• Title/Summary/Keyword: Isostatic

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Large area imprint process using isostatic pressure

  • Lee, Sang-Mun;Mun, Jin-Seok;Gwak, Jeong-Bok;Na, Seung-Hyeon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.209-209
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    • 2007
  • Ni stamper위에 100nm의 Si 코팅후 자기조립 단분자막(SAM)을 액상 코팅방식으로 형성 하였고, 내구성 및 열적 안정성을 검증하기 위해 반복적인 이형 및 압력인가 test가 실시하였다. 20회 이상의 이형실험을 통해 열적, 기계적 안정성을 확인하고, 접촉각 측정을 통해 이형특성의 안정성도 고찰하였다. 이를 Imprint공법을 적용 fine pattern의 구조물을 얻을 수 있었다. SAM코팅은 TRICHLOROSILANE을 사용하였으며 Hexane과 1000:1의 비율로 섞어서 stirrer에서 mixing하는 방식을 사용했으며, UV-ozone처리를 통한 이형성 제거 효과도 관찰하였다.

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Fabrication of SiCN structures using PDMS mold for high-temperature applications (PDMS 몰드를 이용한 초고온용 SiCN 구조물의 제작)

  • Woo, Hyung-Soon;Kim, Gue-Hyun;Chung, Gwiy-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.376-379
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    • 2003
  • In this paper, a novel processing technique for fabrication of high-temperature MEMS based on polymer-derived SiCN microstructures is described. PDMS molds are fabricated on SU-8 photoresist using standard UV-photolithographic processes. Liquid precursors are injected into the PDMS mold. And then, the resulting solid polymer structures are crosslinked under isostatic pressure, and pyrolyzed to form a ceramic capable of withstanding over $1500^{\circ}C$. These fabricated SiCN structures would be applied for high-temperature applications, such as heat exchanger and combustion chamber.

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MICROSTRUCTURAL OBSERVATION AND TENSILE ISOTROPY OF AN AUSTENITIC ODS STEEL

  • Kim, Tae-Kyu;Bae, Chang-Soo;Kim, Do-Hyang;Jang, Jin-Sung;Kim, Sung-Ho;Lee, Chan-Bock;Hahn, Do-Hee
    • Nuclear Engineering and Technology
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    • v.40 no.4
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    • pp.305-310
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    • 2008
  • Based on a composition of 99.4 wt% AISI 316L stainless steel, 0.3wt% Ti and 0.3 wt% $Y_2O_3$, an austenitic ODS steel was fabricated by a process of mechanical alloying, hot isostatic pressing and rolling. Fine oxide particles were observed in the matrix, and their chemical formulations were determined to be $Y_2Si_2O_7$ and TiO. Heat treatment of the cold-rolled sample at $1200^{\circ}C$ induced an isotropic tensile behavior at room temperature and at $700^{\circ}C$. This result would be mainly attributed to the equiaxed grains that form as a result of the heat treatment for recrystallization.

Evaluation and Comparison of the Topographic Effect Determination Using Korean Digital Elevation Model (우리나라 수치표고모델을 이용한 지형효과 산출방식의 비교평가)

  • Lee, Suk-Bae;Lee, Dong-Ha;Kwon, Jay-Hyun
    • Journal of Korean Society for Geospatial Information Science
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    • v.16 no.1
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    • pp.83-93
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    • 2008
  • The topographic effect is one of the most important component in the solution of the geodetic boundary value problem (geodetic BVP). Therefore, topographic effect should be considered properly for developing the precise geoid model, especially for the area where contains many mountains like Korea. The selection of gravity reduction method in the context of the precise geoid determination depends on the magnitude of its indirect effect, the smoothness and magnitude of the reduced gravity anomalies, and their related geophysical interpretation. In this study, Korean digital elevation model with 100m resolution was constructed and topographic effect was calculated by three reduction methods as like Helmert condensation method and RTM method and Airy-isostatic reduction method. Through the analysis of computation results, we can find that RTM reduction method is the best optimal method and the results shows that gravity anomaly and indirect effect of geoidal height are $0.660{\pm}13.009mGal$, $-0.004{\pm}0.131m$ respectively and it is the most gentle slow of the three methods. Through this study, it was found that the RTM method is better suitable for calculating topographic effect precisely in context of precise geoid determination in Korea than other reduction methods.

