• Title/Summary/Keyword: Inside diameter

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Physicochemical properties and methane adsorption performance of activated carbon nanofibers with different types of metal oxides

  • Othman, Faten Ermala Che;Yusof, Norhaniza;Hasbullah, Hasrinah;Jaafar, Juhana;Ismail, Ahmad Fauzi;Nasri, Noor Shawal
    • Carbon letters
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    • v.24
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    • pp.82-89
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    • 2017
  • In this study, composite PAN-based ACNFs embedded with MgO and $MnO_2$ were prepared by the electrospinning method. The resultant pristine ACNFs, ACNF/MgO and $ACNF/MnO_2$ were characterized in terms of their morphological changes, SSA, crystallinity and functional group with FESEM-EDX, the BET method, XRD and FTIR analysis, respectively. Results from this study showed that the SSA of the ACNF/MgO composite ($1893m^2g^{-1}$) is significantly higher than that of the pristine ACNFs and $ACNF/MnO_2$ which is 478 and $430m^2g^{-1}$, respectively. FTIR analysis showed peaks of 476 and $547cm^{-1}$, indicating the presence of MgO and $MnO_2$, respectively. The FESEM micrographs analysis showed a smooth but coarser structure in all the ACNFs. Meanwhile, the ACNF/MgO has the smallest fiber diameter ($314.38{\pm}62.42nm$) compared to other ACNFs. The presence of MgO and $MnO_2$ inside the ACNFs was also confirmed with EDX analysis as well as XRD. The adsorption capacities of each ACNF toward $CH_4$ were tested with the volumetric adsorption method in which the ACNF/MgO exhibited the highest $CH_4$ adsorption up to $2.39mmol\;g^{-1}$. Meanwhile, all the ACNF samples followed the pseudo-second order kinetic model with a $R^2$ up to 0.9996.

CORRELATION ASSESSMENT BETWEEN RESONANCE FREQUENCY ANALYSIS AND RADIOGRAPHIC METHOD ACCORDING TO PERI-IMPLANT BONE CHANGE

  • Lee Mi-Ran;Cho Lee-Ra;Yi Yang-Jin;Choi Hang-Moon;Park Chan-Jin
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.6
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    • pp.736-744
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    • 2005
  • Statement of problem. Initial stability of implant is an important factor for predicting osseointegration. It requires a rapid, non-invasive, user-friendly technique to frequently assess the implant stability and the degree of osseointegration. Purpose. The aim of this study was to evaluate the correlation between the resonance frequency analysis (RFA) and the radiographic method for peri-implant bone change under in vitro conditions. Material and Method. Twenty implants of 3.75 mm in diameter(Neoplant, Neobiotech, Korea) were used. To simulate peri-implant bone change, 2 mm-deep $45^{\circ}$ range horizontal defect and 2 mm-deep $90^{\circ}$ range horizontal defect area were serially prepared perpendicular to the X-ray beam after conventional implant insertion. Customized film holding device was fabricated to standardize the projection geometry for serial radiographs of implants and direct digital image was obtained. ISQ values and gray values inside threads were measured before and after peri-implant bone defect preparation. Results. Within a limitation of this study, ISQ value of resonance frequency analysis was changed according to peri-implant bone change (p<0.05) and gray value of radiographic method was changed according to peri-implant bone change (p<0.05). There was no correlation between the ISQ value and the gray value for peri-implant bone change (p>0.05). But, in horizontal defect condition, relatively positive correlation were between ISQ and gray values(r=0.663). Conclusion. This results provided a possibility that peri-implant bone change may be evaluated by both RFA and radiographic method.

Bone-to-Implant Contact according to the Surface Roughness of the Implants (임플란트의 표면조도가 골융합에 미치는 영향)

  • Choi, Kwi-Hyun;Herr, Yeek;Lee, Man-Sub;Kwon, Young-Hyuk
    • Journal of Periodontal and Implant Science
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    • v.33 no.4
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    • pp.717-728
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    • 2003
  • This study was performed to evaluate the difference of the bone-to-implant contact according to the surface roughness of the implants. Two beagles were used in the experiment. Extraction of the all premolars was performed in the mandible. In 3 months of healing, screw-shaped pure titanium machined surface implants (Implantium(R), Dentium Co. Korea), implants blasted with 45${\mu}m$ $TiO_2$ particles, (Implantium(R), Dentium Co. Korea) and implants blasted with 100${\mu}m$ $TiO_2$ particles (Implantium(R), Dentium Co. Korea) in diameter 3.4mm and length 6mm were installed in the edentulous mandible. Each dog was sacrificed at 4, 12 weeks after placement and then nondecalcified specimens were prepared for histologic analysis. The results of this study were as follows. 1. At 4 , 12 weeks after the surgery, bone-to-implant contact in the surface blasted with $TiO_2$ particles was higher than that in the pure titanium machined surface respectively. 2. Osseointegration in the surface blasted with 45${\mu}m$ $TiO_2$ particles was more increased than that in the surface blasted with 100${\mu}m$ $TiO_2$ particles. 3. Bone-to-implant contact was increased with time independent of surface roughness. 4. Bone formation was in the outfolded area more than inside the threads independent of surface roughness. From the above results, we were able t o find the most bone-to-implant contact in 45${\mu}m$ $TiO_2$ blasted implant.

