• Title/Summary/Keyword: Impregnation process

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Study on Dewatering and Impregnation Soaking Process (침지공정에서의 탈수 및 용질 침투현상에 관한 고찰)

  • Choe, Dong-Won;Sin, Hae-Heon;Choe, Hyeong-Taek
    • The Korean Journal of Food And Nutrition
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    • v.10 no.4
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    • pp.462-467
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    • 1997
  • The DIS process(dewatering and impregnation soaking process) are using for dewatering of food materials at room temperature. And the DIS process are resulted in diffusion process as well as dewatering phenomena. During the DIS process, plasmolysis or cytorrhysis was happened by according to solute size. A tissue state of food material was very important variables for movement of water or solute, and running conditions are important for dewatering and impregnation. And models for DIS process were fundamentally given by Fick's law at unsteady state or mass balance. For example, Bicompartmental Model was given for quantification of water loss and solid gain.

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A study on the improvement of impregnation on the surface of injection-molded thermoplastic woven carbon fabric composite (열가소성 직물탄소복합소재 사출 성형품의 표면 함침 개선에 관한 연구)

  • Jeong, Eui-Chul;Yoon, Kyung-Hwan;Lee, Sung-Hee
    • Design & Manufacturing
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    • v.15 no.3
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    • pp.39-44
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    • 2021
  • In molding of continuous fiber-reinforced thermoplastic composites, it is very difficult to impregnate between the reinforcements and the matrix since the matrix has a high melting temperature and high viscosity. Therefore, most of composite molding processes are divided in the manufacturing processes of intermediate materials called prepreg and the forming of products from intermediate materials. The divided process requires additional facilities and thermoforming, and they increase the cycle time and cost of composite products. These problems can be resolved by combining the continuous fiber-reinforced composite molding process with injection molding. However, when a composite material is manufactured by inserting woven fabric into the injection mold, poor impregnation occurs on the surface of the molded product. It affects the properties of the composites. In this paper, through an impregnation experiment using cores with different heat transfer rates and pore densities, the reason for the poor impregnation was confirmed, and molding experiments were conducted to produce composite with improved surface impregnation by inserting the mesh. And also, the surface impregnation and deformation of composites molded using different types of mesh were compared with each other.

Pd-doped $SnO_2$-based oxide semiconductor thick-film gas sensors prepared by three different catalyst-addition processes

  • Lee, Kyu-Chung;Hur, Chang-Wu
    • Journal of information and communication convergence engineering
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    • v.7 no.1
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    • pp.72-77
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    • 2009
  • Three different procedures for adding Pd compounds to $SnO_2$ particles have been investigated. These processes are: (1) coprecipitation; (2) dried powder impregnation; and (3) calcined powder impregnation. The microstructures of $SnO_2$ particles have been analyzed by X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). In the coprecipitaion method, the process does not restrain the growth of $SnO_2$ particles and it forms huge agglomerates. In the dried powder impregnation method, the process restrains the growth of $SnO_2$ particles and the surfaces of the agglomerates have many minute pores. In the calcined powder impregnation method, the process restrains the growth of $SnO_2$ particles further and the agglomerates have a lot more minute pores. The sensitivity ($S=R_{air}/R_{gas}$) of the $SnO_2$ gas sensor made by the calcined powder impregnation process shows the highest value (S = 21.5 at 5350 ppm of $C_3H_8$) and the sensor also indicates the lowest operating temperature of around $410^{\circ}C$. It is believed that the best result is caused by the plenty of minute pores at the surface of the microstructure and by the catalyst Pd that is dispersed at the surface rather than the inside of the agglomerate. Schematic models of Pd distribution in and on the three different $SnO_2$ particles are presented.

