• Design & Manufacturing
• /
• v.15 no.3
• /
• pp.39-44
• /
• 2021

In molding of continuous fiber-reinforced thermoplastic composites, it is very difficult to impregnate between the reinforcements and the matrix since the matrix has a high melting temperature and high viscosity. Therefore, most of composite molding processes are divided in the manufacturing processes of intermediate materials called prepreg and the forming of products from intermediate materials. The divided process requires additional facilities and thermoforming, and they increase the cycle time and cost of composite products. These problems can be resolved by combining the continuous fiber-reinforced composite molding process with injection molding. However, when a composite material is manufactured by inserting woven fabric into the injection mold, poor impregnation occurs on the surface of the molded product. It affects the properties of the composites. In this paper, through an impregnation experiment using cores with different heat transfer rates and pore densities, the reason for the poor impregnation was confirmed, and molding experiments were conducted to produce composite with improved surface impregnation by inserting the mesh. And also, the surface impregnation and deformation of composites molded using different types of mesh were compared with each other.

• Journal of Korean Physical Therapy Science
• /
• v.15 no.1
• /
• pp.1-9
• /
• 2008

Background and Purpose : This study serves the purpose to present the effective way on back pain therapy for women during their pregnancy by comparing and analyzing the effects influencing on pain index, limits on daily life, and diminution of lumbar curve, when having treated for 6 weeks, dividing into therapy group, applied by decompression therapy on spine without unnecessary effects on the pregnant women and their fetus and the existent general physiotherapy group, applied on diminution of their back pain. Subject & methods : We made impregnate women of 30(25${\sim}$34years), as the subject of this study, who understood, and agreed with, this study, among pregnant women who were diagnosed as back pain. Pain intensity, limit index on daily life, and lumbar curve test, prior to experiment was implemented as paired t－test, comparison of the difference of average by each group before and after experiment was analysed as independent t－test, and statistical examination level was set up as 0.05. Results : The difference of average of pain and limit on daily life between the group, SDTG(spinal decompression therapy group), and the group, GPTG(general physical therapy group), before and after experiment was diminished as much as 44.4% and 16.79% each after completed 6 weeks' experiment, limit on daily life in both groups showed as much as 37.2% and 21.5% each, in the end, they statistically showed conspicuous difference(p<.05). Comparison of lumbar curves between both groups, SDTG and GPTG, before and after experiment, were diminished from -23.13${\pm}$4.85 to -15.66${\pm}$3.71, and there was no remarkable difference(p<.05). Conclusion : As, in this study, decompression therapy is more effective than general physical therapy with pregnancy low back pain in pain, limitation of daily life, lumbar curve.

• 한국신재생에너지학회:학술대회논문집
• /
• 2010.06a
• /
• pp.68.2-68.2
• /
• 2010

Dye-sensitized solar cells (DSSC) show great promise as an inexpensive alternative to conventional p-n junction solar cells. Investigations into the various factors influencing the photovoltaic efficiency have recently been intensified. The conventional absorber electrode in DSSC is composed of compacted or sintered $TiO_2$ nanopowder that carries an anchored organic dye. The absorbance of incident light in the DSC is realized by specifically engineered dye molecules placed on the semiconductor electrode surface ($TiO_2$). The dye absorbs light at wavelengths up to about 920nm, the energy of the exited state of the molecule should be about 1.35eV above the electronic ground state corresponding to the ideal band gap of a single band gap solar cell. The dye molecules ar adhered onto the nanostrutured $TiO_2$ electrode by immersing the sintered electrode into a dye solution, typically 3mM in alcohol, for a long enough period to fully impregnate the electrode. However, the concentrations of the dye is slightly changed due to the evaporation of the alcohol. The dye is more expensive than other materials in DSSC and related to the efficiency of DSSC. Therefore, the concentrations of the dye should be carefully measured. In this study, we investigated to the dye loading on fired $TiO_2$ powder as a function of temperature by the TG-DTA and the dye solution by UV-visible spectroscopy after the impregnation process. The dye loading is related to the porosity of the nanostructured $TiO_2$ electrode.

• The Journal of the Korea Contents Association
• /
• v.5 no.6
• /
• pp.146-151
• /
• 2005

The coral is precious and organic gemstone. It is Beautifully Red color. Coral jewelry have been used for a long time in Asia. Especially in Korea, The Coral is an traditional and popular gemstone. It is significant to get the base data for the purpose of distinguishing natural coral from imitation coral by comparing about gemmological character in this study. Color, luster, transparency, streak color, refractive index, hardness, chemical reaction, ultraviolet fluorescence, specific gravity, observation of microscope and XRD analysis were conducted for identification of natural and imitation coral. As a result, natural coral has usually $CaCO_3$ composition and calcite structure. But, it is known that imitation coral impregnate calcic and dyeing materials with pigment. And they were distinguished also from not only XRD analysis but also a few simple experiments like specific gravity, refractive index and chemical reaction. Natural coral is harder and luster then imitation coral. In breaking method, the streak color is used certification.

• Composites Research
• /
• v.28 no.5
• /
• pp.249-253
• /
• 2015

This paper reports a study on a method for achieving lightweight thermoplastic laminate composites referred to as tow spreading technology. Thickness of an unspread 12 K carbon fiber tow is reduced by increasing the tow width from 7 mm to 20 mm. The polypropylene (PP) film was used to stabilize and impregnate the spread tow, covering it into a partially consolidated prepreg: 12 K carbon fiber spread tow/PP. Laminates were fabricated from the spread tow prepreg and control laminate composites were produced from unspread tow prepreg consisting of 12 K carbon fiber and PP. The void content, tensile and flexural properties of the composite laminates were investigated. Consequently, the spread tow laminate composite exhibited lower void content and improved mechanical properties.