Relations Between Impact Damage and Ply Angle Under Same Impact Energy Condition (同一한 衝擊에너지 條件下의 CFRP 斜交積層板의 衝擊損傷과 配向角의 關係)

  • ;笠野英秋
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.16 no.10
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    • pp.1824-1832
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    • 1992
  • This study investigated the compressive Young's modulus and the impactinduced damage of CFRP angle-ply laminate under same impact energy condition. The specimens of angle-ply laminate composites [0.deg.$_{6}$/ .theta..deg.$_{10}$/ 0.deg.$_{6}$] with .theta..deg. =30.deg., 45.deg., 60.deg. and 90.deg. were employed, and damaged by steel balls of diameter of 5mm and 10mm propelled by air gun type impact testing machine. The impact damaged zones were observed through a scanning acoustic microscope(SAM), and their cross-sections were observed through a scanning electron microscope(SEM). The compressive Young's moduli before and after impact were measured, and compared with the theoretical values calculated. The results obtained were as follows: (1) The damage areas on the interfacial boundaries showed more severe change on the back side interface than on the impact side interface with increasing ply-angle. (2) The damage areas on the interfacial boundaries became larger with increasing impact velocity or ply-angle. (3) The impact damaged zone showed the delamination on the interfacial boundaries and transverse cracks inside laminas. (4) The impact damaged zone was affected by the impactor size and speed or ply-angle under same impact energy condition. (5) Compressive Young's moduli before and after impact were lower than theoretical value, but showed a similar change according to ply-angle. (6) Compressive Young's moduli after impact were higher than those before impact, but there was no remarkable change in apparent compressive modulus after impact.t.act.

Signal Characteristics of Multi-coil Probe for the Test of Reinforcement Embedded in Concrete (다중 코일에 의한 콘크리트내의 철근 탐지 시 신호 특성)

  • Kim, Young-Joo;Lee, Seung-Seok;Yoon, Dong-Jin
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.4
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    • pp.285-289
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    • 2000
  • This study suggests a rebar detection technique for simultaneous detection of size and cover of embedded reinforcement in concrete. The structure of the probe made in this study is somewhat different from commercial ones. This probe has three sensing coils. Rebar size and cover depth can be evaluated by detecting and analyzing the signal from them. Amplitude and phase variation of each coil in the probe was investigated using an impedance analyzer and the loci of transfer functions of the coils were analyzed. The locus of transfer function from the sensing coil positioned inside excitation coil was simple as well known, but the others from the coils outside excitation coil were not so. Actual experiment on rebar detection was performed with our probe and an eddy current test system for various rebar sizes and depths. The signal shape according to variation of cover depths showed the same tendency with the transfer function loci acquired by impedance analyzer. The different variation pattern of signal enabled to evaluate rebar size and cover depth simultaneously.

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Evaluation of the Biocompatibility of Cuttlebone in Mouse (쥐에서 오적골 생체적합성 평가)

  • Won, Sangcheol;Lee, Joo Myoung;Cheong, Jongtae;Park, Hyunjung;Seo, Jongpil
    • Journal of Veterinary Clinics
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    • v.32 no.5
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    • pp.417-421
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    • 2015
  • Bone grafting is widely used to bridge major bone defects or to promote bone union. Natural calcium carbonate (CC) has been used as a bone substitute material and used to scaffold for bone morphogenetic protein (BMP). The aims of this study is to evaluate the biocompatibility of cuttlebone (CB) and hydroxyapatite from CB (CBHA). Each material was shaped into disks (5 mm in diameter and 2 mm in thickness). To test biocompatibility, the disks were implanted into the dorsal subcutaneous tissue in mice. Fibrous capsule thickness around each disk was evaluated histologically at 2 and 4 weeks after implantation. Concerning biocompatibility, fibrous capsule thickness of CBHA was significantly thinner than that of CB and CHA (p < 0.05) at 2 and 4 weeks after implantation. Based on the clinical and histological results, CBHA would be a safe material for use inside the body and has more effective osteoconduction than CB.

Chemical Composition and Lead Isotope Ratio of Divine Bell of King Seongdeok (성덕대왕신종(국보 제29호)의 성분조성과 납동위원소비)

  • Kang, Hyungtae;Kim, Jongoh;Kwon, Hyuknam;Yu, Heisun
    • Conservation Science in Museum
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    • v.5
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    • pp.49-57
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    • 2004
  • The Divine Bell of King Seongdeok was completed in 771 A.D. It is a true masterpiece both grand in its size and style (height 3.66 m, diameter 2.23 m, thickness 20.3 cm, weight 18.9 ton), illustrating the essence of the Korean bronze culture. However, there are no remaining records about its casting: where the raw material came from, how the materials were mixed and how the bell was casted. The absence of such records has limited the understanding of the bell. This article contains analysis of three samples collected from a protruding part inside of the bell during a safety test for the bell by the Gyeongju National Museum. The main issues are the element composition of the bell, microstructure on the casting time and the source where the raw material came from.