Characterization of ultra Precision Grinding Plate for GMR Head Manufacturing by Measuring Frictional Force (마찰력 측정을 통한 GMR 헤드 제작용 초정밀 연마판의 특성화)

  • 노병국;김기대
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.7
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    • pp.78-83
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    • 2003
  • Characterization of an ultra precision grinding plate for GMR head manufacturing is performed by measuring frictional forces between the grinding plate and the advanced ceramic Two kinds of methods of producing the precision grinding plates are presented: texturing and micro-channeling. Texturing is effective in terms of production time but micro-channeling excels in quality control. It is found that the frictional coefficient of a precision grinding plate decreases as the impregnation of diamond grain onto the precision-grinding plate progresses, and remains unchanged once the impregnation process is successfully completed, even after 100 revolutions of the precision-grinding plate against the advanced ceramic under 40 N of normal force. Therefore, the measurement of the frictional coefficient can replace costly and time-consuming process of estimating the level of impregnation of diamond grain on the precision-grinding plate, which has been performed by using scanning electron microscope, and be employed as an index to determine the level of impregnation of diamond grain.

Effect of Coal Tar Pitch Viscosity on Impregnation for Manufacture of Carbon Blocks with High Density (고밀도화 탄소 블록 제조 시 콜타르계 피치의 점도가 함침에 미치는 영향)

  • Cho, Jong Hoon;Hwang, Hye In;Kim, Ji Hong;Lee, Young-Seak;Im, Ji Sun;Kang, Seok Chang
    • Applied Chemistry for Engineering
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    • v.32 no.5
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    • pp.569-573
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    • 2021
  • In this study, high-density carbon blocks were manufactured using coke, binder pitch, and impregnated pitch, then the effect of pitch fluidity on the densification of carbon blocks during the impregnation process was investigated. A green block was manufactured through high-pressure figuration of coke and binder pitch, and a carbon block was obtained through a heat treatment process. An impregnation process was performed to remove pores generated by volatilization of the binder pitch during the heat treatment process. The impregnation process was carried out the high-pressure reaction step of impregnating the pitch into the carbon block followed by the pretreatment step of melting the impregnation pitch. Melting of the impregnation pitch was carried out at 140~200 ℃, and the viscosity of the impregnation pitch decreased as the heat treatment temperature increased. The decrease in the viscosity of the impregnation pitch improved the fluidity and effectively impregnated the pores inside the carbon block, reducing the porosity of the carbon block by 83% and increasing the apparent density by 5%.

Waterborne PU Impregnation and Color Fastness of Ultramicrofiber PET Knitted Fabric (폴리에스테르 초극세 편직물의 수분산 PU 함침가공 및 염색견뢰도)

  • 정동석;천태일;이문철
    • Textile Coloration and Finishing
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    • v.15 no.3
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    • pp.168-175
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    • 2003
  • Ultramicrofiber(UMF) PET knitted fabric and regular PET plain woven fabric as reference sample were impregnated with waterborne polyurethane(PU) in a two-step process with dyeing/PU treatment and PU treatment/dyeing to investigate the effect of the treatment sequence. The waterborne PU impregnated fabrics were dyed with two kinds of vat and disperse dyes to investigate the dyeing properties and the dyeing fastnesses. In vat dyeing the rank of color strength(K/S) was in order of dyeing/PU impregnation > dyeing only > PU impregnation/dyeing, whereas in case of disperse dyeing, the order was dyeing/PU impregnation > PU impregnation/dyeing >dyeing only. Wash fastness of vat dyeing showed a higher 2-3 grade than disperse dyeing, while rubbing and light fastnesses were not good for disperse dyes.

A study on the drawing device and curing mold in CFRP rectangular pipe pultrusion process using a closed impregnation method (밀폐형 함침법을 이용한 CFRP 사각 파이프 인발성형에서 인발장치 및 경화금형에 관한 연구)

  • Kang, Byung-Soo;Yoo, Hyeong-Min
    • Design & Manufacturing
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    • v.16 no.2
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    • pp.60-65
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    • 2022
  • In the pultrusion process for the CFRP (Carbon fiber reinforced plastic) rectangular pipe, the drawing device is eseential which can continuously produces products and draws the carbon fiber tow. In addition, since the degree of cure changes depending on the temperature and the temperature ditribution of the curing mold changes depending on the pultrusion speed, the temperature distribution of the curing mold under certain conditions must be studied before processing. In this study, in the pultrusion process using a closed impregnation method, which has several advantages compared to the general pultrusion process using a open bath impregnation method, the drawing force required to pull the carbon fiber tows and the temperature distribution of the curing mold was analyzed to design the drawing device and the curing mold efficiently.

