• 한국식품영양학회지
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• 제10권4호
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• pp.462-467
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• 1997

최근 건조 및 탈수공정으로 사용되고 있는 침지(soaking)에 의한 방법인 DIS 공정(dewatering and impregnation soaking process)은 상온에서 침지용액에 식품시료를 담금으로서 시료내의 수분이 탈수되는 현상을 이용한 공정으로서 이 때 용액 속의 용질들이 시료 속의 세포 내로 침투하는 확산현상도 동시에 발생한다. 따라서 영양분의 손실과 관능적 품질저하를 억제할 수 있으며, 건조시의 에너지를 절감하는 등의 특성을 갖는다. DIS 공정에서는 용질의 크기에 따라 원형질막 분리현상과 세포벽 붕괴현상이 발생하며, 시료의 조직상태와 운전조건에 의하여 그 탈수 정도는 차이가 나타난다. DIS 공정을 제어하기 위한 모형화는 주로 비정상상태에서의 Fick의 법칙과 물질수지를 기초로 한 여러 가지 모델들이 제안되어 등온상태에서 시간에 따른 탈수량과 용질 침투량을 정확히 예측하고자 하고 있다.

• Design & Manufacturing
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• 제15권3호
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• pp.39-44
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• 2021

In molding of continuous fiber-reinforced thermoplastic composites, it is very difficult to impregnate between the reinforcements and the matrix since the matrix has a high melting temperature and high viscosity. Therefore, most of composite molding processes are divided in the manufacturing processes of intermediate materials called prepreg and the forming of products from intermediate materials. The divided process requires additional facilities and thermoforming, and they increase the cycle time and cost of composite products. These problems can be resolved by combining the continuous fiber-reinforced composite molding process with injection molding. However, when a composite material is manufactured by inserting woven fabric into the injection mold, poor impregnation occurs on the surface of the molded product. It affects the properties of the composites. In this paper, through an impregnation experiment using cores with different heat transfer rates and pore densities, the reason for the poor impregnation was confirmed, and molding experiments were conducted to produce composite with improved surface impregnation by inserting the mesh. And also, the surface impregnation and deformation of composites molded using different types of mesh were compared with each other.

• Journal of information and communication convergence engineering
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• 제7권1호
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• pp.72-77
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• 2009

Three different procedures for adding Pd compounds to $SnO_2$ particles have been investigated. These processes are: (1) coprecipitation; (2) dried powder impregnation; and (3) calcined powder impregnation. The microstructures of $SnO_2$ particles have been analyzed by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). In the coprecipitaion method, the process does not restrain the growth of $SnO_2$ particles and it forms huge agglomerates. In the dried powder impregnation method, the process restrains the growth of $SnO_2$ particles and the surfaces of the agglomerates have many minute pores. In the calcined powder impregnation method, the process restrains the growth of $SnO_2$ particles further and the agglomerates have a lot more minute pores. The sensitivity ($S=R_{air}/R_{gas}$) of the $SnO_2$ gas sensor made by the calcined powder impregnation process shows the highest value (S = 21.5 at 5350 ppm of $C_3H_8$) and the sensor also indicates the lowest operating temperature of around $410^{\circ}C$. It is believed that the best result is caused by the plenty of minute pores at the surface of the microstructure and by the catalyst Pd that is dispersed at the surface rather than the inside of the agglomerate. Schematic models of Pd distribution in and on the three different $SnO_2$ particles are presented.

• 한국정밀공학회지
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• 제20권7호
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• pp.78-83
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• 2003

Characterization of an ultra precision grinding plate for GMR head manufacturing is performed by measuring frictional forces between the grinding plate and the advanced ceramic Two kinds of methods of producing the precision grinding plates are presented: texturing and micro-channeling. Texturing is effective in terms of production time but micro-channeling excels in quality control. It is found that the frictional coefficient of a precision grinding plate decreases as the impregnation of diamond grain onto the precision-grinding plate progresses, and remains unchanged once the impregnation process is successfully completed, even after 100 revolutions of the precision-grinding plate against the advanced ceramic under 40 N of normal force. Therefore, the measurement of the frictional coefficient can replace costly and time-consuming process of estimating the level of impregnation of diamond grain on the precision-grinding plate, which has been performed by using scanning electron microscope, and be employed as an index to determine the level of impregnation of diamond grain.

• 공업화학
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• 제32권5호
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• pp.569-573
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• 2021

본 연구에서는 코크스, 바인더 피치 및 함침 피치를 사용하여 고밀도 탄소 블록을 제조하고, 함침 공정 시 피치의 유동성이 탄소 블록의 고밀도화에 미치는 영향을 고찰하였다. 코크스와 바인더 피치의 고압 성형을 통해 그린블록을 제조하고 열처리 공정을 통하여 탄소 블록을 얻었다. 열처리 공정 시 바인더 피치의 휘발에 의해 생성된 기공을 제거하고자 함침 공정을 진행하였다. 함침 공정은 함침 피치를 용융하는 전처리 단계와 피치를 탄소 블록에 함침하는 고압 반응 단계로 나누어 진행하였다. 함침 피치의 용융은 140~200 ℃에서 진행하였으며, 열처리 온도가 증가할수록 함침 피치의 점도가 감소하였다. 함침 피치의 점도 감소는 유동성을 향상시켜 탄소 블록 내부 기공을 효율적으로 함침하여 탄소 블록의 기공률을 83% 감소시켰고 겉보기 밀도를 5% 상승시켰다.

