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The effect of Tempering on the Mechanical Properties of Mod. 440A Martensitic Stainless Steel (Mod. 440A 마르텐사이트 스테인리스강의 기계적 성질에 미치는 템퍼링의 영향)

  • Kwon, S.D.;Kim, Y.C.;Kang, C.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.3
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    • pp.120-125
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    • 2013
  • In this study, the effect of tempering treatment on the mechanical properties in modified 440A steel has been investigated. The amount of remaining carbide decreased with increasing the austenitizing treatment temperature, and all carbides were completely dissolved at $1250^{\circ}C$. The amount of remaining carbide decreased with increasing the time of austenitizing, but the carbide remained insoluble up to 120 minutes at $1050^{\circ}C$. With increasing the tempering temperature, tensile strength decreased, and elongation increased slowly, while hardness rapidly decreased, and impact value unchanged and then rapidly increased over $500^{\circ}C$. The strength and hardness slowly decreased, while the elongation and impact absorbed energy increased with increasing the tempering time. $Cr_{23}C_6$ type carbide was precipitated and sharp decrease of elongation and toughness by tempering did not appear.

Synthesis and Properties of Photocurable Dipentaerythritol Modified Polymethacrylates (광경화형 Dipentaerythritol 변성 폴리메타아크릴레이트의 합성과 물성)

  • Kim, Dong Kook;Lim, Jin Kyu;Kim, Woo Geun;Haw, Jung Rim
    • Applied Chemistry for Engineering
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    • v.16 no.1
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    • pp.101-106
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    • 2005
  • Photocurable modified 6 functional polyacrylate(PA-1) were prepared from dipentaerythritol derivatives (DPET) and acrylic acid, and 12 functional polymethacrylate(PA-2) were prepared from dipentaerythritol derivatives (DPET), trimellitic anhydride, and glycidyl methacrylate. And physical properties of photocurable modified poly(meth)acrylate were increased with increasing functionality of (meth)acrylate. Thermal stability of UV cured film obtained by using TGA was shifted to higher temperature as the increasing of functionality. Hardness, abrasion resistance and tensile strength of UV cured film were increased with increasing functionality of (meth)acrylate. Values of yellow index were increased with increasing functionality of (meth)acrylate.

Stochastic Properties of Life Distribution with Increasing Tail Failure Rate and Nonparametric Testing Procedure

  • Lim, Jae-Hak;Park, Dong Ho
    • Journal of Applied Reliability
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    • v.18 no.3
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    • pp.220-228
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    • 2018
  • Purpose: The purpose of this study is to investigate the tail behavior of the life distribution which exhibits an increasing failure rate or other positive aging effects after a certain time point. Methods: We characterize the tail behavior of the life distribution with regard to certain reliability measures such as failure rate, mean residual life and reliability function and derive several stochastic properties regarding such life distributions. Also, utilizing an L-statistic and its asymptotic normality, we propose new nonparametric testing procedures which verify if the life distribution has an increasing tail failure rate. Results: We propose the IFR-Tail (Increasing Failure Rate in Tail), DMRL-Tail (Decreasing Mean Residual Life in Tail) and NBU-Tail (New Better than Used in Tail) classes, all of which represent the tail behavior of the life distribution. And we discuss some stochastic properties of these proposed classes. Also, we develop a new nonparametric test procedure for detecting the IFR-Tail class and discuss its relative efficiency to explore the power of the test. Conclusion: The results of our research could be utilized in the study of wide range of applications including the maintenance and warranty policy of the second-hand system.

Evaluation or various vehicles and O/W Microemulsions of Flurbiprofen as Transdermal Delivery System (경피제제로서 수종의 플루비프로펜 Vehicle과 O/W 마이크로에멀젼의 평가)

  • Lee, Gye-Won;Jee, Ung-Kil
    • Journal of Pharmaceutical Investigation
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    • v.28 no.3
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    • pp.141-149
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    • 1998
  • In order to reduce systemic side effects following administration, flurbiprofen was formulated as O/W microemulsion consisting of the surfactant, oil phase and aqueous phase. Particle size distribution, apparent viscosity, solubility and skin permeation of flurbiprofen in various vehicles and microemulsion were evaluated. The domain of O/W microemulsion s phase diagram had difference between oil types and the area of O/W microemulsion was wide distributed by adding to PG and cosurfactant than that of water alone. As increasing 10, 15 and 20% of Brij 97 content and 1, 2.5, 5% of oil content, the solubility of flurbiprofen in O/W microemulsions and various vehicles was $400{\sim}1,000$ and $10{\sim}500$ times higher than that of control. Also, apparent viscosity of soybean oil microemulsions was higher than that of IPM microemulsions and that of vehicle were increased as increasing vehicle content. Since skin permeation of flurbiprofen decreased as increasing viscosity, in each vehicle, it was not affected 2% ${\beta}-CD$ and decreased as increasing PG content and to 2, 5 and 10% of $HP-{\beta}-CD$. In O/W microemulsion, 5% soybean oil. 20% Brij 97 and 75% water(A-1) with high viscosity showed low skin penetration.

