• Journal of the Korean Ceramic Society
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• v.31 no.8
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• pp.849-860
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• 1994

The microstructural evolution and crystalline phases of this infiltration of Ti+Al liquids in TiC, SiC, TiC+C, and SiC+C preforms have been investigated. As the Ti and Al mixing ratio in Ti+Al infiltrated liquid changes, the newly formed reaction products, which were reacted from the Ti+Al liquid with preforms, consisted of three major phases as Ti3AlC, Al2Ti4C2 or Al4C3. The TiC grain shape was changed to spheroid, when Ti3AlC was formed. In case of Al2Ti4C2 formation, the platelet grain was formed from the original TiC grain. When Al4C3 was formed, nodular or intergranular fine-grained Al4C3 was formed around the TiC grain, while the original TiC grain shape was not changed.

• Journal of the Korean Ceramic Society
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• v.22 no.2
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• pp.11-16
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• 1985

The semiconducting ceramics having positive temperature coefficient of resistivity in he family of 0.25mol% $Sb_2O_3$ doped barium titanates were prepared with AST ($4Al_2O_3$.$9SiO_2$.$3TiO_2$) and $MnO_2$ as additives and these electrical properties were investigated. The PTCR characteristic in these ceramic materials was improved by the addition of AST and $MnO_2$ because the addition of AST decreased the room temperature resistivity and controlled grin size due to the formation of a liquid phase during sintering and the addition of $MnO_2$ improved by forming acceptor level on the intergranular layer. On dependence on the switching time as switching temperature was increased the initial power and switching time increased.

• Journal of Ocean Engineering and Technology
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• v.9 no.2
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• pp.98-111
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• 1995

High temperature low cycle fatigue shows that cycle-dependent crack growth owing to cyclic plastic deformation occurred simultaneosly with time-dependent crack growth owing to intergranular deformation. Consequently, to estimate crack growth rate uniquely, many to investigators have proposed various kinds of parameters and theories but these could not produce satisfactory results. Therefore the goal of this study is focused on prediction of crack growth rate using predominant damage rule, linear cumulative damage rule and transitional parameter ${\Delta}J_c/{\Delta}J_f$. On the basis of these sinusoidal loading waveform at 600$^{\circ}C$ and 700$^{\circ}C$.

• The Korean Journal of Ceramics
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• v.1 no.1
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• pp.45-54
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• 1995

Four kinds of silicon nitride based ceramic materials have been hot pressed. Effect of the sintering additives on the phase transformation, microstructural development and mechanical properties was investigated. While sintering under the same condition a big difference among the microstructures of the specimens, they appeared alike if sintered to have a similiar $\alpha$-$\beta$ phase ratio. The specimen of the stoichiometric $\alpha$-$\beta$ sialon composition showed very limited amount of the intergranular glassy phase and a significant degree of the residual stress. It exhibited almost no strength degradation up to $1300^{\circ}C$, and the strength of the specimen degraded more as its composition deviated from the stoichiometry.

• Journal of the Korean Ceramic Society
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• v.32 no.4
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• pp.471-481
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• 1995

Unirradiated UO2 pellets were pulverized by oxidation in air at 40$0^{\circ}C$, and the oxidized powders were reduced in H2 and CO atmospheres at $600^{\circ}C$. During the oxidation of UO2 at 40$0^{\circ}C$, intergranular cracks which caused the spallation were mainly developed by the volume contraction due to the formation of intermediate phase (U4O9 or U3O7). As oxidation proceeded, U3O8 finally formed. As the oxidation/reduction cycles were repeated, the powder surface became coarser, specific surface area was increased and average particle size was decreased. The sintered densities of the powder were increased by the oxidation/reduction cycle due to the characteristic changes of the powder.

• Transactions of the Korean Society of Mechanical Engineers
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• v.5 no.2
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• pp.110-121
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• 1981

In order to study on the fracture behavior and the fracture thoughness of combined structure, the specimens, structural steel (SM28C) and 6:4 brass are annealed for ductility and investigated for the befavior of fracture and the absorbed energy at the variation of the impact velocity. The results obtained by this study are as follows: (1)The maximum load increases with the impact velocity, but in the condition of constant impact velocity it decreases as the ductility increases. (2)The absorbed energy increases with the impact velocity, but in the condition of constant impact velocity it is constant as the ductility increases. (3)In the case of the combined structure of peralite and ferrite, the microcracks initiates and propagates mainly in the ferrite structure intergranular in accompany with the slip, and the slip concentration phenomena occur in the boundary of pearlite structure However, in case of the combined structure of .alpha. and ..betha. phase, the microcracks initiates and propagares mainly in the .alpha. phase intergranularly, and slip concentration phenomena not ocur in the boundary of .betha. phase.

