of Exhaust Gas in Diesel Generator for Low Pressure SCR)

  • 홍철현;이창민;이상득
    • 해양환경안전학회지
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    • 제27권2호
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    • pp.355-362
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    • 2021
  • L.P SCR의 촉매 반응을 위해 선박의 발전기용 4행정 디젤엔진의 배기가스 온도를 높게 설계 할 수밖에 없었다. 본 연구의 목적은 밸브개폐시기와 연료분사시기를 조정을 통한 배기가스의 온도 감소가 L.P SCR의 운전조건을 만족시키고 고온으로 인한 발전기 엔진의 사고를 예방하기 위함이었다. 배기가스 온도를 하강시키기 위해 캠샤프트의 각도를 조정하고 연료분사펌프의 Shim을 추가하였다. 그 결과 최대폭발압력은 12.8 bar 증가하였고 터보차저 출구온도 평균값은 13.3 ℃ 하강하였다. 터보차저 출구에서 SCR 입구까지의 열손실을 감안하더라도 L.P SCR 운전조건인 SCR 챔버 입구 온도인 290 ℃를 만족하였다. 배기가스 온도 하강을 통해 디젤발전기의 안전운전이 가능하게 한 연구였다.

미만성 척수 경막외 농양을 동반한 화농성 척추염 - 증 례 보 고 - (Pyogenic Spondylitis with Diffuse Spinal Epidural Abscess - A Case Report -)

  • 김훈;김성민;정대진;심영보;박용기;최선길
    • Journal of Korean Neurosurgical Society
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    • 제29권8호
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    • pp.1074-1079
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    • 2000
  • We report a case of pyogenic spondylitis on L2 and L3 with diffuse epidural abscess up to T4 to L3 and large psoas abscess. A forty-nine-year old male was presented with progressive back pain, left flank pain and ab-dominal distention, weakness of the both legs and voiding and defecation difficulty during last 2 months. Initially multiple coronal hemilaminectomies from T4 to T12 were done for the treatment of diffuse thoracic epidural ab-scess. Then second operation via left retroperitoneal approach was performed for lumbar spondylitis and psoas abscess on third day after initial operation. After removal and curettage of pyogenic psoas and epidural abscess and spondylitis (L2-L3), iliac bone grafting with Keneda instrumentation from L1 to L4 was done simultaneously. Postoperative course has been unevenful without recurrent infection. The literature on diffuse epidural and large psoas abscess with pyogenic spondylitis are reviewed and instrumentation for stabilization of pyogenic spondylitis is also discussed.

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Macrocyclic Isomers with S2O-Donor Set as Silver(I) Ionophores

  • Park, Sung-Bae;Yoon, Il;Seo, Joo-beom;Kim, Hyun-Jee;Kim, Jae-Sang;Lee, Shim-Sung
    • Bulletin of the Korean Chemical Society
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    • 제27권5호
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    • pp.713-717
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    • 2006
  • $S_2O$-donor macrocyclic isomers incorporating a xylyl group in o- ($L^1$), m- ($L^2$) and p-positions ($L^3$) extract no metal ions except silver(I) from aqueous to chloroform phase. And the magnitudes of %Ex for silver(I) are in the order of $L^1$ > $L^2$ > $L^3$. Taking this result into account, $L^1$-$L^3$ were utilized as membrane active components to prepare potentiometric silver(I)-selective electrodes. The proposed macrocycles-based electrodes E1 ($L^1$), E2 ($L^2$) and E3 ($L^3$) exhibited comparable results which show considerable selectivity toward silver(I) over alkali, alkali earth and other transition metal ions. Comparative NMR study on $L^1$-$L^3$ and their complexes with silver(I) in solution was also accomplished. In addition, a unique sandwich-type complex $[Ag(L^1)_2]CIO_4$ was prepared from the assembly reaction of $L^1$ with $AgClO_4$ and structurally characterized by an X-ray diffraction analysis.

식물성 천연 항산화물질의 검색과 그 항산화력 비교 (Screening of Natural Antioxidant from Plant and Their Antioxidative Effect)

  • 최웅;신동화;장영상;신재익
    • 한국식품과학회지
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    • 제24권2호
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    • pp.142-148
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    • 1992
  • 95종의 식용 혹은 약용식물로부터 에탄올과 물을 용매로 하여 얻은 126종의 추출물을 괌유, 돈지 및 대두유에 첨가하여 Rancimat으로 항산화 효과를 비교하였다. 항산화 효과가 인정되면서 추출 수율이 높은 민들레, 질경이, 붉나무, 택란엽, 황기, 포공영 등 6종을 1차 선발하여 각 추출물을 농도별로 실험한 결과 붉나무 추출물이 팜유 및 돈지의 유도기간을 연장시키는데 우수한 효과를 보였다. 붉나무 추출물을 팜유에 600ppm 첨가시 AI(Antioxidant index, 각 항산화제 첨가구의 유도기간을 무첨가구의 유도기간으로 나눈 값)는 1.35였고, 돈지에서는 AI가 3.03으로 돈지에 효과가 우수하였다.

