• Title/Summary/Keyword: Infrared analysis

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ANALYTICAL APPLICATIONS OF NEW PORTABLE NEAR INFRARED (NIR) SPECTROMETER SYSTEM

  • Ahn, Jhii-Weon;Kang, Na-Roo;Lim, Hung-Rang;Lee, Jung-Hun;Woo, Young-Ah;Kim, Hyo-Jin
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1122-1122
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    • 2001
  • A compact and handhold near infrared (NIR) system using microspectrometer was developed. This system was suitable not only in the laboratory, but also in the field or in the process. This system was first applied for classification of geographical origin of herbal medicine such as ginseng and sesame. To identify the origin of ginseng on site, the portable NIR system is more suitable for real field application. For this study, using the compact NIR system, soft independent modeling of class analogies (SIMCA) with 1100-1750 nm NIR spectra was utilized for classification of geographical origin (Korea and China) of both ginseng and sesame. The accuracy of results is more than 90%. Quantitative analysis for petroleum such as toluene, benzene, tri-methyl benzene, and ethyl benzene was performed with partial least squares (PLS) regression with NIR 1100-1750 nm spectra. This study showed that the NIR method and gas chromatography (GC), which is a standard method, have good correlations. Furthermore, the ash content of Cornu Cervi Parvum was analyzed and the accuracy was confirmed by the developed compact NIR system.

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Discrimination Analysis of Gallstones by Near Infrared Spectrometry Using a Soft Independent Modeling of Class Analogy

  • Lee, Sang-Hak;Son, Bum-Mok;Park, Ju-Eun;Choi, Sang-Seob;Nam, Jae-Jak
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.4106-4106
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    • 2001
  • A method to discriminate human gallstones by nea. infrared(NIR) spectrometry using a soft independent modeling of class analogy (SIMCA) has been studied. The fifty NIR spectra of gallstones in the wavenumber range from 4500 to 10,000 cm$\^$-1/ were measured. The forty samples were classified to three classes, cholesterol stone, calcium bilirubinate stone and calcium carbonate stone according to the contents of major components in each gallstone. The training set which contained objects of the different known class was constructed using forty NIR spectra and the test set was made with ten different gallstone spectra. The number of important principal components(PCs) to describe the class was determined by cross validation in order to improve the decision criterion of the SIMCA for the training set. The score plots of the class training set whose objects belong to the other classes were inspected. The critical distance of each class was computed using both the Euclidean distance and the Mahalanobis distance at a proper level of significance(${\alpha}$). Two methods were compared with respect to classification and their robustness towards the number of PCs selected to describe different classes.

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Scene-based Nonuniformity Correction Algorithm Based on Temporal Median Filter

  • Geng, Lixiang;Chen, Qian;Qian, Weixian;Zhang, Yuzhen
    • Journal of the Optical Society of Korea
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    • v.17 no.3
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    • pp.255-261
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    • 2013
  • Scene-based nonuniformity correction techniques for infrared focal-plane arrays have been widely considered as a key technology, and various algorithms have been proposed to compensate for fixed-pattern noise. However, the existed algorithms' capability is always restricted by the problems of convergence speed and ghosting artifacts. In this paper, an effective scene-based nonuniformity correction method is proposed to solve these problems. The algorithm is an improvement over the constant statistics method and a temporal median is utilized with the Gaussian kernel to estimate the nonuniformity parameters. Also theoretical analysis is conducted to demonstrate that effective ghosting artifacts elimination and superior convergence speed can be obtained with the proposed method. Finally, the performance of the proposed technique is tested with infrared image sequences with simulated nonuniformity and with infrared imagery with real nonuniformity. The results show the proposed method is able to estimate each detector's gain and to offset reliably and that it performs better in increasing convergence speed and reducing ghosting artifacts compared with the conventional techniques.