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Stability of Attached Flame in $H_2$/CO Syngas Non-premixed Turbulent Jet Flame ($H_2$/CO 합성가스 비예혼합 난류 제트화염에서 부착화염의 화염안정화)

  • Hwang, Jeong-Jae;Bouvet, Nicolas;Sohn, Ki-Tae;Yoon, Young-Bin
    • Journal of the Korean Society of Combustion
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    • v.17 no.1
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    • pp.22-29
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    • 2012
  • The detachment stability characteristics of syngas $H_2$/CO jet attached flames were studied. The flame stability was observed while varying the syngas fuel composition, coaxial nozzle diameter and fuel nozzle rim thickness. The detachment stability limit of the syngas single jet flame was found to decrease with increasing mole fraction of carbon monoxide in the fuel. In hydrogen jet flames with coaxial air, the flame detachment stability was found to be independent of the coaxial nozzle diameter. However, velocities of appearance of liftoff and blowout velocities of lifted flames have dependence. At lower fuel velocity range, the critical coaxial air velocity leading to flame detachment increases with increasing fuel jet velocity, whereas at higher fuel velocity range, it decreases. This increasing-decreasing non-monotonic trend appears for all $H_2$/CO syngas compositions (50/50~100/0% $H_2$/CO). To qualitatively understand the flame behavior near the nozzle rim, $OH^*$ chemiluminescence imaging was performed near the detachment limit conditions. For all fuel compositions, local extinction on the rim is observed at lower fuel velocities(increasing stability region), while local flame extinction downstream of the rim is observed at higher fuel velocities(decreasing stability region). Maximum values of the non-monotonic trends appear to be identical when the fuel jet velocity is normalized by the critical fuel velocity obtained in the single jet cases.

The characteristics of the sulfur-doped $In_{1-x}Ga_xP$ Light emitting diode (Sulfur를 첨가한 $In_{1-x}Ga_xP$의 발광 다이오드 특성)

  • Cho, M.W.;Moon, D.C.;Kim, S.T.
    • Proceedings of the KIEE Conference
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    • 1988.11a
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    • pp.168-171
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    • 1988
  • The p-n homo junction diode of the III-V ternary alloy semiconductor $In_{1-x}Ga_xP$ : S grown by the temperature gradient solution (TGS) was fabricated by Zn-diffusion, and it's characteristics was investigated. The carrier concentration of $In_{1-x}Ga_xP$ doped with sulfur, 0.5 mol %, was $1{\times}10^{17}cm^{-3}$ and the mobility was varied with the composition. In the case that the diffusion time was constant as 30 minutes. The temperature dependence of diffusion coefficient was decreased from D= $4.2{\times}10^{-5}$ exp (-1.74/$k_{B}T$) to D= $2.5{\times}10^{-5}$ exp (-3.272/$k_{B}T$) with increasing of composition $\times$ from 0.43 to 0.98. The major peak of E.L spectrum was due to D-A pair recombination and the peak intensity was increased with the increasing of input current. And the E.L intensity was decreased with the increasing temperature, and shift to the long wavelength. The luminescence efficiencies measured at $5^{\circ}C$, atmosphere temperature, was decreased from $2.6{\times}10^{-4}$% to $9.49{\times}10^{-6}$ % with increasing of composition it from 0.39, direct transition region, to 0.98, indirect transition region.

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Parametric Study on the Aerodynamic Drag of Ultra High-speed Train in Evacuated Tube - Part 2 (진공튜브 내 초고속열차의 공기저항 파라메타 연구 - 2)

  • Kwon, Hyeok-Bin;Nam, Seong-Won;Kim, Dong-Hyeon;Jang, Yong-Jun;Kang, Bu-Byoung
    • Journal of the Korean Society for Railway
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    • v.13 no.1
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    • pp.51-57
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    • 2010
  • The aerodynamic drag of ultra high-speed train in evacuated tube have been calculated using computational fluid dynamics and the variation of aerodynamic drag for the change of major system parameter of tube-vehicle system such as the train speed, air density, and the tunnel diameter. The aerodynamic drag in the tube increases with increasing train speed, however, the ratio of drag increase in tube is larger than that on the open field, the V square rule. The aerodynamic drag decreases with increasing tunnel diameter and increasing air density, and the drag increasing for air density is almost linear just like that on open field. For some combination of the parameters, the trend of aerodynamic drag of train showed irregularity.

