• Title/Summary/Keyword: Isostatic

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Mechanical and tribological characterization of $Si_{3}N_{4}-ZrO_{2}$ composites (질화규소-지르코니아 복합체의 기계적 및 내마모 특성)

  • 김성호;이수완;엄호성;정용선
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.2
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    • pp.217-223
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    • 1999
  • In this study, the effects of the content of $ZrO_{2}$ in $Si_{3}N_{4}$ on mechanical and wear properties were investigated. $Si_{3}N_{4}$ based composites containing 0~40 wt% $ZrO_{2}$ powders were fabricated using hot isostatic pressing (HIP), at $1750^{\circ}C$, 172 MPa for 1 hour in $N_{2}$ gas. Mechanical properties and wear properties of composites were examined. Mechanical properties (hardness, strength, and fracture toughness) of $Si_{3}N_{4}-ZrO_{2}$ composite were decreased with increasing the amount of $ZrO_{2}$, but relative density of composites were increased. Further, the increase in amount of $ZrO_{2}$, reduced wear rates in air. It was found that wear behaviors in air were related to microcracking.

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Effect of Hot Isostatic Pressing on the Microstructure and Properties of Kinetic Sprayed Nb Coating Material (Kinetic Spray 공정으로 제조된 Nb 코팅 소재의 미세조직 및 물성에 미치는 열간 등압 성형(HIP)의 영향)

  • Lee, Ji-Hye;Yang, Sangsun;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.23 no.1
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    • pp.15-20
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    • 2016
  • Niobium is one of the most important and rarest metals, and is used in the electronic and energy industries. However, it's extremely high melting point and oxygen affinity limits the manufacture of Nb coating materials. Here, a Nb coating material is manufactured using a kinetic spray process followed by hot isotactic pressing to improve its properties. OM (optical microscope), XRD (X-ray diffraction), SEM (scanning electron microscopy), and Vickers hardness and EPMA (electron probe micro analyzer) tests are employed to investigate the macroscopic properties of the manufactured Nb materials. The powder used to manufacture the material has angular-shaped particles with an average particle size of $23.8{\mu}m$. The porosity and hardness of the manufactured Nb material are 0.18% and 221 Hv, respectively. Additional HIP is applied to the manufactured Nb material for 4 h under an Ar atmosphere after which the porosity decreases to 0.08% and the hardness increases to 253 Hv. Phase analysis after the HIP shows the presence of only pure Nb. The study also discusses the possibility of using the manufactured Nb material as a sputtering target.

Fabrication and Tensile Properties of Alloy 617 base ODS Alloy (Alloy 617계 산화물 분산강화(ODS) 합금의 제조와 인장특성)

  • Min, Hyoung-Kee;Kang, Suk-Hoon;Kim, Tae-Kyu;Han, Chang-Hee;Kim, Do-Hyang;Jang, Jin-Sung
    • Journal of Powder Materials
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    • v.18 no.6
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    • pp.482-487
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    • 2011
  • Alloy 617, Ni-22Cr-12Co-9Mo base oxide dispersion strengthened alloy was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Uniaxial tensile tests were performed at room temperature and at $700^{\circ}C$. Compared with the conventional Alloy 617, ODS alloy showed much higher yield strength and tensile strength, but lower elongation. Fracture surfaces of the tensile tested specimens were investigated in order to find out the mechanism of fracture mode at each test temperature. Grain adjustment during tensile deformation was analyzed by electron backscattered diffraction mapping, inverse pole figures and TEM observation.

A Densification Model for Mixed Metal Powder Under Cold Compaction (냉간압축하에서 혼합 금속분말의 치밀화 모델)

  • Jo, Jang-Hyeok;Jo, Jin-Ho;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.10 s.181
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    • pp.2628-2636
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    • 2000
  • Densification behavior of mixed copper and tool steel powder under cold compaction- was investigated. By mixing the yield functions proposed by Fleck et al. and by Gurson for pure powder in terms o f volume fractions and contact numbers of Cu powder, new mixed yield functions were employed for densification of powder composites under cold compaction. The constitutive equations were implemented into a finite element program (ABAQUS) to compare with experimental data and with calculated results from the model of Kim et al. for densification of mixed powder under cold isostatic pressing and cold die compaction. Finite element calculations by using the yield functions mixed by contact numbers of Cu powder agreed better with experimental data than those by volume fractions of Cu powder.

Deformation of the Rubber Mold by Using the Cohesive Zone Model Under Cold Isostatic Pressing (응집영역모델을 이용한 정수압 성형 해석시 고무몰드의 변형거동)

  • Lee, Sung-Chul;Kim, Ki-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.5
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    • pp.387-395
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    • 2008
  • Stress distribution and interfacial debonding process at the interface between a rubber mold and a powder compact were analyzed during unloading under cold isostatic pressing. The Cap model proposed by Lee and Kim was used for densification behavior of powder based on the parameters involved in the yield function of general Cap model and volumetric strain evolution. Cohesive elements incorporating a bilinear cohesive zone model were also used to simulate interfacial debonding process. The Cap model and the cohesive zone model were implemented into a finite element program (ABAQUS). Densification behavior of powder was investigated under various interface conditions between a rubber mold and a powder compact during loading. The residual tensile stress at the interface was investigated for rubber molds with various elastic moduli under perfect bonding condition. The variations of the elastic energy density of a rubber mold and the maximum principal stress of a powder compact were calculated for several interfacial strengths at the interface during unloading.

