• 제목/요약/키워드: In-situ measurements

검색결과 524건 처리시간 0.032초

Semi-Automatic Hydride Generation and Atomic Absorption Determination of Bismuth with in situ Concentration in a Graphite Furnace

  • Yong-Keun Lee;Dong Soo Lee;Byung Mok Yoon;Hoon Hwang
    • Bulletin of the Korean Chemical Society
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    • 제12권3호
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    • pp.290-295
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    • 1991
  • A semi-automatic method for the determination of dissolved bismuth at parts per trillion levels is described. The method involves bismuthine generation, in situ collection of bismuthine in a graphite furnace, and atomic absorption detection. In order to facilitate semi-automation of bismuthine generation and separation from aqueous solution, Gore-tex microporous PTEE membrane is used. The absolute detection limit, taken as three times the standard deviation of the instrument noise is 2 pg. The precisions are 3.1% for 100 pg and 1.9% for 1 ng of bismuth, respectively. As many as 90 measurements can be made in an hour.

Back Analysis of Displacements Measured During Excavation of Underground Storage Caverns

  • Lee, Chung-In;Lee, Youn-Kyou;Kim, Chee-Hwan
    • 한국지반공학회지:지반
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    • 제12권3호
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    • pp.83-98
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    • 1996
  • 이 논문에서는 역순법 원리를 이용한 역해석 결과를 제시하였다. 국내에서 건설된 두 곳의 지하비축기지 공사 중에 계측한 자료를 이용하여 비축기지 진입터널 주위 암반의 변형계수와 초기 지압을 계산하였다. 역해석에서 얻어진 결과를 입력자를로 하여 유한요소해석을 수행하였으며 그 결과를 계측치와 비교, 검토하였다.

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미고결 퇴적암층에서의 현장타설말뚝 지지력 특성 연구 (Bearing Capacity of In-situ Cast Piles in Weak Sedimentary Rocks)

  • 심동현;김기섭;유석준
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2004년도 춘계학술발표회
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    • pp.100-109
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    • 2004
  • Is this study, results of static pile load tests of in-situ cast piles in weak or uncemented sedimentary rock layers have been analyzed and presented. Consdierations on the characteristics of soils sedimentary rocks have been made. From the measurements of strain gauges and extensometers the relationship of unit skim friction versus displacement and that of unit end bearing versus displacement have been obatined to verity the characteristics of bearing capacity of this uncemented sedimentary rock layers. Also, a comparison has been made between ultimate skin friction in compression and tension.

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Optical Interferometry as Electrochemical Emission Spectroscopy of Metallic alloys in Aqueous Solutions

  • Habib, K.;AI-Mazeedi, H.
    • Corrosion Science and Technology
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    • 제2권6호
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    • pp.277-282
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    • 2003
  • Holographic interferometry, an electromagnetic method, was used to study corrosion of carbon steel, aluminum and copper nickel alloys in NaOH, KCI and $H_2SO_4$ solutions respectively. The technique, called electrochemical emission spectroscopy, consisted of in-situ monitoring of changes in the number of fringe evolutions during the corrosion process. It allowed a detailed picture of anodic dissolution rate changes of alloys. The results were compared to common corrosion measurement methods such as linear polarization resistance measurements and electrochemical impedance spectroscopy. A good agreement between both data was found, thus indicating that holographic interferometry can be a very powerful technique for in-situ corrosion monitoring.

Effect of Various Supports on the Physico-chemical Properties of V-Sb Oxides in the Oxidative Dehydrogenation of Isobutane

  • Shamilov, N.T.;Vislovskiy, V.P.
    • 대한화학회지
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    • 제55권5호
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    • pp.812-818
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    • 2011
  • [ $V_{0.9}Sb_{0.1}O_x$ ]systems, bulk and deposited on different supports (five types of ${\gamma}$-aluminas, ${\alpha}$-alumina, silica-alumina, silica gel, magnesium oxide), have been tested in the oxidative dehydrogenation (ODH) of iso-butane. This statement is derived from the data obtained by a set of characterisation techniques(specific surface area measurements, X-ray diffraction, X-ray photoelectron spectroscopy, laser Raman spectroscopy, in situ differential scanning calorimetry and in situ diffuse reflectance-absorption infrared Fourier transform spectroscopy).

10RT급 공기열원 열펌프의 현장 성능측정 및 예측 (In-situ Performance Test and Prediction of a 10 RT Air Source Heat Pump)

  • 김영일;백영진;장영수
    • 설비공학논문집
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    • 제14권3호
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    • pp.221-230
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    • 2002
  • In this study, in-situ performance test of an air source heat pump which has a arted capacity of 10 RT is carried out. Since test conditions, such as indoor and outdoor air conditions cannot be controlled to satisfy the standard test conditions, experiments are done with the inlet air conditions as they exist. To estimate the performance for other conditions, he heat pump is modeled with a small number of selected parameters. The values of the parameters are determined from the few measurements measured on-site during normal operation. A simulation program is developed to calculate cooling capacity and power consumption t any other operating conditions. The simulation results are in good agreement with the experiment. This study provides a method of an on-site performance diagnosis of an air source heat pump.

