• Title/Summary/Keyword: Iron sample

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Measurement of Effective Linewidth for Ca-Zr Substituted YIG (Ca-Zr치환 YIG의 유효 선폭 측정)

  • 김약연;한진우;한기평;김덕준;이상석;최태구
    • Journal of the Korean Magnetics Society
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    • v.10 no.1
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    • pp.22-29
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    • 2000
  • The effective linewidth was measured using the conventional cavity perturbation method at 9.43 GHz in room temperature for Ca-Zr substituted yttrium iron garnet plate. The experimental set-up consists of the network analyzer, the electromagnet and the cylimdrical TE001 cavity. Measurement was performed in the static magnetic field perpendicular to the sample plane. The real and imaginary parts of diagonal component of the microwave susceptibility tensor are obtained from the resonance frequency and the quality factor Q of the cavity. Variations of the effective linewidth was qualitatively explained with the spin wave scattering theory.

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Study on The Measurement of Corrosion Product Concentration in The Feed Water System of A Power Plant (발전소 급수계통 부식생성물 농도 측정에 관한 연구)

  • Moon, Jeon Soo;Lee, Jae Kun
    • Corrosion Science and Technology
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    • v.10 no.4
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    • pp.151-155
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    • 2011
  • The iron oxide particles could be resulted from the corrosion of the circulating water system of a power plant. Because it may be one of the trouble materials which affect the power generation efficiency due to the deposition on steam generator tube and turbine blade, the continuous observation of its concentration is very important. The laser induced break-down detection (LIBD) technology was applied to monitor continuously the concentration of corrosion products with the detection limit of ppb level. The measurement system consists of a Nd:YAG pulsed laser, a polarizing beam splitter, a flow-type sample cell, an acoustic emission sensor, a high speed data acquisition board, a personal computer, etc.. The performance test results confirmed that this technology can be effective to monitor the corrosion product concentration of the circulating water system of a power plant.

Mössbauer Study of Two Discernable Fe Sites in CaFe2O4

  • Yoon, Sung-Hyun
    • Journal of Magnetics
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    • v.14 no.2
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    • pp.86-89
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    • 2009
  • Structural and magnetic properties of polycrystalline $CaFe_2O_4$ prepared by the solid state reaction method were studied using powder X-ray diffraction (XRD) and $M{\ddot{o}}ssbauer$ spectroscopy. The structure of $CaFe_2O_4$ belongs to an orthorhombic system (space group: Pnma) with the lattice parameters $a=9.2373\;{\AA}$, $b=3.0237\;{\AA}$, and $c=10.7124\;{\AA}$. Results of structural refinement indicate, however, that there are two slightly different iron sites in the sample. The $M{\ddot{o}}ssbauer$ spectrum at 4.2 K shows a hyperfine sextet with a hyperfine magnetic field and an isomer shift of 47.3 T and 0.36 mm/s, respectively. An examination of the spectrum revealed that the line widths of the spectral lines were not uniform. The degree of asymmetric line broadening decreases with increasing temperature, suggesting that the difference in the degree of crystalline distortions between two $FeO_6$ octahedra is eliminated as the temperature rises.

Development of Functional Milk and Dairy Products by Nanotechnology (나노 기술을 이용한 기능성 우유 및 유제품의 개발 연구)

  • Gwak, Hae-Su
    • Journal of Dairy Science and Biotechnology
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    • v.23 no.1
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    • pp.27-37
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    • 2005
  • The development of functional foods started booming from several years ago in the world. The size of functional materials are in the range of micrometer level. This size can be much smaller into nanometer level to be more effective. We face some problems from the materials, such as flavor, taste, color, viscosity, etc. in functional materials. The problems can be solved by micro / nanoencapsulation technique. This paper showed some results of the research related on the technique for functional milks and dairy products. The nono / microcapsules are the form of liquid instead of solid. Coating materials used were fatty acid esters, and core materials were lactase, iron, ascorbic acid. isoflavone, and chitooligosaccharide. The ranges of capsules are from 100 nm to 200 ${\mu}$m. The sample milks added nano/microcapsules were homogeneous and prevented the defects of core materials. It was observed that nano / microcapsules in milk and dairy products were effective as functional material without defaults. It was indicated that targeted functional foods can be developed further in various foods by nanotechnology.

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Round-robin Test on AC Losses in a Technical High-Tc Superconducting Tape (실용고온초전도테이프의 교류손실에 대한 Round-robin테스트)

  • 류경우;최병주;황시돌
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.53 no.7
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    • pp.437-443
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    • 2004
  • In this work the AC loss measurement setup based on an iron core background magnet, not used in a conventional one, has been successfully developed. To prove its validity, a round-robin test for the same Bi-2223 tape sample among three institutes has been done. The results show that the self-field and magnetization losses from the developed setup well agree with the losses measured at two other institutes of Korea Basic Science Institute and Yokohama National University. The measured magnetization losses for parallel or perpendicular fields can be well predicted from the slab model or the strip model for a filamentary region. However the magnetization losses for longitudinal fields can be rather predicted by the slab model for a decoupled filament. The self-field losses are well explained by the Norris ellipse model.

