• 제목/요약/키워드: K-EDS

검색결과 1,296건 처리시간 0.026초

A study on the coating of silver nanoparticles on fabric surfaces with 3-Mercaptopropyltrimethoxysilane(MPTMS)

  • Park, Jeong-Eun;Jung, Da-Un;Lee, Jae-Woong;Kim, Sam-Soo
    • 한국염색가공학회:학술대회논문집
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    • 한국염색가공학회 2009년도 학술발표대회
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    • pp.110-111
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    • 2009
  • A solution containing 3-Mercaptopropyltr-imethoxysilane(MPTMS) was employed to modify surface of cotton fabrics with a silver colloid. Silver nanoparticles were applied on cotton fabrics via treatment with 3-MPTMS. The rate of silver nanoparticles on the fabric surface were measured with Energy Dispersive Spectroscopy(EDS). EDS results confirm the silver atom on the cotton surface.

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DC 계통연계형 태양광 PCS 개발 (Development of DC grid-connected Photovoltaic PCS)

  • 윤여영;김홍성;최재호
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2016년도 전력전자학술대회 논문집
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    • pp.19-21
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    • 2016
  • 본 논문에서는 DC 계통연계형 태양광 PCS 개발에 대해서 다루고 있다. 개발된 DC 계통연계형 태양광 PCS 시스템의 전력회로 구성, 전력회로 동작원리, Fixed Frequency Series Resonant DC/DC Converter 출력 전압 제어 원리 및 제어기 구성에 대해서 살펴보고, 시뮬레이션 및 제작된 시스템의 실험결과를 통해 개발된 시스템의 타당성을 입증하였다.

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전기방전소결에 의해 제조된 다공성 Titanium 임플란트의 기계적 특성 (Mechanical Properties of Electro-Discharge-Sintered Porous Titanium Implants)

  • 현창용;허재근;이원희
    • 한국재료학회지
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    • 제16권3호
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    • pp.173-177
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    • 2006
  • Porous surfaced Ti implant compacts were fabricated by electro-discharging-sintering (EDS) of atomized spherical Ti powders. Powders of $50-100{\mu}m$ in diameter were vibratarily settled into a quarts tube and subject to a high voltage and high density current pulse in Ar atmosphere. Single pulse of 0.7 to 2.0 kJ/0.7 gpowder, from 150, 300, and $450{\mu}F$ capacitors was applied in less than $400{\mu}sec$ to produce twelve different porous-surfaced Ti implant compacts. The solid core formed in the center of the compact shows similar microstructure of cp Ti which was annealed and quenched in water. Hardness value at the solid core was much higher than that at the particle interface and particles in the porous layer, which can be attributed to both heat treatment and work hardening effects induced by EDS. Compression tests were made to evaluate the mechanical properties of the EDS compacts. The compressive yield strength was in a range of 12 to 304MPa which significantly depends on input energy. Selected porous-surfaced Ti-6Al-4V dental implant compacts with a solid core have much higher compressive strengths compared to the human teeth and sintered Ti dental implants fabricated by conventional sintering process.

인천국제공항 공항전력정보시스템 설계 (Airport Power Information System Design in the Inchon Inta'l Airport)

  • 오영달;민성준;임정규;문정호;이태식;윤태혁;김문호;문영현
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1998년도 하계학술대회 논문집 C
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    • pp.1121-1124
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    • 1998
  • Inchon International Airport(IIA) is constructed for Northeast Asia Gate as is important for IIA to become a 21 century's leader in the world, as is planned for open at december 2000 as a important economic link for unified korea. Airport Power Information System(APIS) is designed through investigation of advanced domestic and international example. In addition to power facility operation it is designed for using an information infrastructure of whole airport. APIS is newly designed for uninterupted power supply, effective power management, information infrastructure's construction. making a profit by positively introduction of new technology for collection and conservation of power related data, correlation with airport infra systems, data interrelative arrangement about related systems like outdoor lighting system and automatic measuring record, CCTV systems for remote power facility monitoring, and promotion of management ability in the emergency status.

