• Title/Summary/Keyword: Infiltration growth process

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Comparative Study on the Fabrication of Single Grain YBCO Bulk Superconductors using Liquid Infiltration and Conventional Melt Growth Processes (단결정 YBCO 벌크 초전도체 제조에 대한 액상침투법과 고전적 용융공정의 비교연구)

  • Mahmood, Asif;Jun, Byung-Hyuk;Kim, Chan-Joong
    • Progress in Superconductivity
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    • v.11 no.1
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    • pp.42-46
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    • 2009
  • With an aim of comparison, single grain Y-Ba-Cu-O (YBCO) bulk superconductors were fabricated using a liquid infiltration growth (LIG) process and a conventional melt growth (MTG) process with top seeding. The MTG process uses an $YBa_2Cu_3O_{7-x}$(Y123) powder as a precursor, while the LIG process uses $Y_2BaCuO_5(Y211)/Ba_3Cu_5O_8(Y035)$ pre-forms. The growth of a single Y123 domain on the top seed was successful in the both processes. Different feature between the two processes is the interior microstructure regarding the critical current density ($J_c$). The LIG-processed YBCO sample showed a lower porosity, more uniform distribution of Y211 particles and the enhanced Y211 refinement compared to the conventional MTG process. The $J_c$ improvement in the LIG process is attributed to the dispersion of finer Y211 particles as well as lower porosity within the Y123 superconducting matrix.

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Fabrication and mechanical properties of $Al_2O_3/AL$ composites by reactive melt infiltration (반응용융 침투법에 의한 $Al_2O_3/AL$복합재료의 제조 및 기계적 특성 평가)

  • ;;;T. Watari
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.4
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    • pp.610-618
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    • 1997
  • $Al_2O_3$/Al composite was produced by the infiltration of molten Al Into $Al_2$O$_3$ preform at 900-$1200^{\circ}C$, The process was accelerated by spreading borosilicate glass powder onto the interface between Al powder compact and $Al_2O_3$ preform. Melt infiltration initialed after incubation period, and the growth of infiltration was observed to be linearly propotional with time. The major components of the composite are $Al_2O_3$ and Al with a trace of Si which is remained from borosilicate, the reaction accelerator. Relative density of the composite increased with the particle size of $Al_2O_3$ but decreased with infiltration temperature. As infiltration temperature increases from room to $950^{\circ}C$ higher strength and fracture toughness were obtained.

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A sturdy on the sintering characteristics for Cu-Cr contact material (Cu-Cr 계 접점재료의 소결특성에 관한 연구)

  • Yeon, Young-Myoung;Oh, Il-Sung;Park, Hong-Tae;Lee, Sang-Yeup;Seo, Jung-Min
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.1643-1645
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    • 2000
  • The effects of pre-sintering and infiltration conditions on the electrical and physical properties of Cu-Cr contact material have been studied. Specimens were prepared by infiltration technique, aiming at the final composition of Cu50w%Cr, with varying pre-sintering and infiltration conditions. It showed that increased pre-sintering temperature had a little influence on the final microstructure of Cu-Cr contact material, but improved the surface morphology of Cr-skeleton resulting in better wettability in the followed infiltration process. It also showed that Cr grain growth and gram shape change became prominent with increasing infiltration temperature and time.

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Processing and properties of $Al_{2}O_{3}/SiC$ nanocomposites by polycarbosilane infiltration

