• 한국분말재료학회지
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• 제2권2호
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• pp.149-157
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• 1995

In this study, an attempt was made to fabricate TiAl as well as its in situ composite via combustion synthesis. The processing variable of the combustion synthesis which include aluminum content and the heating rate were found to affect the combustion temperature. The combustion temperature measured, however, was lower than the melting temperature of TiAl and the reaction product were found to include incomplet reaction products. Carbon was added in order to increase the combustion temperature as well as to form in situ reinforcements. The reaction products showed homogeneous microstructures with carbide phases formed within indicating that the addition of carbon increased the combustion temperature above the melting temperature of TiAl.

• 한국결정성장학회지
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• 제7권3호
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• pp.494-503
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• 1997

Polyimide(PI)위에서 Cu의 초기 성장과정을 설명하기 위해, PI 위에 Cu를 조금씩 증착시키면서 그리고 PI 위에 Cu 층을 쌓아놓고 이 Cu 층을 $Ar^+$ 이온으로 깍아내면서 계면에서의 변화를 XPS를 이용하여 비교ㆍ관측하였다. 상온에서 PI위에 Cu를 조금씩 증착하면서 관측하였을 때, 그 성장과정에 따르는 phase의 변화는 Cu-N-O complex에서 $Cu_2O$ phase로, 그리고 metallic Cu 순으로 성장하는 것이 관측되었다. 반면에 PI위에 증착되어 있는 Cu를 조금씩 깎아내면서 관측하였을 때, metallic Cu가 $Ar^+$ 이온으로 깍아내어 polyimide와의 계면에 도달하게 되었을 때에는 Cu$_2$O phase로서 관측되었다. 이상의 결과로부터, in-situ로 Cu를 조금씩 올리면서 계면을 조사하는 것과 Cu를 증착시킨 후, 깍으면서 계면을 조사하는 것과는 다른 결과를 얻게 된다는 것을 알 수 있었다.

• Korea-Australia Rheology Journal
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• 제16권3호
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• pp.147-152
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• 2004

Ultrasound-assisted melt mixing was applied to blending polystyrene (PS) and low density polyethylene(LDPE). The influence of the ultrasonic irradiation on the morphology and mechanical properties of the blends was investigated. It was observed that the domain sizes of the blend were significantly reduced and phase stability was well sustained even after a thermal treatment. Such morphological feature was consistent with the improvements in mechanical performance of the blends. The desirable results of ultrasonic compatibilization are mainly attributed to the in-situ formation of PS-LDPE copolymers as confirmed by a proper separation experiment. An important relationship between ultrasonic irradiation time and mechanical properties is revealed and an issue on the thermal stability of the blend is discussed.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1290-1291
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• 2006

Fabrication of $Fe_3AlC$ matrix in-situ composite, reinforced by a FeAl phase, was studied by using the powder metallurgical processing route. Especially, in order to disperse the second phase more finely, we chose the mechanical alloying process. We investigated the microstructural and mechanical properties of the consolidated material. After consolidation by vacuum hot pressing, the compact showed almost full density and consisted of a $Fe_3AlC$ matrix and FeAl second phase (average particle size was less than 1m). The compact showed HV746, which was higher than that of the arc melted $Fe_3AlC$ monolithic material, HV603.

• 한국세라믹학회지
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• 제28권12호
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• pp.1005-1011
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• 1991

Y-Ba-Cu-O thin films were in-situ fabricated on LaAlO3(100) substrates using the second harmonics of a pulsed Nd:YAG laser. Thin films were deposited under 200 (mtorr) of oxygen atmosphere, when the substrate temperature was changed between 67$0^{\circ}C$ and 82$0^{\circ}C$. After deposition, the films were in-situ annealed at 50$0^{\circ}C$ under 2/3 bar of oxygen pressure. We showed that the deposition temperature affects the formation of superconducting phase, the resistance, and the surface morphology. The Y-Ba-Cu-O thin films deposited at 76$0^{\circ}C$ show the zero resistance critical temperature of 85 K.

• 한국지반공학회논문집
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• 제21권2호
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• pp.5-16
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• 2005

모형지반을 이용한 각종 모형말뚝실험에서 자주 문제가 되는 것이 크기효과에 따른 실험의 정량적 분석에 대한 한계성이다. 이러한 문제를 보완하기 위하여 본 연구에서는 대형의 원통형 토조에 인공지반을 제작함으로써 지반 특성에 대한 크기효과를 최소화하도록 노력하였다. 또한 지반의 자연생성과정을 재현하고 빠를 시간내에 방밀을 완펄하기 위하여 케올리나이트와 실리카를 1:1로 혼합한 슬러리를 토조에서 압밀하여 인공지반을 생성하였다. 본 연구에서 마련한 모든 인공지딴의 특성을 자세히 파악하고 실제의 지반특성과 비교하기 위하여 베인시험기, 피조프로브, 콘관입시험기 등 여러가지의 원위치 소형조사장비를 제작 및 사용하였다. 본 연구에서 행한 원위치 시험 결과, 앞선 연구에서 밝힌 시험결과와 일치하는 결과를 얻었다. 또한 인공지반에서 행한 모형실험결과와 실제 상황과의 차이를 규명함으로써 모형실험결과에 근거하여 실물의 거동을 예측하는 방법을 찾고자 차였다.

