• Corrosion Science and Technology
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• v.20 no.6
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• pp.426-434
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• 2021

The effect of two different annealing temperatures on the level of the second phase precipitated in the microstructure and the corrosion behaviors of super austenitic stainless steel were examined. The sample annealed at a higher temperature had a significantly lower fraction of the sigma phase enriched with Cr and Mo elements, showing more stable passivity behavior during the potentiodynamic polarization measurement. However, after the welding process with Inconel-type welding material, severe corrosion damage along the interface between the base metal and the weld metal was observed regardless of the annealing temperature. This was closely associated with the precipitation of the fine sigma phase with a high Mo concentration in the unmixed zone (UMZ) during the welding process, leading to the local depletion of Mo concentrations around the sigma phase. On the other hand, the fraction of the newly precipitated fine sigma phase in the UMZ was greatly reduced by post-weld heat treatment (PWHT), and the corrosion resistance was greatly improved. Based on the results, it is proposed that the alloy composition of welding materials and PWHT conditions should be further optimized to ensure the superior corrosion resistance of welded super austenitic stainless steel.

• Proceedings of the KWS Conference
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• 2007.11a
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• pp.42-44
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• 2007

Methods of repair welding are different to production welding for welding position, welding process, welding power source, heating methods. This study investigated proper the welding process used the welding process SMAW and GTAW in the weldment of inconel filler metals. Mechanical test showed that SMAW and GTAW process had higher mechanical properties than those of material specification. Both SMAW and GTAW welding process can appy the repair welding. In comparison, GTAW welding process had more higher mechanical properties in the weldment.

• Journal of Aerospace System Engineering
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• v.8 no.1
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• pp.24-29
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• 2014

Turbopump is typically an assembly of rotors and casings, and there are a number of joints between them. Every joint should be leak-proof, so there is always a seal to accomplish the goal. Among various seals, metal seals are advantageous in that they are robust at high pressure, and at wide range of temperature. On the other hand, they require very high tightening forces, so that flanges, bolts and nuts should be carefully designed to ensure structural integrity and to prevent detrimental yielding of components. In this study, flange joints using conical seals made of stainless steel, solid flat metal seals made of copper and metal C-seals made of Inconel 718 were structurally designed and analyzed, considering both initial tightening and operating conditions.

• Journal of the Korean institute of surface engineering
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• v.31 no.6
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• pp.334-344
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• 1998

Yew coating pmccss t.o form a surface layer ol CrN phasc on mild steel (A81 1020!, AlSI Hi3, 1Cr-0.5Mo steel (ASTM A213 and Nickrl-base superalloy (Inconel 718) was developed. Surlaces of various alloys t,n.ateii by chromizing for the formation ol Cr diffusion layer was subsequently trcaled by plasma nitriding in order t.o form the hard CrS coating layer on the surfaces. This duplex plasma surface tri-atments of chromizing and plasma nitriding have induced a lormation of a duplex-lrcated surfacr hyer of approximat~ls 70-80 $\mu\textrm{m}$thickncss with a iargcly improved microiiardnrss up to approxiniateW 1500Hv(50gf). The main cause for the lage improvment in the surface hardncss is altribilted to [.he fact that CrN and $Fe_xN$ phases are created successfully by ccliromizins and plasma nilriding treatment. High tenipera1,urc wear resislance of the duplex-treated mild steel and HI3 steels at $600^{\circ}C$ was examined. Comparing the duplex-treated specimens with the specimens treated only by chromizing, the rcsults shovmi that, thc wear volume of the duplex-treated mild skcl and 1113 stcel aSt.er a wear test, at $600^{\circ}C$ were reduced hy a Iactor of 8 and 3, respectively. Characteristics of the CrS phase by duplrx treatment were compared with $CrN_x$,/TEX> film by ion plating and the wear behaviors of CrN film lormed by two different nroccsses arc nea.riy identical.

• Korean Journal of Materials Research
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• v.11 no.12
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• pp.1052-1056
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• 2001

Pure tantalum powder has been produced by sodium as a reluctant, $K_2TaF_7$as a feed material and KCl/KF as a diluent in an inconel stainless steel bomb by the metallothermic reduction. The influence of experimental variable, such as temperature of reduction on the yield and characteristics of the Ta powder has been studied. As the temperature of the reduction was varied from$ 800{\circ}C~980{\circ}C$, the yield of tantalum powder increased from 41% to 56%. However no appreciable improvement was observed above$920{\circ}C$. The fraction of fine Ta Powder decreased appreciably with the increase of temperature, and particle size was$2~3{\mu}m$at reduction temperature of$920{\circ}C$.Therefore a reduction temperature of$920{\circ}C$was optimally fixed for subsequent runs.