  • Jung-Soo Ha;Chang-Sung Lim;Chang-Sam Kim
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.12 no.2
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    • pp.80-86
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    • 2002
  • $Al_{2}O_{3}/SiC$ nanocomposites were made by infiltrating partially sintered alumina bodies with polycarbosilane (PCS) solutions, which is a SiC polymer precursor, with pressureless sintering. The SiC content, densification, phases, strength, and microstructure were investigated with the processing parameters such as PCS solution concentration and heat treatment condition for PCS pyrolysis and sintering. The results were compared with those for pure alumina and nanocomposite samples made by the existing polymer precursor route (i.e. the PCS addition process). The SiC contents of up to 1.5 vol% were obtained by the PCS infiltration. PCS pyrolysis, followed by air heat treatment, was needed before sintering to avoid a cracking problem and to attain a densification as high as 98 % of theoretical. The nanocomposites exhibited significantly higher strength than pure alumina and those prepared by the PCS addition process despite larger grain size. Besides $\alpha-Al_{2}O_{3}/SiC$ and $\beta-SiC$ phases, mullite was present a little in the nanocomposites, which resulted from the reaction of $SiO_{2}$ in the pyrolysis product of PCS with the $Al_{2}O_{3}$ matrix during sintering. The nanocomposites had intagranular particles believed to be SiC, which is a typical feature of $Al_{2}O_{3}/SiC$ nanocomposites.

Modeling Effective Rainfall for Upland Crops (밭에서의 유효우량 산정모형 개발)

  • 정하우;김성준
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.35 no.1
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    • pp.29-39
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    • 1993
  • A model for estimating daily effective rainfall of upland crops was developed. The infiltration process was described by Green-Ampt infiltration model developed by Chu(1978). The model considers delayed surface ponding and surface detention storage under a uniform soil profile. The Green-Ampt parameters, that is, average hydraulic conductivity and average capillary pressure head on a sandy loam soil were determined from field experiment using Air-entry permeameter developed by Bouwer(1966). The model was verified by comparing measured and simulated surface runoff. The ratios of effective rainfall to total rainfall for red pepper, soybean, sesame and Chinese cabbage were evaluated using Borg's root growth model( 1986) respectively. The followings are a summary of this study results; 1.In a sandy loam soil average hydraulic conductivity was 3.28cm/hr and average capillary pressure head was 3.00cm. 2.The root growth of upland crops could be expressed by Borg's root growth model successively. 3.The measured and simulated surface runoff was agreed well with each other. 4.As the rainfall amount was increased, the ratio of effective rainfall to total rainfall was decreased exponentially till a certain growing period.

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Growth of Al2O3/Al Composite by Directed Metal Oxidation of Al Surface Doped with Sodium Source

  • Park, Hong Sik;Kim, Dong Seok;Kim, Do Kyung
    • Journal of the Korean Ceramic Society
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    • v.50 no.6
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    • pp.439-445
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    • 2013
  • Both an unreinforced $Al_2O_3$/Al matrix and a ${\alpha}-Al_2O_3$ particulate reinforced composite have been produced by the oxidation of an Al surface doped with NaOH in the absence of any other dopant. Fabrication of the matrix was initiated by the formation of $NaAlO_2$, which provides a favorable surface structure for the matrix formation by breaking the protective $Al_2O_3$ layer on Al. During the matrix growth, the external surface of the growth front was covered with a very thin sodium-rich oxide. A cyclic formation process of the sodium-rich oxide on the growth surface was proposed for the sodium-induced directed metal oxidation process. This process involves dissolution of the sodium-rich oxide, motion of Na to the growth front, and re-formation of the oxide on the surface. Near-net-shape composites were fabricated by infiltrating an $Al_2O_3$/Al matrix into a ${\alpha}-Al_2O_3$ particulate preform, without growth barrier materials. The infiltration distance increased almost linearly in the NaOH-doped preform.