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A Strategy for Phase Identification of Precipitates in High Al-containing Austenitic and Ferritic Steels Using Electron Diffraction

  • Heo, Yoon-Uk
    • Applied Microscopy
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    • 제44권4호
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    • pp.144-149
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    • 2014
  • A strategy for phase identification of precipitates in high Al-containing austenitic and ferritic steels using electron diffraction (ED) is studied. Comparative studies of the various Al-containing precipitates (k-carbide, $Ni_3Al$, $Fe_3Al$, FeAl) show the similarities of crystal structure and lattice parameter. However, the slight differences of lattice parameter and structure display characteristic ED patterns (EDPs) which can be identified. $L1_2$ k-carbide and $Ni_3Al$ can be differentiated by the length of ${\rightarrow}_g$ (the reciprocal lattice vector), even though they show perfectly identical shapes of EDPs. $DO_3$ $Fe_3Al$ and $B_2$ FeAl show the characteristic EDs in [110] and [112] beam directions due to the differences of Fe site occupancies in unit cells. k-carbide, $Ni_3Al$, and FeAl show also the similar EDs in [112], [112], and [110] beam directions, respectively. All the possible similarities of EDs among each phases and the strategy for phase identification are discussed on the bases of kinematical ED simulation.

과학적 분석방법을 이용한 무령왕릉 목관재의 옻칠 기법 연구 (Lacquer Manufacturing Method for the Wooden Coffins of King Muryeong's Tomb based on the Scientific Analysis)

  • 김수철;이광희;강형태;신성필;한민수
    • 보존과학회지
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    • 제26권3호
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    • pp.247-258
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    • 2010
  • 무령왕릉 출토 목관재 6점의 칠도막 편에 대하여 광학 현미경 관찰, 적외선 분광분석 및 SEM-EDS 분석을 실시하였다. 목관재에 도장된 옻칠 기법은 크게 네 가지 방법으로 분류되었다. 목재 표면에 그을음(미립자의 흑색 안료)을 혼합한 흑색 안료층이 밑층으로 존재하면서 그 위로 칠이 1회(그룹 II) 도장된 것과 3회(그룹 I) 도장된 것, 흑색 안료층이 존재하지 않으면서 칠 도장이 1회(그룹 IV)와 2회(그룹 III) 되어있는 것으로 분류되었다. 이는 목관의 제작기법과 부재의 결구 방법을 밝히는데 좋은 정보가 될 것으로 생각된다. 적외선 분광분석을 통해 무령왕릉 칠도막은 자외선에 의한 열화 요인이 적은 것으로 나타났다. 이는 이동이 어려운 목관의 크기와 무덤이라는 매장 환경 등에 기인한 결과로 보인다. 또한 SEM-EDS 분석결과 현재까지 고대 칠분석에서 보고된 바 없는 Ca, Fe, Cu의 성분이 확인되어 의미가 있다.

보통의 식품첨가제의 SEM-EDS와 ICP-AES 분석 (SEM-EDS and ICP-AES Analysis of Common Food Additives)

  • Hussain, Raja Azadar;Yasmin, Farida;Nawaz, Hamid;Badshah, Amin
    • 대한화학회지
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    • 제54권5호
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    • pp.551-555
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    • 2010
  • Cinnamomum Iners (Darchini, 쟈 바 계피), Elettaria Cardamomum (Elachi, 백두구, 소두구, 카다몬, 카도몬), Punica Granatum (Anar Dana, 석류), Curcuma Longa (Haldi, 터메릭, 투메릭, 심황, 울금, 울금은, 컬쿠마), Piper Nigrum (Kali Mirch, 페퍼, 페퍼블랙, 후추, 블랙 페퍼), Syzygium aromaticum (Loung, 클로브, 정향, 정향나무,), Capsicum Annum (Laal Mirch, 붉은 고추), Mentha Arvensis (Pahari Podina, 박하), Curcuma Zedoaria (Kachur, 가쥬츠, 봉출, 아출, 커큐머 제도) Zingiber officinale (Adrak, 건강, 생강, 진저) 그리고 Garam Masala (매운맛, 혼합물)은 SEM-EDS와 ICP-AES의 도움으로 그 속의 금속 성분을 위해 본 연구에서 분석되어졌다. 작은 농도는 ICP-AES로 찾아냈고 주된 농도는 SEM-EDS로 찾아냈다.