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Evaluation of the Microstructure and Mechanical Properties for Ni Superalloy Materials Using HIP and Post Heat Treatment (HIP과 열처리공정을 이용한 Ni기 초합금 소재의 미세조직 및 기계적 특성 분석)

  • Kim, Youngdae;Hyun, Jungseob;Chang, Sungyong
    • KEPCO Journal on Electric Power and Energy
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    • v.6 no.2
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    • pp.137-143
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    • 2020
  • The CM247LC, a Ni-based superalloy material used for gas turbine hot gas path parts, is casted using directionally solidified technology to analyze the mechanical properties and microstructures through HIP (Hot Isostatic Pressing) and post-heat treatment, and to derive optimal HIP treatment conditions. The CM247LC material is being researched in various ways as an alternative material for prototyping gas turbine blades. In particular, the blade rotating part is exposed and operated in a high temperature and high-pressure environment, and when damaged, it may cause huge economic losses. Therefore, in order to use the CM247LC material as prototyping materials for gas turbine blades, the reliability of the microstructure and mechanical properties must be verified. In this study, after casting rod test specimens using CM247LC material by directionally solidified technology, after that the specimens were performed by HIP treatment and post-heat treatment to test two HIP conditions designed by KEPCO to derive the possibility of prototyping of CM247LC material and optimization of HIP treatment conditions. Additionally, the properties of CM247LC material were compared to the GTD111DS material using for 1,300℃ class gas turbine blades.

A Study on the Manufacturing Characteristics and Field Applicability of Engineering-scale Bentonite Buffer Block in a High-level Nuclear Waste Repository (고준위폐기물처분장 내 공학규모의 균질 완충재 블록 성형특성 및 현장적용성 분석)

  • Kim, Jin-Seop;Yoon, Seok;Cho, Won-Jin;Choi, Young-Chul;Kim, Geon-Young
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.16 no.1
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    • pp.123-136
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    • 2018
  • The objective of this study is to propose a new methodology to fabricate a reliable engineering-scale buffer block, which shows homogeneous and uniform distribution in buffer block density, for in-situ experiments. In this study, for the first time in Korea, floating die press and CIP (Cold Isostatic Press) are applied for the manufacture of an engineering-scale bentonite buffer. The optimized condition and field applicability are also evaluated with respect to the method of manufacturing the buffer blocks. It is found that the standard deviation of the densities obtained decreases noticeably and that the average dry density increases slightly. In addition, buffer size is reduced by about 5% at the same time. Through the test production, it is indicated that the stress release phenomenon decreases after the application of the CIP method, which leads to a reduction in crack generation on the surface of the buffer blocks over time. Therefore, it is confirmed that the production of homogeneous buffer blocks on industrial scale is possible using the method suggested in this study, and that the produced blocks also meet the design conditions for dry density of buffer blocks in the AKRS (Advanced Korea Reference Disposal System of HLW).

Digital Gravity Anomaly Map of KIGAM (한국지질자원연구원 디지털 중력 이상도)

  • Lim, Mutaek;Shin, Younghong;Park, Yeong-Sue;Rim, Hyoungrea;Ko, In Se;Park, Changseok
    • Geophysics and Geophysical Exploration
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    • v.22 no.1
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    • pp.37-43
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    • 2019
  • We present gravity anomaly maps based on KIGAM's gravity data measured from 2000 to 2018. Until 2016, we acquired gravity data on about 6,400 points for the purpose of regional mapping covering the whole country with data density of at least one point per $4km{\times}4km$ for reducing the time of the data acquisition. In addition, we have performed local gravity surveys for the purpose of mining development in and around the NMC Moland Mine at Jecheon in 2013 and in the Taebaeksan mineralized zone from 2015 to 2018 with data interval of several hundred meters to 2 km. Meanwhile, we carried out precise gravity explorations with data interval of about 250 m on and around epicenter areas of Gyeongju and Pohang earthquakes of relatively large magnitude which occurred in 2016 and in 2017, respectively. Thus we acquired in total about 9,600 points data as the result. We also used additional data acquired by Pusan National University for some local areas. Finally, gravity data more than 16,000 points except for the repetition and temporal control points were available to calculate free-air, Bouguer, and isostatic gravity anomalies. Therefore, the presented anomaly maps are most advanced in spatial distribution and the number of used data so far in Korea.