Preparation and Properties of Disc Type CuO Catalyst Impregnated Ceramic Filters (디스크형 산화구리 촉매담지 세라믹필터의 제조와 물성)

  • Hong Min-Sun;Moon Su-Ho;Lee Jae-Chun;Lee Dong-Sub;Lim Woo Taik
    • Journal of Korean Society for Atmospheric Environment
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    • v.20 no.2
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    • pp.185-193
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    • 2004
  • A catalyst with CuO ceramic filter for simultaneous treatment of dust and HAP was prepared and characterized. Catalytic ceramic filter can not only potentially achieve the substantial savings in energy but provide with effective optimization and integration of process for simultaneous removal of SO$_2$, NO$_{x}$ and particulates from flue gases. Catalytic ceramic filters remove simultaneously particulates on exterior surface of filters and reduce NO to $N_2$ and $H_2O$ by SCR (Selective Catalytic Reduction) process. Preparation of catalyst impregnated ceramic filter with disk shape (Ψ 50) follow the processing of alumino-silicate ceramic filter, support impregnation and catalyst impregnation (copper oxide). Preparation routes of alumino-silicate catalyst carrier suitable for production of catalytic filters practically were studied and developed using the sol-gel and colloidal processing, homogeneous precipitation and impregnation method. Characterization of the catalyst, catalyst carrier catalytic filter materials have been performed the using various techniques such as BET, XRD, TGA, SEM. Combination of the sol-gel and colloidal processing and impregnation method is recommended to prepare catalyst carriers economically for catalytic filter applications.s.

A study on carbon composite fabrication using injection/compression molding and insert-over molding (사출/압축 공정과 인서트 오버몰딩을 이용한 탄소복합소재 성형에 대한 연구)

  • Jeong, Eui-Chul;Yoon, Kyung-hwan;Hong, Seok-Kwan;Lee, Sang-Yong;Lee, Sung-Hee
    • Design & Manufacturing
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    • v.14 no.4
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    • pp.11-16
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    • 2020
  • In this study, forming of carbon composite parts was performed using an injection/compression molding process. An impregnation of matrix is determined by ability of wet and flow rate between the matrix and reinforcement. The flow rate of matrix passing through the reinforcements is a function of permeability of reinforcement, a viscosity of matrix and pressure gradient on molding, and the viscosity of the matrix depends on the mold temperature, molding pressure and shear strain of matrix. Therefore, compression molding experiment was conducted using a heating mold in order to confirm the possibility of matrix impregnation. The impregnation of the matrix through the porosities between the woven yarns was confirmed by the cross-sectional SEM image of compression molded parts. An injection molding process was also performed at a short cycle time, high molding pressure and low mold temperature than those of compression experiment conditions. Deterioration of impregnation on the surface of molded parts were caused by these injection conditions and it could be the reason of decreasing the maximum tensile strength. In order to improve impregnation of matrix on the surface, injection/compression molding and insert-over molding were applied. As a result of applying injection/compression molding and insert-over molding, it was shown that the improvement of impregnation on the surface and the maximum tensile strength was increased about 2.8 times than the virgin matrix.

Analysis of Densification Process of Carbon/Carbon Composites with Pitch as an Impregnant

  • Oh, Seh-Min;Park, Yang-Duk
    • The Korean Journal of Ceramics
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    • v.4 no.3
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    • pp.240-244
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    • 1998
  • The analytical method was developed to calculate efficiency of densifying carbon/carbon (C/C) composites using coal tar pitch as a matrix precursor at each cyle. Three factors were defined in analyzing the densification process: impregnation efficiency, retention efficiency, and overall densification efficiency. The relationships developed were applied to the experimental results for three densification cycles of C/C composites with pitches as an impregnant to evaluate the factors which may depend on the impregnant and on the route of carbonization. The impregnation efficiency increased with the repeated process cycles whereas the retention efficiency decreased irrespective of the impregnant and carbonization route. Carbonization route P+A+G, in which pressure carbonizationl (P) and graphitization (G) were done before after atmospheric pressure carboniztion (A) respectively, using impregnant of high carbon yields was the most effective method in densifying C/C composites.

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