Development of Automatic Nut Inspection System using Image Processing (이미지 프로세싱을 이용한 자동 너트 검사 장비 개발)

  • Lee, Sang-Hak;Seo, Myong-Ho;Chung, Tae-Choong
    • The KIPS Transactions:PartA
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    • v.11A no.4
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    • pp.235-242
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    • 2004
  • When manufacturing information and communication device that consists of lots of part, it is important to improve the quality of the produced system by inspecting the system accurately and exclude the defected part. In case of LCD which is recently in a great demand, the inspection process of the nut which bonds the back frame to protect the LCD panel has to be done by human labor. It highly required an automatic inspection system which can inspect the nut without wasting human resources. In this paper, we describe the process of developing a system which automatically inspect the status of nuts inserted during the manufacturing of LCD. The nut inspection vision system developed measures the number of nut's spiral, the distance between pitches, the width of a pitch, and the inside diameter of nut. We have adopted lens with high magnifying power and calibration tool and intended to produce automatic lighting for maintaining a stable environment for a high precision system. We also developed the algorithms for analyzing the nut. We apply the system to real factory field and verify that it is better than the man power in terms of error rate.

Development of Prepolarization Coil Current Driver in SQUID Sensor-based Ultra Low-field Magnetic Resonance Apparatuses (SQUID 센서 기반의 극저자장 자기공명 장치를 위한 사전자화코일 전류구동장치 개발)

  • Hwang, S.M.;Kim, K.;Kang, C.S.;Lee, S.J.;Lee, Y.H.
    • Progress in Superconductivity
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    • v.13 no.2
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    • pp.105-110
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    • 2011
  • SQUID sensor-based ultra low-field magnetic resonance apparatus with ${\mu}T$-level measurement field requires a strong prepolarization magnetic field ($B_p$) to magnetize its sample and obtain magnetic resonance signal with a high signal-to-noise ratio. This $B_p$ needs to be ramped down very quickly so that it does not interfere with signal acquisition which must take place before the sample magnetization relaxes off. A MOSFET switch-based $B_p$ coil driver has current ramp-down time ($t_{rd}$) that increases with $B_p$ current, which makes it unsuitable for driving high-field $B_p$ coil made of superconducting material. An energy cycling-type current driver has been developed for such a coil. This driver contains a storage capacitor inside a switch in IGBT-diode bridge configuration, which can manipulate how the capacitor is connected between the $B_p$ coil and its current source. The implemented circuit with 1.2 kV-tolerant devices was capable of driving 32 A current into a thick copper-wire solenoid $B_p$ coil with a 182 mm inner diameter, 0.23 H inductance, and 5.4 mT/A magnetic field-to-current ratio. The measured trd was 7.6 ms with a 160 ${\mu}F$ storage capacitor. trd was dependent only on the inductance of the coil and the capacitance of the driver capacitor. This driver is scalable to significantly higher current of superconducting $B_p$ coils without the $t_{rd}$ becoming unacceptably long with higher $B_p$ current.

A Study of the Pollutant Formation and Spectral Radiation Properties in Ceramic Fiber Radiant Burner (세라믹 화이버 버너의 배기 배출물과 분광학적 특성에 관한 연구)

  • Jeong, Yong-Ki;Kim, Young-Soo;Lee, Dae-Rae;Yang, Dae-Bong;Ryu, Jung-Wan;Yun, Alexander;Ha, Man-Young;Chang, Young-June;Jeon, Chung-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.31 no.9
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    • pp.790-798
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    • 2007
  • An experimental study was performed to investigate the effects of mixing quality, inlet pressure, nozzle diameter on CO, NO emission and radiation characteristics in porous ceramic fiber radiant burners. Observations of combustion characteristics occurring inside the burner system which was insulated fiber mat, were investigated by measuring emission and radiation characteristics. Combustion was achieved at the firing rate of $88{\sim}99\;kcal/hr$, inlet pressure of $100{\sim}250mmH_2O$. The fiber burner exhibit significant both spectral intensity peaks in the bands at $2.5{\mu}m\;and\;4.0{\mu}m$ relatively. There is a small difference in the variable mixing tube. However spectral intensity increased with the firing rate. CO emissions were found to be strongly dependent on the operating conditions. There was a tendency that CO concentration increased as the firing rate increases. the reason for rise of CO concentration is that is becomes it the relatively rich condition. Relatively low NO emission was observed for the whole operating range. The NO concentration is maximal at the firing rate of approximately 2850 kcal/hr and an air ratio of about 1.