A research of Cheju Island plain coarse pottery and pantiles magnetism characteristic

  • Yoon, Tae-Gun;Park, Won-Jun;Ko, Jeong-Dae;Hong, Sung-Rak
    • Proceedings of the Korean Magnestics Society Conference
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    • 2000.09a
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    • pp.413-420
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    • 2000
  • Cheju Island has nature of typical trass through volcanic activities in many times. The soil in Cheju Island has principally sprung from basalt and partially made up of trachyte, trachyte's nature and site. Also ancient relics, plain coarse pottery's kilns and pantiles kilns are homogeneously distributed all over the Cheju Island. In this study, as a result of X-ray fluorescence spectrometer and Mossbauer spectroscopy of a sample are from plain coarse pottery and pantiles in 5 regions of Cheju Island. It is thought that these samples are partially formed from neutral volcanic rock like trachyte and Atomicity state of iron is almost Fe$\^$3+/. Also the magnetic hyperfine field length of goethite, contained these samples is less than synthetic goethite magnetic hyperfine field length and this result shows that disintegration of inner magnetic order, created by partial substitution of diamagnetic positive ion containing Fe$\^$3+/ and Al$\^$3+/ in goethite lattice.

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Green Body Behaviour of High Velocity Pressed Metal Powder

  • Jonsen, P.;Haggblad, H.A.;Troive, L.;Furuberg, J.;Allroth, S.;Skoglund, P.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.22-23
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    • 2006
  • High velocity compaction (HVC) is a production technique with capacity to significantly improve the mechanical properties of powder metallurgy (PM) parts. Investigated here are green body data such as density, tensile strength, radial springback, ejection force and surface flatness. Comparisons are performed with conventional compaction using the same pressing conditions. Cylindrical samples of a pre-alloyed water atomized iron powder are used in this experimental investigation. The HVC process in this study resulted in a better compressibility curve and lower ejection force compared to conventional quasi static pressing. Vertical scanning interferometry measurements show that the HVC process gives flatter sample surfaces.

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The Determination of Dissolved Total Fe by Flow Injection Analysis in Environmental Samples

  • Kim, Do Hoon;Takeda, Kazuhiko;Sakugawa, Hiroshi;Lee, Jin Sik
    • Analytical Science and Technology
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    • v.14 no.6
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    • pp.510-515
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    • 2001
  • There has been an increasing need for analytical methods of dissolved total iron (tFe) that are highly sensitive, rapid, inexpensive and simple for environmental samples. A sensitive flow injection analysis (FIA) method for determining the concentration of tFe in environmental samples was developed. The proposed method required 10 minutes and only $500{\mu}L$ of sample for and analysis. The standard deviation was 5.0% at $0.5{\mu}gL^{-1}$ (n=6), and the detection limit was $0.075{\mu}gL^{-1}$. The developed method was applied to environmental samples such as tap water, mineral water, rain, snow and cloud water. Since this FIA system was free form interferences of coexisting ions commonly found in samples, sub-${\mu}gL^{-1}$ level of tFe could be easily determined without further preconcentration and separation.

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Origin of Spherule Samples Recovered from Antarctic Ice Sheet-Terrestrial or Extraterrestrial?

  • Sekimoto, Shun;Kobayashi, Takayuki;Takamiya, Koichi;Ebihara, Mitsuru;Shibata, Seiichi
    • Nuclear Engineering and Technology
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    • v.48 no.2
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    • pp.293-298
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    • 2016
  • Thirty-eight spherules from the Antarctic ice sheet were analyzed using neutron activation analysis under two different conditions to investigate their origin. In almost all of these spherules, the contents of iron, cobalt, and manganese were determined to be 31% to 88%, 17 mg/kg to 810 mg/kg, and 0.017% to 7%, respectively. A detectable iridium content of 0.84 mg/kg was found in only one spherule, which was judged to be extraterrestrial in origin. A comparison of elemental compositions of the Antarctic spherules analyzed in this study with those of deep-sea sediment spherules and those of terrestrial materials revealed that most of the Antarctic spherules except for the sample in which iridium was detected could not be identified as extraterrestrial in origin.

Study on the Re-corrosion Characteristics of Corrosion Products by Weeping of Iron Artifacts (철제유물 Weeping에 따른 부식화합물의 재부식 특성 연구)

  • Park, Hyung-Ho;Lee, Hye-Youn;Lee, Jae-Sung;Yu, Jae-Eun
    • Journal of Conservation Science
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    • v.29 no.3
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    • pp.287-296
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    • 2013
  • Excavated iron objects are preserved in stable condition through processes of conservation treatment because they are found in the form of various corrosion products. However, the conservation treatment leads to re-corrosion over time and accordingly, iron objects can be severely damaged, and therefore fundamental measures need to be prepared to control it. In this study, the types and characteristics of corrosion products were scientifically analyzed according to the re-corrosion of iron artifacts. In addition, the stability of the corrosion products was evaluated by exposing the standard samples under the re-corrosion environment. Re-corrosion proceeded with weeping in reddish brown on the cracks of iron artifacts. Weeping was detected akagan$\acute{e}$ite had a low hydrogen ion concentration and high chloride ion. The selection of standard sample goethite, lepidocrocite, hematite, and magnetite, were evaluated corrosive by weeping. After the samples were immersed in HCl(pH 1), $H_2SO_4$(pH 1), $H_2O$(pH 6) solution, they had been maintained for 180 days in relative humidity of 20%, 50%, 80% to investiage the changes of chemical components. As a result of analysis, the changes of chemical components were not showed in goethite, lepidocrocite, and hematite. But magnetite was changed to lepidocrocite in solution including chloride ion($Cl^-$) and to goethite and lepidocrocite solution including sulfuric acid($SO{_4}^{2-}$). Results of the study, in the case of magnetite known as s stable corrosion compound, it was identified the corrosion of magnetite occurs by corrosive ions, which means weeping generated in the iron artifacts can corrode magnetite as well as base metal.