Development of Hybrid Geoid using the Various Gravimetric Reduction Methods in Korea (다양한 중력학적 환산방법을 적용한 한국의 합성지오이드 개발)

  • Lee, Dong-Ha;Lee, Suk-Bae;Kwon, Jae Hyoun;Yun, Hong-Sic
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.5D
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    • pp.741-747
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    • 2008
  • Nowadays, the accuracy of the geoid model has been improved through development of the combination model which was composed of traditional gravimetric geoid and geometric geoid by the GPS/leveling data in USA and Japan. It is a state of the art method in geoid modeling field that what so called hybrid geoid. In this paper, as a basic study to develop Korean hybrid geoid model, we studied gravimetric geoid solutions using three gravity reduction methods (Helmert's condensation method, RTM method and Airy-isostatic method) and evaluated the usefulness of each method in context of precise geoid. The gravimetric geoid model were determined by restoring the gravity anomalies (included TC) and the indirect effects were made from various reduction methods on the EIGEN-CG03C reference field. The results are compared with respect to the geometric geoid undulation determined from 498 GPS/leveling after LSC fitting. The results showed that hybrid geoid with RTM (Residual terrain model) reduction method was most accurate method and the value of the difference compared to geometric geoid was $0.001{\pm}0.053m$.

Microstructure Evolution of 15Cr ODS Steel by a Simple Torsion Test (단순 전단변형에 의한 15Cr 산화물 분산강화 강의 미세조직 변화)

  • Jin, Hyun Ju;Kang, Suk Hoon;Kim, Tae Kyu
    • Journal of Powder Materials
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    • v.21 no.4
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    • pp.271-276
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    • 2014
  • 15Cr-1Mo base oxide dispersion strengthened (ODS) steel which is considered to be as a promising candidate for high- temperature components in nuclear fusion and fission systems because of its excellent high temperature strength, corrosion and radiation resistance was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Torsion tests were performed at room temperature, leading to two different shear strain routes in the forward and reverse directions. In this study, microstructure evolution of the ODS steel during simple shearing was investigated. Fine grained microstructure and a cell structure of dislocation with low angle boundaries were characterized with shear strain in the shear deformed region by electron backscattered diffraction (EBSD). Grain refinement with shear strain resulted in an increase in hardness. After the forward-reverse torsion, the hardness value was measured to be higher than that of the forward torsion only with an identical shear strain amount, suggesting that new dislocation cell structures inside the grain were generated, thus resulting in a larger strengthening of the steel.

Effect of Sintering Temperature on the Tensile Properties of Powder Injection Molded PH 17-4 STS (분말사출성형을 통해 제조된 PH 17-4 STS 강의 소결온도에 따른 인장 특성)

  • Sung H. J.;Ha T. K.;Ahn S.;Chang Y. W.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2001.10a
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    • pp.305-308
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    • 2001
  • Powder injection molding (PIM) uses the shaping advantage of injection molding but is applicable to metals and ceramics. This process combines a small quantity of polymer with an inorganic powder to form a feedstock that can be molded. After shaping, the polymeric binder is extracted and the powder is sintered often to near-theoretical densities. Accordingly, PIM delivers structural materials in a shaping technology previously restricted to polymers. The process overcomes the shape limitations of traditional powder compaction, the costs of machining, the productivity limits of isostatic pressing and slip casting, and the defect and tolerance limitations of casting. The 17-4 PH stainless steel powders with average diameter of $10{\mu}m$ were injection-molded into flat tensile specimens. Sintering of the compacts was carried out at the various temperatures ranging from 900 to $1350^{\circ}C$. Sintering behavior of the compacts and tensile properties of sintered specimens were investigated.

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