• Journal of the Korean Society of Industry Convergence
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• v.23 no.5
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• pp.817-823
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• 2020

In recent, the machining of difficult-to-cut materials such as titanium alloys, stainless steel, Inconel, ceramic, glass, and carbon fiber reinforced plastics (CFRP) used in aerospace, automobile, medical industry is actively researched. Abrasive waterjet is a non-traditional processing method in which ultra-high pressure water and abrasive particles are mixed in a mixing chamber and shoot out jet through a nozzle, and removed by erosion due to collision with a material. In particular, the nozzle of the abrasive waterjet is one of the most important parts that affect the machining quality as with a cutting tool in general machining. It is very important to monitor the condition of the nozzle because the workpiece is uncut or the surface quality deteriorates due to wear, expanding of the bore, damage of the nozzle and clogging of the abrasive, etc. Therefore, in this paper, we propose a monitoring system based on Acoustic Emission(AE) sensor that can detect nozzle condition in real time during AWJ processing.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.5
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• pp.532-537
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• 2004

FEF(Focused Electromagnetic Field) technique was newly developed that is based on the induction principle exciting electromagnetic field. The technique consists of an induction wire and a sensor for detecting electromagnetic field, and is applied in a non-contact mode. In this study, the technique was applied to the evaluation of EDM slits in some conductive materials - aluminum alloy, stainless steel and Inconel alloy. The voltage in the non-defect region is depended upon the measurement lift-off. The voltage signals on defects are measured with peak values, and the peak values changed with the depth of defects. The voltage distributions for all conductive materials are the same trend.

• Journal of the Korean Society of Propulsion Engineers
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• v.17 no.6
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• pp.105-112
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• 2013

Turbopump is typically an assembly of rotors and casings, and there are a number of joints between them. Every joint should be leak-proof, so there is always a seal to accomplish the goal. Among various seals, metal seals are advantageous in that they are robust at high pressure, and at wide range of temperature. In this study, flange joints using conical seal made of stainless steel, solid flat metal seal made of copper and metal C seal made of Inconel 718 were structurally designed and analyzed, considering both initial tightening and operating conditions.

• Transactions of the Korean hydrogen and new energy society
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• v.31 no.3
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• pp.284-292
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• 2020

In this study, hydrogen charging was conducted for API X70 steel by the electro-chemical hydrogen charging method. Right after hydrogen was diffused from the specimen surface to the inside of the X70, the small punch tests and hydrogen concentration analysis was conducted within 5 minutes. Hydrogen was analyzed by melting the whole specimen and detect the gas after melting. Mechanical properties were measured by the small punch (SP) testing. Fracture surface and specimen surface were observed using scanning electron microscope. Three tests were repeated for study sensitivity of the SP test results under a same charging condition. It was observed that the variation of the maximum load, SP displacement at failure, hydrogen concentration as the charging period was not much in the case of X70 as the other steel such as Inconel. It can be argued that X70 base metal may have high hydrogen damage resistance and hydrogen diffusion in the base metal would not cause much embrittlement. Limitations of the SP test with 0.5 mm thickness for hydrogen damage test for X70 were discussed.

• Plant Journal
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• v.4 no.2
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• pp.60-65
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• 2008

As the operating conditions in a supercritical oxidation reactor are set in high temperature with high pressure causing a reactor suffering from the harsh circumstances. It means the reactor adopts itself with Fe-Cr alloy in acidic atmosphere with low pH value and Ni alloy in basic atmosphere with high pH value due to its superior corrosion resistance. The study, whose target waster water is pertinent to the latter part, has selected Ni alloy such as ostenite type stainless steel 304 and 316, superstainless steel AL6XN, Inconel 625, MAT 21, and titanium Gr. 5 in order to measure corrosion resistance against those samples under the same conditions of temperature and pressure applied for a supercritical oxidation reactor. The result shows the identifiable difference in corrosion resistance by observing the surface states through a scanning probe microscope as well as measuring the weight loss through making the samples above deposited in wastewater for two-week and four-week stay. The purpose of this corrosion experiment is to identify the most corrosion-resistant material among sample species pre-selected according to pH concentration of wastewater in pursue of applying for a reactor exposed to the extreme corrosion environment. It is because such a reactor made of a verified material enables to safeguard a stable operation under the supercritical wastewater processing facility.