에너지 분산형 미세열량측정에 관한 자료조사 (Survey on microcalorimetry about EDS)

  • 김종헌;박관순;오창섭
    • 에너지공학
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    • 제23권1호
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    • pp.1-6
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    • 2014
  • 본 에너지 분산 형 미세열량측정에 관한 자료는 에너지 분산 형의 우수한 조작 성을 유지하면서 파장 분산 형과 비슷한 정도의 에너지 분해능을 가질 수 있도록 개선한 것으로 광범위한 에너지의 X선을 검출을 할 수 있다. X선을 검출하기 위해서 이용되는 파장 분산 형은 에너지 분해능이 우수하지만 X선의 파장에 대해 검출 각도를 변화시켜야 하고 검출하고자 하는 특정 X선 종류에 따라 몇 가지의 검출기를 필요로 하고 있다. 그러나 에너지 분산 형의 검출기는 한 개의 검출기로 광범위한 X선을 동시에 검출할 수 있으며 조작 방법도 비교적 용이하다. 그러나 에너지 분산 형은 에너지 분해능이 우수하지 못 하고 또한 인접한 에너지를 갖는 X선은 그 피크가 중첩되어 구별하기가 어려운 경우도 있다. 에너지 분해능은 파장분산 형이 2~20 eV이고 에너지 분산 형은 140~180 eV로 상당한 차이가 있다.

Enhanced Electrochemical Properties of Surface Modified LiMn2O4 by Li-Fe Composites for Rechargeable Lithium Ion Batteries

  • Shi, Jin-Yi;Yi, Cheol-Woo;Liang, Lianhua;Kim, Keon
    • Bulletin of the Korean Chemical Society
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    • 제31권2호
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    • pp.309-314
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    • 2010
  • The surface modified $LiMn_2O_4$ materials with Li-Fe composites were prepared by a sol-gel method to improve the electrochemical performance of $LiMn_2O_4$ and were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy-energy dispersive spectroscopy (SEM-EDS), and transmission electron microscopy (TEM)-EDS. XRD results indicate that all the samples (modified and pristine samples) have cubic spinel structures, and XRD, XPS, and TEM-EDS data reveal the formation of $Li(Li_xFe_xMn_{2-2x})O_4$ solid solution on the surface of particles. For the electrochemical properties, the modified material demonstrated dramatically enhanced reversibility and stability even at elevated temperature. These improvements are attributed to the formation of the solid solution, and thus-formed solid solution phase on the surface of $LiMn_2O_4$ particle reduces the dissolution of Mn ion and suppresses the Jahn-Teller effect.

Fusiform Aneurysm Presenting with Cervical Radiculopathy in Ehlers-Danlos Syndrome

  • Kim, Ho-Sang;Choi, Chang-Hwa;Lee, Tae-Hong;Kim, Sang-Phil
    • Journal of Korean Neurosurgical Society
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    • 제48권6호
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    • pp.528-531
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    • 2010
  • Ehlers-Danlos syndrome (EDS) type IV is characterized by its clinical manifestations, which are easy bruising, thin skin with visible veins, and rupture of arteries, uterus, or intestines. Arterial complications are the leading cause of death in vascular EDS because they are unpredictable and surgical repair is difficult due to tissue fragility. The authors report a case presented with cervical radiculopathy due to a segmental fusiform aneurysm of the cervical vertebral artery. Transfemoral cerebral angiography (TFCA) was done to verify the aneurysmal dilatation. However, during TFCA, bleeding at the puncture site was not controlled, skin and underlying muscle was disrupted and profound bleeding occurred during manual compression after femoral catheter removal. Accordingly, surgical repair of the injured femoral artery was performed. At this time it was possible to diagnose it as an EDS with fusiform aneurysm on cervical vertebral artery. Particularly, cervical fusiform aneurysm is rare condition, and therefore, connective tissue disorder must be considered in such cases. If connective tissue disorder is suspected, the authors suggest that a noninvasive imaging modality, such as, high quality computed tomography angiography, be used to evaluate the vascular lesion to avoid potential arterial complications.