• Title/Summary/Keyword: Interfacial Layer

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Patterning Barrier Ribs of PDP by Transparent Soft Mold

  • Paek, Sin-Hye;Choi, Hyung-Suk;Park, Lee-Soon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2002.08a
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    • pp.639-642
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    • 2002
  • A new PDP barrier rib formation technique was investigated utilizing transparent soft maid made of silicon resin. Transparent soft mold was fabricated by pouring a silicone resin into the base mold made with photosensitive glass. The photosensitive barrier rib paste was coated on the glass substrate and dried in a 90 $^{\circ}C$ convection oven for 20min. The transparent soft mold was pressed on top of the semi-dry barrier rib layer and then irradiated with a UV lamp to a total dose of $900{\sim}1000mJ/cm^2$ The soft maid was then removed from the pressed barrier rib by winding up and fine pattern of barrier rib was obtained. The photosensitive barrier rib paste makes the demolding easy due to reduced interfacial forces and shrinking of paste materials.

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XPS Characterization and Morphology of MgO Thin Films grown on Single-Crystalline Diamond (100)

  • Lee, S.M.;Ito, T.;Murakami, H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.19-27
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    • 2003
  • Morphology and composition of MgO films grown on single-crystalline diamond (100) have been studied. MgO thin films were deposited in the substrate temperature range from room temperature (RT) to 723K by means of electron beam evaporation using MgO powder source. Atomic force microscopy images indicated that the film grown at RT without $O_2$ supply was relatively uniform and flat whereas that deposited in oxygen ambient yielded higher growth rates and rough surface morphologies. X-ray photoelectron spectroscopy analyses demonstrate that the MgO film deposited at RT without $O_2$ has the closest composition to the stoichiometric MgO, and that a thin contaminant layer composed mainly of magnesium peroxide (before etching) or hydroxide (after etching) was unintentionally formed on the film surface, respectively. These results will be discussed in relation to the interaction among the evaporated species and intentionally supplied oxygen molecules at the growth front as well as the interfacial energy between diamond and MgO.

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Chemical characteristics of mineral trioxide aggregate and its hydration reaction

  • Chang, Seok-Woo
    • Restorative Dentistry and Endodontics
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    • v.37 no.4
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    • pp.188-193
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    • 2012
  • Mineral trioxide aggregate (MTA) was developed in early 1990s and has been successfully used for root perforation repair, root end filling, and one-visit apexification. MTA is composed mainly of tricalcium silicate and dicalcium silicate. When MTA is hydrated, calcium silicate hydrate (CSH) and calcium hydroxide is formed. Formed calcium hydroxide interacts with the phosphate ion in body fluid and form amorphous calcium phosphate (ACP) which finally transforms into calcium deficient hydroxyapatite (CDHA). These mineral precipitate were reported to form the MTA-dentin interfacial layer which enhances the sealing ability of MTA. Clinically, the use of zinc oxide euginol (ZOE) based materials may retard the setting of MTA. Also, the use of acids or contact with excessive blood should be avoided before complete set of MTA, because these conditions could adversely affect the hydration reaction of MTA. Further studies on the chemical nature of MTA hydration reaction are needed.

The Interfacial Segregation of Elemental Ag in the Sputter-Deposited AgInSbTe Thin Films (스퍼터 증착시킨 AgInSbTe 박막에서 Ag의 계면편석)

  • Choi, Woo-S.;Kim, Myong-R.;Seo, Hun;Park, Jeong-W.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.05a
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    • pp.15-18
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    • 1996
  • The elemental segregation in the sputter-deposited AgInSbTe recording thin films was studied by means of Auger electron spectroscopy and ESCA for the specimens of as-deposited and as heat-treated conditions. Auger electron spectroscopy and ESCA revealed an extremely thin layer of elemental inhomogeneity, especially for the silver, even in as-deposited condition. The chemical analysis results obtained in this alloy system are discussed in terms of process parameters and target microstructure.

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Experimental Study for Evaluating Structural Behavior of RC Beams Strengthened by Tapered Ended CFRP Sheets (계단식 단부 형태의 탄소섬유시트로 보강된 RC보의 구조거동 평가에 관한 실험적 연구)

  • Kim, Young-Hee;Kim, Hee-Sun
    • Journal of the Korean Society for Advanced Composite Structures
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    • v.3 no.4
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    • pp.38-44
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    • 2012
  • This paper presents experimental studies aiming at evaluation of structural behaviors of RC (Reinforced Concrete) beams externally strengthened with taper ended CFRPs(Carbon Fiber Reinforced Polymers). Experiments are performed with RC beams having different numbers of CFRP layers and length of each layer. The beams are subjected to four point-bending with simply supported condition. Test results of taper ended CFRPs and non-tapered CFRPs are compared and the better strengthening effect is observed from tapered ended CFRPs.