• Journal of the Korean Society for Heat Treatment
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• v.6 no.2
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• pp.79-88
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• 1993

The static creep mechanism and behaviour of Al-Zn-Mg alloy have been investigated under condition of constant stress tension creep test in the temperature and stress range of $170-260^{\circ}C$ and 5-12.5 $kg/mm^2$ respectively. The experimental result are follows : The stress exponent value for creep was observed to about 7.3-6.43 and the activation energy for creep deformation was 44-41 kcal/mol. Larson-Miller parameter P for the crept specimens under the creep condition was obtained as P = (T + 460) (log $t_r$ + 8.6). Emperical equation for the creep rate was obtained by the computer simulation as follows. $${\varepsilon}\;=\;\exp[(-5.519{\times}10^{-4}{\sigma}+2.33{\times}10^{-2})T-6.98{\sigma}+18.295]{\times}{\sigma}^{-0.0142+10.18}\exp[\frac{(-6{\sigma}+47.8)1000}{RT}]$$ Fracture was dominated by intergranular mechanism over the experimental range.

• Tribology and Lubricants
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• v.16 no.6
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• pp.477-483
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• 2000

Rolling contact fatigue (RCF) tests were performed for two kinds of commercial silicon nitride balls using 4-Ball rolling contact fatigue life tester under EHL condition (Λ=8.9) and boundary lubrication condition (Λ=0.2). All the test balls were finished up to the dimensional accuracy of Grade 5 defined in KS B 2001 (Steel Balls for Ball Bearings) with a size of 8.731 mm. RCF tests were then conducted under the initial theoretical maximum contact stress 6.63 GPa and the spindle speed 10,000 rpm. All the test balls were not failed until 3.75 $\times$ 107 contact cycles and wear tracks of test balls were not conspicuous under EHL condition (Λ= 8.9). In the operations of low lambda regime (Λ= 0.2), all the test balls were surface damaged and high rolling wear resistance was achievable in fully densified using MgO 1 wt% and HIPed balls. Rolling wear of silicon nitride balls under boundary lubrication condition depend mainly on grain size and intergranular phase content of silicon nitride balls.

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.66-71
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• 1998

A study of treatment effects on laser surface melted Ni-base alloy 600, especially on precipitation behavior ad chemical composition changes on the grain boundary were conducted with microscopic equipments. Long-term aging treatment at 40$0^{\circ}C$ caused no considerable effects on the grain boundary properties. Cr-rich M$_2$$_3$C$_{6}$ and Cr$_{7}$C$_3$ carbides were precipitated and the resultant Cr depletion below 12 wt pct on some high angle grain boundaries was occurred by heat treatment at $600^{\circ}C$ for 24 hours. These results can imply that the resistance of intergranular stress corrosion cracking of heat treated alloy 600 might not be changed considerably in comparion with the as-LSM one.e.e.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1997.04a
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• pp.143-149
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• 1997

the horizontal corrosion fatigue tester has been developed for investigating environmental strength. Using this tester, we investigated about corrosion fatigue caracteristic for A106 GrB steel weldments in 3.5% synthetic seawater and room temperature. Considered parameter is only frequency of 1,3 and 5Hz. and Corrosion fatigue crack length was measured by DC potential difference method. From the results, we could find that the horizontal corrosion fatiued tester could be well applied to estimation of fatigue strength. and In case of 5Hz, corrosion fatigue crack growth path of A106 GrB steel weldment was transgranular, and of 1 and 3Hz showed that transgranular and intergranular was mixed. Also, Corrosion fatigue crack growth caracteristic values estimated in each frequency were C=9.33 x 10-9 and m=2.93 in 1Hz, C=9.77x10-10 and m=3.47 in 3Hz, C=1.02x10-10 and m=4.05 in 1Hz