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A Triple-Probe Channel NO2S2-Macrocycle: Synthesis, Sensing Characteristics and Crystal Structure of Mercury(II) Nitrate Complex

  • Lee, Ji-Eun;Choi, Kyu-Seong;Seo, Moo-Lyong;Lee, Shim-Sung
    • Bulletin of the Korean Chemical Society
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    • 제31권7호
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    • pp.2031-2035
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    • 2010
  • A triple-probe channel type chemosensor based on an $NO_2S_2$-macrocycle functionalized with phenyltricyanovinyl group was synthesized and its sensing characteristics were examined. The pink-red solution of L changed selectively to pale yellow upon addition of $Hg^{2+}$. The selective fluorometric response of L to all the tested metal ions was studied. The results showed that a large enhancement of the fluorescence of L was observed only in the case of $Hg^{2+}$. In addition, L showed large anodic shift (~ 0.3 V) for the addition of excess $Hg^{2+}$. Through above three observed results by the different techniques, we confirmed that the proposed chemosensor acts as the multiple-probe channel sensing material. The crystal structure of mercury(II) nitrate complexs of L which shows a 1-D polymer network with a formula $[Hg_2(L)_2(NO_3)_2({\mu}-NO_3)_2]_n$ was also reported.

Elucidation of Antifungal Metabolites Produced by Pseudomonas aurantiaca IB5-10 with Broad-Spectrum Antifungal Activity

  • Park, Gwee-Kyo;Lim, Jong-Hui;Kim, Sang-Dal;Shim, Sang-Hee
    • Journal of Microbiology and Biotechnology
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    • 제22권3호
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    • pp.326-330
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    • 2012
  • Antifungal metabolites were isolated from a culture of Pseudomonas aurantiaca IB5-10. Chemical structures of the metabolites were elucidated as phenazine-1-carboxylic acid (PCA; 1), 2-hydroxyphenazine (2-OH-PHZ; 2), and cyclo-(L-Pro-L-Val; 3), respectively, based on spectroscopic methods. Among them, 3 was isolated for the first time from this strain. The antifungal activities of 1-3 were evaluated against a variety of plant pathogens. To the best of our knowledge, the antifungal activities of 3 against plant fungal pathogens have been evaluated for the first time in this work. PCA (1) showed the most potent antifungal activities against Phytophthora capsici, Rhizoctonia solani AG-1(IA), and Pythium ultimum with MICs (${\mu}g/ml$) of less than 1.0, 1.3, and 2.0, respectively. On the other hand, 2-OH-PHZ (2) showed potent antifungal activity against R. solani AG-1(IA) with the MIC (${\mu}g/ml$) of 2.0, whereas it showed moderate antifungal activity against P. ultimum with the MIC (${\mu}g/ml$) of 50.0. In addition, 3 showed antifungal activity against only R. solani AG-1(IA).

목모 패널용 Geopolymer Binder 개발에 관한 실험적 연구 (An Experimental Study on the Geopolymer for Wood Wool Ceramic Board)

  • 박동철;이세현;송태협;심종우
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2005년도 추계 학술발표회 제17권2호
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    • pp.711-714
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    • 2005
  • This paper focused on development of geopolymer for wood wool ceramic board. Geopolymer can substitude ordinary portland cement and its accelerator of wood wool cement board as inorganic polymer. In this study, what we would obtain geopolymer's properties such as initial setting time(KS L 5108), flow(KS L 5102) and compressive strength of 3days aged(KS L 5105), was less than 1 hour, more than $110\%$, more than 40Mpa. Geopolymer have three essential materials called filler, hardener and geopolymer liquor. So, We applied filler by quartz, hardener by blast furnace slag powder, metakaoline and fly ash, geopolymer liquor by NaOH, KOH and sodium silicate solution. As result of this experiment, what we could obtain best fitted geopolymer's properties such as initial setting time, flow and compressive strength of 3days aged, was 45min, $116\%$ and 43.6Mpa. This result can be applicable to commercial wood wool ceramic board.

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한국산(韓國産) 칠성장어속(屬) 무악류(無顎類)(Agnatha, Petromyzonidae)의 핵형(核型) (The Chromosomes of the Lamprey on the Genus Lampetra (Agnatha, Petromyzonidae) from Korea)

  • 심재환;김익수;이은희
    • 한국어류학회지
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    • 제4권2호
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    • pp.77-81
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    • 1992
  • 한국산(韓國産) 칠성장어속(屬) 무악류(無顎類) 3종(種) L. japonica, L. reissneri, L. sp.에 대한 핵형(核型)을 조사하였던 바, 이들은 모두 약 160여개 정도의 dot chromosome형태였으며 염색체(染色體) 수(數)에 있어서 종간(種間)의 유의한 차이는 인정할 수 없었다.

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