Cross-Sectional Transmission Electron Microscopy Sample Preparation of Soldering Joint Using Ultramicrotomy

  • Bae, Jee-Hwan;Kwon, Ye-Na;Yang, Cheol-Woong
    • Applied Microscopy
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    • v.46 no.3
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    • pp.167-169
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    • 2016
  • Solder/electroless nickel immersion gold (ENIG) joint sample which is comprised of dissimilar materials with different mechanical properties has limited the level of success in preparing thin samples for transmission electron microscopy (TEM). This short technical note reports the operation parameters for ultramicrotomy of solder joint sample and TEM analysis results. The solder joint sample was successfully sliced to 50~70 nm thick lamellae at slicing speed of 0.8~1.2 mm/s using a boat-type $45^{\circ}$ diamond knife. Ultramicrotomy can be applied as a routine sample preparation technique for TEM analysis of solder joints.

Selective modulation of charge carrier transport of photo-anode in PEC cell by a graphitized fullerene interfacial layer (C70이 도입 된 물분해 수소생산용 텅스텐 산화물의 광촉매 특성 연구)

  • Hong, Eun-Mi;Kim, Min-Gyeong;Lee, Ju-Yeol;Park, Seon-Yeong;Mul, Guido;Im, Dong-Chan
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2014.11a
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    • pp.150-150
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    • 2014
  • 지구상 존재하는 화석연료의 고갈에 대한 우려와 함께 최근 들어 지구 온난화로 인해 야기되고 있는 심각한 지구환경 문제에 대한 관심이 고조되고 있다. 이산화탄소로 대표되는 지구 온난화를 일으키는 공해물질의 많은 부분이 현재 주에너지원으로 사용되는 화석연료에 기인하기 때문에 이를 대체할 수 있는 청정에너지 개발은 이미 세계적 당면 과제라고 할 수 있다. 그 중, 수소에너지는 청정에너지로써의 역할 뿐만 아니라 에너지 저장매체로써의 기능 또한 담당할 수 있어 주목 받고 있다. 본 연구에서는 텅스텐 광촉매를 사용하여 물을 수소와 산소로 분해 하고자 하였고 C70을 도입하여 분해 효율을 향상시키고자 하였다.

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Interfacial Microstructures between Ag Wiring Layers and Various Substrates (Ag 인쇄배선과 이종재료기판과의 접합계면)

  • Kim, Keun-Soo;Suganuma, Katsuaki;Huh, Seok-Hwan
    • Journal of Welding and Joining
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    • v.29 no.5
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    • pp.90-94
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    • 2011
  • Ag metallic particles from nano-scale to submicron-scale are combined with organic solvent to provide fine circuits and interconnection. Ink-jet printing with Ag nano particle inks demonstrated the potentials of the new printed electronics technology. The bonding at the interface between the Ag wiring layer and the various substrates is very important. In this study, the details of interfaces in Ag wiring are investigated primarily by microstructure observation. By adjusting the materials and sintering conditions, nicely formed interfaces between Ag wiring and Cu, Au or organic substrates are achieved. In contrast, transmission electron microscope (TEM) image clearly shows interface debonding between Ag wiring and Sn substrate. Sn oxides are formed on the surface of the Sn plating. The formation of these is a root cause of the interface debonding.

CuS/ZnO 이종 나노구조의 합성과 광촉매로의 응용 및 특성평가

  • Lee, Mi-Gyeong;Choe, Min-Gi;Yong, Gi-Jung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.609-609
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    • 2013
  • 나노선은 대표적인 일차원 나노구조로 높은 부피-표면적 비율과, 조절 가능한 밴드갭 에너지, 뛰어난 광학적/전기적 특성으로 인해 다양한 잠재적 응용처를 가지며, 많이 연구되고 있다. 특히 ZnO 나노선은 대표적인 광촉매로, 높은 감광성과 높은 부피-표면적 비율 등의 특징을 가지지만, 상대적으로 넓은 밴드갭 에너지 때문에 가시광선 영역을 사용하지 못하는 단점이 있다. 본 연구에서는 CuS 나노입자/ZnO 나노선 이종구조를 간단한 두 가지의 방법으로 합성하였다. ZnO 나노선은 간단한 수열합성 방법으로 합성하였고, 그 위에 CuS 나노입자를 successive ionic layer adsorption and reaction (SILAR) 방법으로 증착하였다. 합성된 나노 구조는 기존의 ZnO 구조와는 달리 가시광 영역에서도 향상된 광촉매 특성을 보였으며, 이는 ZnO와 CuS사이의 interfacial charge transfer (IFCT)에서 기인한 것이다. SEM, TEM, XRD를 통해 CuS/ZnO 이종구조의 형태와 결정구조, 구성성분을 분석할 수 있었고, Acid Orange 7의 광분해 실험을 통해 향상된 광촉매 특성을 확인 할 수 있었다.

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Investigation of charge injection in organic thin film transistor using ink-jet printed silver electrodes

  • Kim, Dong-Jo;Jeong, Sun-Ho;Lee, Sul;Jang, Dae-Hwan;Moon, Joo-Ho
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08a
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    • pp.730-732
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    • 2007
  • We fabricated a coplanar type organic thin-film transistors using ink-jet printed silver source/drain electrodes and ${\alpha},{\omega}-dihexylquaterthiophene$ (DH4T) which is an active layer. Use of ink-jet printed silver nanoparticle-based metal electrode assists the energetic mismatch with p-type organic semiconductor via modification of their interfacial properties to enable ohmic contact formation.

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