• 한국재료학회지
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• 제17권1호
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• pp.11-17
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• 2007

Turbulent in-situ mixing process is a new material process technology to get dispersed phase in nanometer size by controlling reaction of liquid/solid, liquid/gas, flow ana solidification speed simultaneously. In this study, mixing which is the key technology to this synthesis method was studied by computational fluid dynamics. For the simulation of mixing of liquid metal, static mixers investigated. Two inlets for different liquid metal meet ana merge like 'Y' shape tube having various shapes and radios of curve. The performance of mixer was evaluated with quantitative analysis with coefficient of variance of mass fraction. Also, detailed plots of intersection were presented to understand effect of mixer shape on mixing. The simulations show that the Reynolds number (Re) is the important factor to mixing and dispersion of $TiB_2$ particles. Mixer was designed according to the simulation, and $Cu-TiB_2$ nano composites were evaluated. $TiB_2$ nano particles were uniformly dispersed when Re was 1000, and cluster formation and reduction in volume fraction of $TiB_2$ were found at higher Re.

• Journal of Advanced Marine Engineering and Technology
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• 제27권7호
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• pp.889-898
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• 2003

The soot yield is studied by a premixed propane-oxygen-inert gas combustion in a specially designed disk-type constant-volume combustion chamber to investigate the effect of turbulence on soot formation. Premixtures are simultaneously ignited by eight spark plugs located on the circumference of chamber at 45 degree intervals in order to observe the soot formation under high pressures and high temperatures. The eight flames converged compress the end gases to a high pressure. The laser schlieren and direct flame photographs for observation field with 10 mm in diameter are taken to examine into the behaviors of flame front and gas flow in laminar and turbulent combustion. The soot volume fraction in the chamber center during the final stage of combustion at the highest pressure is measured by the in situ laser extinction technique and simultaneously the corresponding burnt gas temperature by the two-color pyrometry method. It is found that the soot yield of turbulent combustion decreases in comparison with that of laminar combustion because the burnt gas temperature increases with the drop of heat loss.

• 한국자동차공학회논문집
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• 제9권4호
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• pp.1-9
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• 2001

The soot yield has been studied by a premixed propane-oxygen-inert gas combustion in a specially designed disk-type constant-volume combustion chamber to investigate the effects of pressure, temperature and turbulence on soot formation. Premixtures are simultaneously ignited by eight spark plugs located on the circumference of chamber at 45 degree intervals in order to observe the soot formation under high pressures. The eight flames converged compress the end gases to a high pressure. The laser schlieren and direct flame photographs for observation field with 10 mm in diameter are taken to examine into the behaviors of flame front and gas flow in laminar and turbulent combustion. The soot volume fraction in the chamber center during the final stage of combustion at the highest pressure is measured by the in situ laser extinction technique and simultaneously the corresponding burnt gas temperature by the two-color pyrometry method. The pressure and temperature during soot formation are changed by varying the initial charge pressure and the volume fraction of inert gas compositions, respectively. It is found that the soot yield increases with dropping temperature and rising pressure at constant equivalence ratio, and that the soot yield of turbulent combustion decreases in comparison with that of laminar combustion because the burnt gas temperature increases with the drop of heat loss.

• 한국산학기술학회논문지
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• 제14권7호
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• pp.3164-3169
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• 2013

본 연구에서는 수직형 지중 열교환기의 3차원 CFD 해석 기법을 제안하여 2개소의 현장 열응답 시험과 비교하였다. CFD 해석 비교를 위해 GAMBIT을 이용하여 지중과 지중 열교환기 형상을 모델링하였으며, 상용코드인 FLUENT를 사용하여 3차원 열전달 유동 해석을 수행하였다. 2개소의 현장 열응답 시험에서 도출된 지중 유효 열전도도와 지중 초기온도를 경계조건으로 사용하였으며, 시간에 따른 지중 열교환기의 입구온도 변화는 profile을 사용하여 실제 조건을 모사하였다. CFD 해석 결과 2개소의 지중 열교환기 출구온도는 $0.5^{\circ}C$ 범위 내에서 예측하였고, 기울기는 1.6% 이내에서 적절히 예측하였다. 향후 CFD 해석 기법을 활용하여 지중 열교환기 깊이, 형상 및 배열 변화 등에 따른 성능예측에 활용하고자 한다.