• 한국염색가공학회지
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• 제15권3호
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• pp.168-175
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• 2003

Ultramicrofiber(UMF) PET knitted fabric and regular PET plain woven fabric as reference sample were impregnated with waterborne polyurethane(PU) in a two-step process with dyeing/PU treatment and PU treatment/dyeing to investigate the effect of the treatment sequence. The waterborne PU impregnated fabrics were dyed with two kinds of vat and disperse dyes to investigate the dyeing properties and the dyeing fastnesses. In vat dyeing the rank of color strength(K/S) was in order of dyeing/PU impregnation > dyeing only > PU impregnation/dyeing, whereas in case of disperse dyeing, the order was dyeing/PU impregnation > PU impregnation/dyeing >dyeing only. Wash fastness of vat dyeing showed a higher 2-3 grade than disperse dyeing, while rubbing and light fastnesses were not good for disperse dyes.

• Design & Manufacturing
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• 제16권2호
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• pp.60-65
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• 2022

In the pultrusion process for the CFRP (Carbon fiber reinforced plastic) rectangular pipe, the drawing device is eseential which can continuously produces products and draws the carbon fiber tow. In addition, since the degree of cure changes depending on the temperature and the temperature ditribution of the curing mold changes depending on the pultrusion speed, the temperature distribution of the curing mold under certain conditions must be studied before processing. In this study, in the pultrusion process using a closed impregnation method, which has several advantages compared to the general pultrusion process using a open bath impregnation method, the drawing force required to pull the carbon fiber tows and the temperature distribution of the curing mold was analyzed to design the drawing device and the curing mold efficiently.

• 한국대기환경학회지
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• 제20권2호
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• pp.185-193
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• 2004

A catalyst with CuO ceramic filter for simultaneous treatment of dust and HAP was prepared and characterized. Catalytic ceramic filter can not only potentially achieve the substantial savings in energy but provide with effective optimization and integration of process for simultaneous removal of SO$_2$, NO$_{x}$ and particulates from flue gases. Catalytic ceramic filters remove simultaneously particulates on exterior surface of filters and reduce NO to $N_2$ and $H_2O$ by SCR (Selective Catalytic Reduction) process. Preparation of catalyst impregnated ceramic filter with disk shape (Ψ 50) follow the processing of alumino-silicate ceramic filter, support impregnation and catalyst impregnation (copper oxide). Preparation routes of alumino-silicate catalyst carrier suitable for production of catalytic filters practically were studied and developed using the sol-gel and colloidal processing, homogeneous precipitation and impregnation method. Characterization of the catalyst, catalyst carrier catalytic filter materials have been performed the using various techniques such as BET, XRD, TGA, SEM. Combination of the sol-gel and colloidal processing and impregnation method is recommended to prepare catalyst carriers economically for catalytic filter applications.s.

• Design & Manufacturing
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• 제14권4호
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• pp.11-16
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• 2020

In this study, forming of carbon composite parts was performed using an injection/compression molding process. An impregnation of matrix is determined by ability of wet and flow rate between the matrix and reinforcement. The flow rate of matrix passing through the reinforcements is a function of permeability of reinforcement, a viscosity of matrix and pressure gradient on molding, and the viscosity of the matrix depends on the mold temperature, molding pressure and shear strain of matrix. Therefore, compression molding experiment was conducted using a heating mold in order to confirm the possibility of matrix impregnation. The impregnation of the matrix through the porosities between the woven yarns was confirmed by the cross-sectional SEM image of compression molded parts. An injection molding process was also performed at a short cycle time, high molding pressure and low mold temperature than those of compression experiment conditions. Deterioration of impregnation on the surface of molded parts were caused by these injection conditions and it could be the reason of decreasing the maximum tensile strength. In order to improve impregnation of matrix on the surface, injection/compression molding and insert-over molding were applied. As a result of applying injection/compression molding and insert-over molding, it was shown that the improvement of impregnation on the surface and the maximum tensile strength was increased about 2.8 times than the virgin matrix.

• The Korean Journal of Ceramics
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• 제4권3호
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• pp.240-244
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• 1998

The analytical method was developed to calculate efficiency of densifying carbon/carbon (C/C) composites using coal tar pitch as a matrix precursor at each cyle. Three factors were defined in analyzing the densification process: impregnation efficiency, retention efficiency, and overall densification efficiency. The relationships developed were applied to the experimental results for three densification cycles of C/C composites with pitches as an impregnant to evaluate the factors which may depend on the impregnant and on the route of carbonization. The impregnation efficiency increased with the repeated process cycles whereas the retention efficiency decreased irrespective of the impregnant and carbonization route. Carbonization route P+A+G, in which pressure carbonizationl (P) and graphitization (G) were done before after atmospheric pressure carboniztion (A) respectively, using impregnant of high carbon yields was the most effective method in densifying C/C composites.