수압파쇄를 이용한 초기지압측정과 기존경사균열의 영향 (Estimation of in-situ Stresses and the Effect of a Preexisting Inclined Fracture by Hydraulic Fracturing)

  • 신중호;신희순;최성웅;이희근
    • 터널과지하공간
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    • 제4권1호
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    • pp.55-62
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    • 1994
  • The hydraulic fracturing in a field site was performed for the measurement of in-situ stresses. For the estimation of the effect of a preexisting inclined fracture, the test on a preexisting fracture zone was also conducted. From the measurements at three shallow depths, the ratios of max. to min. horizontal stress showed the range of 1.19-1.56 and the K values showed the range of 2.62-3.86. In case of a preexisting fracture with the inclination of 15 degrees, the stresses calculated as upper bound values by considering it. It seemed from this that the inclination less than 15 degrees had small effect on the stress calculation.

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연약지반의 강성도 측정을 위한 관입형 벤더 엘리먼트 프로브의 개발 및 적용 (Development and Application of Penetration-type Bender Elements Probe for Stiffness Measurements of Soft Soils)

  • 목영진;정재우;김학성
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2008년도 춘계 학술발표회 초청강연 및 논문집
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    • pp.119-126
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    • 2008
  • Ground stiffness(shear wave velocity) is one of the key parameters in geotechnical earthquake engineering. An In-situ seismic technique has its own advantages and disadvantages over the others in stiffness measurements. By combining the crosshole and seismic cone techniques and utilizing favourable features of bender elements, a new hybrid probe has been developed in order to enhance data quality and easiness of testing. The basic structure of the probe, called "MudFork", is a fork composed of two blades, on each of which source and receiver bender elements were mounted respectively. To evaluate the disturbance caused by the penetration of the probe, shear wave velocity measurements were carried out in the Kaolinite slurry in the laboratory. Finally, the probe was penetrated in coastal mud near Incheon, Korea, using SPT(standard penetration test)rods pushed with a routine boring machine and shear wave velocity measurements were carried out. The results were verified with data from laboratory and cone testing. The performance of the probe turns out to be excellent in terms of data quality and testing convenience.

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북동아시아 해역에서 인공위성 관측에 의한 해수면온도의 오차 특성 (Error Characteristics of Satellite-observed Sea Surface Temperatures in the Northeast Asian Sea)

  • 박경애
    • 한국지구과학회지
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    • 제29권3호
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    • pp.280-289
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    • 2008
  • 북동아시아 해역에서 10년 동안 관측된 광범위한 해양관측 자료와 인공위성 자료를 이용하여 인공위성이 관측한 해수면온도의 정확도를 평가하고 오차(인공위성 해수면온도-실측수온)의 특성을 조사하였다. 845개의 일치점 자료를 분석한 결과 위성 해수면온도 (MCSST)는 해양 관측치에 대해 0.89$^{\circ}C$의 제곱평균오차와 0.18$^{\circ}C$의 편차를 보였다. 위성 수온의 오차는 40$^{\circ}N$에서 $\pm3^{\circ}C$에 달하는 위도에 따른 의존성을 보였는데 이는 고위도 해역에 존재하는 작은 소용돌이, 해류, 열전선의 큰 시공간적 변동성과 관련 있는 것으로 판단된다. 많은 수의 위성 해수면온도 자료는 겨울철에 해양관측치보다 낮게 산출되고 여름철에는 높게 산출되는 경향이 있었다. 이러한 계절적 의존성은 인공위성 표층부이 자료가 아닌 해양조사선과 계류부이의 수온자료에서 발견되었는데 해양 상층의 수 m 이내에 강한 수직적 수온 구배가 있음을 보여준다. 본 연구는 인공위성 자료로부터 해수면온도를 산출할 때 해양 피층과 그 아래 층 사이의 수온 차이를 고려하고 보정하려는 노력이 필요함을 강조한다.

분산형 백색광 간섭계를 이용한 미세 박막 구조물의 삼차원 두께 형상 및 굴절률의 실시간 측정 (Dispersive White-light Interferometry for in-situ Volumetric Thickness Profile of Thin-film Layers and a refractive index)

  • 김영식;김승우
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.23-24
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    • 2006
  • We present a dispersive scheme of white-light interferometry that enables not only to perform tomographical measurements of thin-film layers but also to measure a refractive index without mechanical depth scanning. The interferometry is found useful particularly for in-situ 3-D inspection of micro-engineered surfaces such as liquid crystal displays, semi-conductor and MEMS structure, which requires for high-speed implementation of 3-D surface metrology.

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