Effect of particle size and scanning cup type for near infrared reflection on the soil property measurement

  • Ryu, Kwan-Shig;Cho, Rae-Kwang;Park, Woo-Churl;Kim, Bok-Jin
    • Near Infrared Analysis
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    • v.1 no.2
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    • pp.35-39
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    • 2000
  • The purpose of this research was to find out suitable soil sample preparation and sample holding tools for NIR reflection radiation for estimating soil components. NIR reflectance was scanned at 2nm intervals from 1,100 to 2,500nm with an InfraAlyzer 500(Bran+Luebbe Co.). Coarse(2.0mm) and fine(0.5mm) soil sample and various sample holding tools were used to obtain mean diffuse reflection of the soil for the calibration and validation of the calibration set in estimating moisture, organic matter and total nitrogen of the soils. Multiple linear regression was used to obtain the best correlation of NIR spectroscopy method. Correlation of NIR spectroscopy method. Correlation of NIR spectra for finely and coarsely sized soil did not show much difference. The standard errors of prediction(SE) using different types of sample holding tools for organic matter, total nitrogen and soil moisture were better than 0.765, 0.041 and 0.63% respectively. From the results it can be concluded that NIR spectroscopy with flow type cell could be used as a fast routine testing method in quantitative determination of organic matter, total nitrogen and soil moisture.

Application Study of Chemoinfometrical Near-Infrared Spectroscopic Method to Evaluate for Polymorphic Content of Pharmaceutical Powders (일본의 근적외선분광법에 대한 제약회사 응용 및 현황)

  • Otsuka, Makoto
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2002.11a
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    • pp.97-117
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    • 2002
  • A chemoinfometrical method for quantitative determination of crystal content of indomethacin (IMC) polymorphs based on fourie-transformed near-infrared (FT-NIR) spectroscopy was established. A direct comparison of the data with the ones collected from using the conventional powder X-ray diffraction method was performed. Pure $\alpha$ and ${\gamma}$ forms of IMC were prepared using published methods. Powder X-ray diffraction profiles and NIR spectra were recorded for six kinds of standard materials with various content of ${\gamma}$ form IMC. The principal component regression (PCR) analyses were performed based on normalized NIR spectra sets of standard samples of known content of IMC ${\gamma}$ form. A calibration equation was determined to minimize the root mean square error of the prediction. The predicted ${\gamma}$ form content values were reproducible and had a relatively small standard deviation. The values of ${\gamma}$ form content predicted by two methods were in close agreement. The results were indicated that NIR spectroscopy provides for an accurate quantitative analysis of crystallinity in polymorphs compared with the results obtained by conventional powder X-ray diffractometry.

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A Study of the Fatigue Crack Propagation Behavior According to the Moment Change using Infrared Thermography (열화상기술을 이용한 모멘트 변화에 따른 피로균열진전 연구)

  • Kim, Kyeong-Suk;Jung, Hyun-Chul;Pack, Chan-Joo;Jung, Duk-Woon;Chang, Ho-Sub
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.19 no.3
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    • pp.359-364
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    • 2010
  • The objective of this study is to propose an effective method for measurement and analysis of fatigue crack. A technique that can measure the statue of fatigue crack propagation fast and correctly for enhancing safety of constructions and securing reliability is necessary. Moreover, the crack propagation behavior characteristics evaluation technique has to be developed using this technique. In this paper, fatigue crack was caused via the fatigue experiment with repeated load on the CT specimen that is made up of STS304. Fatigue crack propagation was measured by tracing the position of the maximum temperature according to the cycles using infrared thermography. The crack growth characteristics was evaluated by applying the moment values on the measuring area to the measured value. As a result of this study, the possibility that the infrared thermography could be applied to measure the fatigue crack was identified. Moreover, it was identified that fatigue crack propagation have a relationship with the moment value of construction.