Effect of Processing Variables on the Texture of Ni Substrate for YBCO Coated Conductor (YBCO 박막선재용 Ni 기판의 집합도에 미치는 제조공정 변수효과)

  • 지봉기;임준형;이동욱;주진호;나완수;김찬중;홍계원
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.10
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    • pp.938-945
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    • 2003
  • We fabricated Ni-substrate for YBCO coated conductors and evaluated the effects of pressing and annealing temperature and time on texture. Ni substrate was fabricated by powder metallurgy technique and compacts were prepared by applying uniaxial or isostatic pressure. The texture of substrate made by applying cold isostatic pressure (CIP) was stronger than that by uniaxial pressure which we attribute to the fact that the CIP method provided higher density and more uniform density distribution. It was observed that the substrate annealed at 400 C showed both retained texture and recrystallized texture. On the other hand, the texture of substrate significantly improved at annealing temperature above 500 C, forming strong 4-fold symmetry, [111] II ND texture, and FWHM of 9∼10 . It is to be noted that the degree of texture was almost independent of annealing temperature (500∼1000 C) and annealing time(1∼54 min, at 1000 C). EBSD and AFM analysis indicated that 99% of grain boundaries was low angle grain boundary and RMS was approximately 3 nm, respectively. Development of strong cube texture and high fraction of low angle grain boundary of Ni-substrate made by powder metallurgy technique in our study is considered to be suitable for the application of YBCO coated conductors.

Microstructures of Hot Isostatic Pressed High Speed Steels (히핑처리된 분말 고속도공구강의 미세조직에 관한 연구)

  • 이언식
    • Journal of Powder Materials
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    • v.4 no.1
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    • pp.18-25
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    • 1997
  • High speed steels with commercial compositions of 10V, Rex20, Rex25, T15, and ASP30 were gas-atomized and then consolidated by hot isostatic pressing (HIPping). The microstructures of gas-atomized powder, as-HiPped billet, and heat-treated billet have been characterized using optical microscope, scanning electron microscope and X-ray diffractometer. In the gas-atomized powders, the solidification structures of 10V and Rex25 alloys show that primary MC carbides embedded within the fine equiaxed dendrites, whereas those of Rex20, T15 and ASP30 alloys exhibited eutectic MC and/or M$_2$C carbides in the interdendritic region. The trace and dendritic morphologies of gas-atomized powder have been retained in as-HiPped billets. The microstructures of as-HiPped billets have been observed to consist of ferrite, $M_6C$ and MC carbides in other alloys with the exception of 10V alloy, which consists of ferrite and MC carbides. The hardness of heat-treated billet makes a favorable comparison with that of as-HIPped billet. This seems mainly to be due to the strengthening by the precipitation of secondary carbides and the change of matrix phase from $\alpha$-ferrite to martensite.

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Temperature Variations in the Mixed Layer with the Passage of Typhoons Using One-Dimensional Numerical Model (1차원 모델상에서 태풍통과시의 혼합층 수온 변화)

  • Hong, Chul-Hoon;Masuda, Akira
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.51 no.1
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    • pp.107-112
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    • 2018
  • One-dimensional numerical model is implemented to investigate temperature variations in the mixed layer depth (MLD) with the passage of typhoons. In the model, we assume a non-divergent, infinite ocean and consider wind effects only, excluding isostatic effects (inverse barometric effects) and upwelling with vertical movement of the water column. Numerical experiments investigate the effects of typhoon tracks on temperature variations, including their dependence on vertical resolutions in the MLD and these results are compared with those in a three-dimensional primitive equation model (POM). The model reproduces features of the observed temperature variations in the MLD fairly well, and implies that wind effects, rather than isostatic effects, play a predominant role in temporal and spatial temperature variations in the MLD. After the passage of typhoons, however, the model does not reproduce well the temperature variations observed in the MLD, because a limitation of the model is its inability to reproduce events such as cyclonic eddy formation (Hong et al., 2011; Masuda and Hong, 2011). The model also shows well the so called 'rightward bias' (Price, 1981) of sea surface cooling which is the most predominant in the right hand side of typhoon's track.

Development of textured Ni substrate for YBCO coated conductor (YBCO박막선재용 Ni 기판의 집합도 분석)

  • 지봉기;김규태;임준형;이동욱;주진호;나완수;김찬중;홍계원
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.02a
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    • pp.68-71
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    • 2003
  • We fabricated Ni-substrate for YBCO coated conductors and evaluated the effects of pressing and annealing time on texture. Ni substrate was fabricated by powder metallurgy technique and compacts were prepared by applying uniaxial or isostatic pressure. The texture of substrate made by applying cold isostatic pressure (CIP) was stronger than that by uniaxial pressure. The texture of substrate made by CIP had a strong 4-fold symmetry and [111] ∥ ND texture after annealing temperature of 100$0^{\circ}C$. It is to be noted that the degree of texture was almost independent of annealing time and the full-width at half-maximum (FWHM) of in-plane and out-of-plane was measured to be in the range of 9.55$^{\circ}$-10.53$^{\circ}$ and 8.57$^{\circ}$-9.85$^{\circ}$, respectively. Development of strong cube texture of Ni-substrate made by powder metallurgy technique in our study is considered to be suitable for the application of YBCO coated conductors.

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