• 한국신재생에너지학회:학술대회논문집
• /
• 2009.11a
• /
• pp.213-216
• /
• 2009

WGS(Water Gas Shift)반응은 일산화탄소(CO)를 이산화탄소($CO_2$)로 전환하는 반응으로 일체형 수소생산시스템의 실현을 위한 고순도 수소생산에 있어서 중요한 단계이다. WGS 반응은 열역학적 평형을 고려하여 고온전이반응(HTS: High Temperature Shift)과 저온전이반응(LTS: Low Temperature Shift) 두 단계 반응으로 진행된다. 두 단계 공정의 통합을 위해 낮은 온도에서 높은 활성을 갖는 WGS 반응용 촉매 개발이 필요하다. 최근 낮은 온도에서 높은 활성을 갖는 귀금속 촉매에 다양한 담체를 적용시킨 연구가 활발히 진행되고 있다. 선행 연구 결과, Ce-$ZrO_2$ 구조는 Ce/Zr 비에 따라 다양한 특성 변화를 관찰하였다. 따라서 낮은 온도에서 높은 활성을 갖는 WGS 반응용 촉매 제조를 위해 환원성 담체인 $CeZrO_2$에 Pt 을 담지시켜 성능을 평가하였다. 제조된 모든 담체는 공침법(Co-precipitation)으로 제조 하였으며 $500^{\circ}C$에서 6시간 소성하였다. 제조된 담체에 백금(Pt)을 함침법(Incipient Wetness Impregnate)으로 담지시켰다. 특성분석은 BET를 이용하여 표면적을 측정하였다. 촉매 반응 실험조건은 $200^{\circ}C{\sim}400^{\circ}C$ 온도범위에서 기체공간속도(GHSV: Gas Hourly Space Velocity) 45,000 ml/$h{\cdot}g-cat$ 으로 혼합가스($H_2$:60%, $N_2$:20%,$CH_4$:1%,CO:9%,$CO_2$:10%)를 흘려 반응 후 배출되는 가스를 Micro-Gas Chromatography 를 이용하여 측정하였다.

• Applied Chemistry for Engineering
• /
• v.17 no.5
• /
• pp.539-546
• /
• 2006

A study on the polymerization of polyethylenedioxythiophene (PEDOT) and the carbonization process of a separator was carred out in order to apply conductive polymer PEDOT to the winding typed aluminum condenser as a solid electrolyte and a negative electrode. PEDOT was polymerized with ethylenedioxythiophene (EDOT) as a monomer and ferric-p-toluenesulfonate as an oxidizing agent. The separator of condenser element was carbonized to control its fibrous tissue for the purpose of making it easy to impregnate the PEDOT solution into the microporous etched pit of aluminum foil by preventing separator from concentrating the PEDOT solution on itself. The characteristics of condenser such as capacitance, dissipation factor, equivalent series resistance, and thermal resistance depended on a carbonization temperature and a carbonization time. It was found that a thickness and a density of the used separator were major parameters of carbonization process and the characteristics of condenser were affected by these parameters.

• Membrane Journal
• /
• v.26 no.2
• /
• pp.146-151
• /
• 2016

Sulfonated poly (arylene ether sulfone) (SPAES) random copolymers have merits such as high proton conductivity, relatively low production cost, and thermochemical resistance when applied as polymer electrolyte membranes for fuel cells. However, it is difficult to directly employ SPAES copolymers into practical fuel cell membrane applications owing to their low chemical stability and dimensional instability under harsh operation conditions. A plausible solution is to impregnate SPAES copolymers into support films (e.g., electrospun polyimide support) with interconnected pore structures and high thermochemical toughness. In this study, a SPAES copolymer with a swivel group, which induces high free volume for fast ion transport, is chosen as ionomers to prepare pore-filling membranes (PFMs). The feasibility of the resulting membranes is evaluated via membrane characterizations.

• Polymer(Korea)
• /
• v.32 no.3
• /
• pp.213-218
• /
• 2008

About 17% of historical properties in Korea were made of stones and most of them are exposed to weathering, as such that discoloring, cracking, and shattering occur from physical, chemical, mechanical, and biological effects due to outdoor placement. Proper treatments for conservation are necessary to prevent the weathering damage and to retain the original shape of stones. MMA, an acrylic monomer having low viscosity can be impregnated deep inside stones by consecutive compression and decompression process in a pressurized vessel. After the polymerization of MMA impregnate, the space inside of the stone was filled with PMMA. It is expected that water repellent and weather resistant properties will be improved because of the improved bonding of constituent materials in stones. In this study, moisture absorption, chemical resistance, and mechanical property of two domestic granites were examined after treating them with MMA for the purpose of determining the conservation value of this method that was possibly useful to the conservation of stone cultural assets.

• Conservation Science in Museum
• /
• v.14
• /
• pp.7-12
• /
• 2013

The conservation has been conducted for the fragments of an wooden boat in the Neolithic Age, excavated from Bibong-ri, Changnyeong, Korea. The vacuum-freeze drying have been applied to mostly to the small relics, such as wooden lacquerwares or small wooden goods etc.. Therefore, the large objects like a wooden boats have been treated almost by air-drying after impregnation with aqueous PEG solution. The air-drying is needed to impregnate with PEG aqueous solution during long period and run the risk of the fault generation. This report explain an example adapted for the fragments of the wooden boat by humidity-controlled drying(HCD) with slow adjusting moisture content. We did the chemical pre-treatment, PEG aqueous solution. The concentration of the aqueous solution was increased gradually from 10% to 80%. After the impregnation, the objects were dried by the HCD. The dimensional stability of the fragments after treatment was good.