$\beta$-SiC Formation Mechanisms in Si Melt-C-SiC System (용융 Si-C-SiC계에서 $\beta$-SiC 생성기구)

  • 서기식;박상환;송휴섭
    • Journal of the Korean Ceramic Society
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    • v.36 no.6
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    • pp.655-661
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    • 1999
  • ${\beta}$-SiC formation mechanism in Si melt-C-SiC system with varying in size of carbon source was investigated. A continuous reaction sintering process using Si melt infiltration method was adopted to control the reaction sintering time effectively. It was found that ${\beta}$-SiC formation mechanism in Si melt-C-SiC system was directly affected by the size of carbon source. In the Si melt-C-SiC system with large carbon source ${\beta}$-SiC formation mechanism could be divided into two stages depending on the reaction sintering time: in early stage of reaction sintering carbon dissolution in Si melt and precipitation of ${\beta}$-SiC was occurred preferentially and then SIC nucleation and growth was controlled by diffusion of carbon throughy the ${\beta}$-SiC layer formed on graphite particle. Furthmore a dissolution rate of graphite particles in Si melt could be accelerated by the infiltration of Si melt through basal plane of graphite crystalline.

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EFFECT OF LOW LEVEL LASER THERAPY ON HEALING OF OPEN SKIN WOUNDS IN RATS (백서 연조직에 저수준 레이저 요법시 창상 치유기전에 관한 연구)

  • You, Sang-Woo;Kim, Kyung-Wook;Lee, Jae-Hoon;Kim, Chang-Jin
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.26 no.5
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    • pp.481-489
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    • 2000
  • This research was focused on overall examination of tissue alteration, wound healing promotion. After the hair on the dorsal surface was shaved, $5{\times}5mm$ oval skin defect was formed. Experimental wounds of right side were irradiated on every day for 90 second with Ga-Al-As semi-conductor laser. Left side wounds served as control group. The rats were sacrificed on the 1st, 3rd, 5th, 7th, 14th, 21th day. For light microscopically, parafin section were stained with H&E, MT. The outcomes were as follows : 1. On 1st day, experimental and control group were seen acute inflammatory cell infiltration, edema. 2. On the 3rd days, both groups were seen crust development, collagen, blood vessel proliferation. 3. On the 5th days, experimental group were reduced edema and inflammatory cell infiltration than control group. 4. On the 7th days, both groups were observed edema, inflammatory cell infiltration disappearance and keratinocytes motility from wound defect. 5. On the 14th days, experimental group appeared collagen, blood vessel proliferation and hair follicle than control group. 6. On the 21th days, both groups were seen normal status re-epithelization. According to the above results, The wound-healing stimulated by laser radiation involves an increased rate of epithelial growth. LLLT was confirmed that it has fibroblast, blood vessel proliferation, influence initial wound healing process.

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Formation of $Al_2O_3$-Ceramics by Reactive Infiltration of Al-alloy into Insulation Fiber Board (Al-합금의 단열섬유판 반응침투에 의한 $Al_2O_3$-세라믹스의 형성)

  • 김일수
    • Journal of the Korean Ceramic Society
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    • v.34 no.5
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    • pp.483-490
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    • 1997
  • Al2O3/metal composites were fabricated by oxidation and reaction of molten Al-alloy into two types of commercial Al2O3-SiO2 fibrous insulation board. The growth rate, composition and microstructure of these materials were described. An AlZnMg(7075) alloy was selected as a parent alloy. Mixed polycrystalline fiber and glass phase fiber were used as a filler. The growth surface of an alloy was covered with and without SiO2. SiO2 powder was employed as a surface dopant to aid initial oxidation of Al-alloy. Al-alloy, SiO2, fiber block and growth inhibitor CaSiO3 were packed sequentially in a alumina crucible and oxidized in air at temperature range 90$0^{\circ}C$ to 120$0^{\circ}C$. The growth rate of composite layer was calculated by measuring the mass increasement(g) per unit surface($\textrm{cm}^2$). XRD and optical microscope were used to investigate the composition and phase of composites. The composite grown at 120$0^{\circ}C$ and with SiO2 dopant showed rapid growth rate. The growth behavior differed a little depending on the types of fiber used. The composites consist of $\alpha$-Al2O3, Al, Si and pore. The composite grown at 100$0^{\circ}C$ exhibited better microstructure compared to that grown at 120$0^{\circ}C$.

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