Study on Some Physico-chemical Properties of Cigarette Filter Rods by Triacetin Content (Triacetin 함량에 따른 담배필터의 이화학적 특성에 관한 연구)

  • 김종열;신창호;김정열;김영호;이근회
    • Journal of the Korean Society of Tobacco Science
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    • v.19 no.2
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    • pp.129-135
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    • 1997
  • This study was carried out to investigate the influence of triacetin(TA) on some phisico-chemical properties of cigarette filter rods. To find the effect of TA on physical properties, we made six kinds of filters varying the TA levels(0%, 2%, 4%, 6%, 8%, 10%) and measured the hardness, resilience and roundness. The hardness of filter rods was increased from 83.2% to 94.6% with increasing the TA level hut the roundness was not affected by TA levels. After manufacturing the cigarette with the filters, we have analysed the delivery amount of phenol and TA with the content of TA. The amount of phenol was decreased from 20.6$\mu\textrm{g}$/cig. to 12.0 $\mu\textrm{g}$/cig. with increasing the TA level of the filters. The decreasing of phenol amount was thought to be caused by solution effect. Also the TA delivery of TPM was increased from 0% to 5% of TPM with increasing the amount of TA. We have found the interesting phenomena that ventilation rate was also decreasing up to 6oye with increasing TA. It seemed to be due to the encapsulated pressure drop and the reduction of the plugwrap porosity which also caused by the smear with TA on the surface of plugwrap. From this results, we could find that not only the hardness, resilience and ventilation rate but also the contents of phenol and TA in cigarette smoke was affected by the TA levels on the cigarette filter rods.

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Thermal Properties of Semiconductive Materials(Shield) by Sonic Impurities in Carbon Black (카본블랙내 이온성 불순물들에 따른 반도전 재료(층)의 열적특성)

  • Lee Yong-Sung;Choi Yong-Sung;Park Dae-Hee;Lee Kyoung-Yong
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.54 no.4
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    • pp.149-153
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    • 2005
  • We have investigated thermal properties showed by changing the content of carbon black which is the component parts of semiconductive shield in underground power transmission cable. Specimens were made of sheet with the nine of those for measurement. Heat capacity (${\Delta}$H), glass transition temperature (Tg) and melting temperature (Tm) were measured by DSC (Differential Scanning Calorimetry). The ranges of measurement temperature were from -100($^{\circ}C$) to 100($^{\circ}C$), and heating rate was 4($^{\circ}C$/min). And then thermal diffusivity was measured by LFA 447. The dimension of measurement temperature was 25[$^{\circ}C$]. Glass transition temperature of specimens was showed near -25[$^{\circ}C$] and the heat capacity and the melting temperature from the DSC results were simultaneously decreased according to increasing the content of carbon black, while thermal diffusivity was increased according to increasing the content of carbon black. Because ionic impurities of carbon black having Fe, Co, Mn, Al and Zn are rapidly passed kinetic energy increasing the number of times breaking during the unit time with the near particles according to increasing vibration of particles by the applied heat energy.

Thermal Properties According to Ionic Impurities of Semiconductive Material in Power Cable (전력케이블에서 반도전 재료의 이온성 불순물에 따른 열적 특성)

  • Lee, Kyoung-Yong;Choi, Yong-Sung;Park, Dae-Hee
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.12
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    • pp.1326-1331
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    • 2004
  • In this paper, we have investigated thermal properties and Impurities content of specimens showing by changing the content of carbon black that is semiconductive materials for underground power transmission. Specimens were made of sheet form with the three of existing resins and the nine of specimens for measurement. Impurities content of specimens was measured by ICPAES(Inductively Coupled Plasma Atomic Emission Spectrometer). Heat capacity(ΔH) and melting temperature(Tm) were measured by DSC(Differential Scanning Calorimetry). The ranges of measurement temperature were from $0^{\circ}C$ to 20$0^{\circ}C$, and heating temperature was 4$^{\circ}C$/min. And then thermal diffusivity was measured by LFA 447. The measurement temperature was $25^{\circ}C$. Impurities content was highly measured according to increasing the content of carbon black from ICPAES results. And heat capacity and melting temperature from the DSC results were simultaneously decreased according to increasing the content of carbon black, while thermal diffusivity was increased according to increasing the content of carbon black. Because ionic impurities of carbon black containg Fe, Co, Mn, Al, and Zn were rapidly increasing kinetic energy by vibration of ionic impurities through the applied heat energy.