Far-Infrared Ray Drying Characteristics of Rough Rice (I) -Thin layer drying equation- (벼의 원적외선 건조특성 (I) -박층건조방정식-)

  • Keum, D. H.;Kim, H.;Hong, S. J.
    • Journal of Biosystems Engineering
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    • v.27 no.1
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    • pp.45-50
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    • 2002
  • This study was performed to develop thin layer drying equations fur short grain rough rice using far-infrared ray. Thin layer drying tests was conducted at four far-infrared ray temperature levels of 30, 40, 50, 60$^{\circ}C$ and two initial moisture content levels of 20.7, 26.2%(w.b.). The measured moisture ratios were fitted to Lewis and Page drying models by stepwise multiple regression analysis. Half response time of drying was affected by both drying temperature and initial moisture content at drying temperature of below 40$^{\circ}C$, but at above 40$^{\circ}C$ was mainly affected by drying temperature. Experimental constant(k) in Lewis model was a function of drying temperature, but K and N in Page model were function of drying temperature and initial moisture content. Moisture ratios predicted by two drying models agreed well with experimental values. But in the actual range of drying temperature above 30$^{\circ}C$ Page model was more suitable for predicting of drying rates.

Characterisation of Tensile Deformation through Infrared Imaging Technique

  • B. Venkataraman, Baldev Raj;Mukhophadyay, C.K.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.6
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    • pp.609-620
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    • 2002
  • It is well known that during tensile testing, a part of the mechanical work done on the specimen is transformed into heat energy. However, the ultimate temperature rise and the rate of temperature rise is related to the nature of the material, conditions of the test and also to the deformation behaviour of the material during loading. The recent advances in infrared sensors and image/data processing techniques enable observation and quantitative analysis of the heat energy dissipated during such tensile tests. In this study, infrared imaging technique has been used to characterise the tensile deformation in AISI type 316 nuclear grade stainless steel. Apart from identifying the different stages during tensile deformation, the technique provided an accurate full-field temperature image by which the point and time of strain localization could be identified. The technique makes it possible to visualise the region of deformation and failure and also predict the exact region of fracture in advance. The effect of thermal gradients on plastic flow in the case of interrupted straining revealed that the interruption of strain and restraining at a lower strain rate not only delays the growth of the temperature gradient, but the temperature rise per unit strain decreases. The technique is a potential NDE tool that can be used for on-line detection of thermal gradients developed during extrusion and metal forming process which can be used for ensuring uniform distribution of plastic strain.

Design and Analysis of Flame Signal Detection with the Combination of UV/IR Sensors (UV/IR센서 결합에 의한 불꽃 영상검출의 설계 및 분석)

  • Kang, Daeseok;Kim, Eunchong;Moon, Piljae;Sin, Wonho;Kang, Min-goo
    • Journal of Internet Computing and Services
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    • v.14 no.2
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    • pp.45-51
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    • 2013
  • In this paper, the combination of ultraviolet and infrared sensors based design for flame signal detection algorithms was proposed with the application of light-wavelength from burning. And, the performance result of image detection was compared by an ultraviolet sensor, an infrared sensor, and the proposed dual-mode sensors(combination of ultraviolet and infrared sensors).

An Experimental Study on the Thermal Load of a Cryochamber with Radiation Shields (복사 차폐막이 설치된 극저온 용기의 열부하 특성에 관한 실험적 연구)

  • Kim, Young-Min;Kang, Byung-Ha;Park, Seong-Je
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.20 no.1
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    • pp.11-16
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    • 2008
  • Infrared (IR) detectors are widely used for such applications as thermoelastic stress analysis, medical diagnostics and temperature measurement. Infrared detectors commonly need to be refrigerated below 80 K, and thus a cooling system should be equipped together with the detector system. The cooling load, which should be removed by the cooling system to maintain the nominal operating temperature of the detector, critically depends on the insulation efficiency of the cryochamber housing the detector. Thermal load of a cryochamber is attributed to the conduction heat transfer through a cold finger, the gases conduction and radiation heat transfer. The thermal loads of an infrared detector cryochamber with a radiation shield are investigated experimentally in present study. Since the effect of radiation heat transfer on thermal loads is significant, radiation shields is installed in the cold finger part to protect heat input through radiation.