• 대한금속재료학회지
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• 제56권11호
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• pp.787-795
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• 2018

The effects of tempering condition on the microstructure and mechanical properties of 30MnB5 hot stamping steel were investigated in this study. Before the tempering, hot-stamped 30MnB5 steel was composed of only ${\alpha}^{\prime}$-martensite microstructure without precipitates. After the tempering at $180^{\circ}C$ for 120 min, nano-sized ${\varepsilon}$-carbides were precipitated in the ${\alpha}^{\prime}$-martensite laths. After tempering at $250^{\circ}C$ for 60 min, cementite was precipitated along the ${\alpha}^{\prime}$-martensite lath boundaries. The cementite was also observed in the specimens tempered at $350^{\circ}C$ for 30 min and $450^{\circ}C$ for 6 min, respectively. The globular ${\alpha}$-ferrite appeared at $350^{\circ}C-30min$ tempering, and the volume fraction of ${\alpha}$-ferrite increased when the tempering temperature was increased. The yield strength increased after tempering, and it reached a peak with the tempering condition of $180^{\circ}C-120min$, due to the nano-sized precipitates in the ${\alpha}^{\prime}$-martensite lath. After the tempering, the steel's ultimate tensile strength (UTS) was decreased due to the reduction in dislocation density and C segregation to lath boundaries. The highest elongation was observed at the $180^{\circ}C-120min$ tempering condition, due to the reduction of residual stress, and the lack of precipitates along the lath boundaries. The $180^{\circ}C-120min$ tempering condition was considered to have outstanding crash performance, according to toughness and anti-intrusion calculation results. In drop tower crash tests, the 30MnB5 door impact beam tempered at $180^{\circ}C$ for 120 min showed better crash performance compared to a 22MnB5 door impact beam.

• 한국분말재료학회지
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• 제20권4호
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• pp.264-268
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• 2013

Nickel-based superalloy IN 713C powders have been consolidated by hot isostatic pressing (HIPing). The microstructure and mechanical properties of the superalloys were investigated at the HIPing temperature ranging from $1030^{\circ}C$ to $1230^{\circ}C$. When the IN 713C powder was heated above ${\gamma}^{\prime}$ solvus temperature (about $1180^{\circ}C$), the microstructure was composed of the austenitic FCC matrix phase ${\gamma}$ plus a variety of secondary phases, such as ${\gamma}^{\prime}$ precipitates in ${\gamma}$ matrix and MC carbides at grain boundaries. The yield and tensile strengths of HIPed specimens at room temperature were decreased while the elongation and reduction of area were increased as the processing temperature increased. At $700^{\circ}C$, the strength was similar regardless of HIPing temperature; however, the ductility was drastically increased with increasing the temperature. It is considered that these properties compared to those of cast products are originated from the homogeneity of microstructure obtained from a PM process.

• 한국재료학회지
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• 제15권1호
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• pp.25-30
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• 2005

The microstructural changes by hot extrusion of AZ31B magnesium alloy were observed, and the relation to the tensile property was examined. The tensile properties as oriented longitudinal(L), half transverse(HT) and long transverse(LT) to the extrusion direction were investigated at $20^{\circ}C,\;100^{\circ}C,\;200^{\circ}C,\;300^{\circ}C\;and\;400^{\circ}C$, respectively. As the results, many recrystallized small grains distributed uniformly in large banded microstructures formed along the extrusion direction. The grain size of as-extruded specimen was around $30\~150\;{\mu}m$. As increasing the test temperature the tensile and yield strength with respect to the angle between the axis of the tensile and the longitudinal direction in extrusion was decreased, but their elongation were increased and their deviation between L and LT specimens have disappeared from $300^{\circ}C$. This mechanical anisotropy was reduced at elevated temperatures and almost disappeared at $400^{\circ}C$. It was considered that the homogenization was occured by the recrystallization and the change of slip system was occurred during tensile test process in elevated temperatures.

• 한국재료학회지
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• 제28권7호
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• pp.391-397
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• 2018

This study deals with the microstructure and tensile properties of 700 MPa-grade high-strength and seismic reinforced steel bars. The high-strength reinforced steel bars (600 D13, 600 D16 and 700 D13 specimens) are fabricated by a TempCore process, while the seismic reinforced steel bar (600S D16 specimen) is fabricated by air cooling after hot rolling. For specimens fabricated by the TempCore process, the 600 D13 and 600 D16 specimens have a microstructure of tempered martensite in the surface region and ferrite-pearlite in the center region, while the 700 D13 specimen has a microstructure of tempered martensite in the surface region and bainite in the center region. Therefore, their hardness is the highest in the surface region and shows a tendency to decrease from the surface region to the center region because tempered martensite has a higher hardness than ferrite-pearlite or bainite. However, the hardness of the 600S D16 specimen, which is composed of fully ferrite-pearlite, increases from the surface region to the center region because the pearlite volume fraction increases from the surface region to the center region. On the other hand, the tensile test results indicate that only the 700 D13 specimen with a higher carbon content exhibits continuous yielding behavior due to the formation of bainite in the center region. The 600S D16 specimen has the highest tensile-to-yield ratio because the presence of ferrite-pearlite and precipitates caused by vanadium addition largely enhances work hardening.

• 한국식품저장유통학회지
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• 제8권3호
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• pp.302-307
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• 2001

파쇄한 재료와 젖산균 스타터를 사용하여 김치를 숙성시킨 후 열풍건조 (HAD) 및 동결건조 (FD)를 행하고, 성형압력 (100, 150, 200 kg/cm2)과 성형시간별 (0, 1, 2, 3, 4분)로 제조한 김치타블궷 (KT)의 붕해성과 여백의 특성, 텍스쳐, 객도, 흡습성 및 관능적 품질을 조사하였다. FD-KT의 성형압력의 증가에 따른 붕해성은 큰 차이를 보이지 않았으나 HAD-KT는 크게 감소하였으며, FD-KT는 HAD-KT에 비하여 붕해성이 높았다. KT 수용액의 pH는 건조방법과 성형압력에 따른 차이를 보이지 않았으나 산도와 총당은 HAD-KT가 FD-KT에 비하여 낮았다. KT의 max, yield, strength 및 hardness는 HAD-KT가 FD-KT에 비하여 높았다. FD-KT는 HAD-KT에 비하여 다소 낮은 적색도를 보였으나 백색도는 높았다. KT의 색상, 촉감, 향미, 씹는 맛 및 기호도는 전반적으로 FD-KT가 높은 값을 나타내었다. 흡습성은 FD-KT가 HAD-KT에 비하여 성형압력에 관계없이 높았다. HAD-KT는 성형압력과 성형시간이 증가함에 따라 흡습량이 감소하였으나 FD-KT는 흡습량이 증가되었다. 품질특성을 종합한 결과 FD-KT, HAD-KT 다같이 성형 압력은 200kg$\textrm{cm}^2$에서 우수하였으며 성형시간은 3분이 적합하였다.

• 한국재료학회지
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• 제33권10호
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• pp.393-399
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• 2023

In this study, changes in the microstructure and mechanical properties of cast and extruded Al-2Li-1Ce alloy materials were investigated as the Mg content was varied. The density decreased to 2.485, 2.46 and 2.435 g/cm³ when the Mg content in the Al-2Li-1Ce alloy was increased to 2, 4 and 6 wt%, respectively. Intermetallic compounds of Al₁₁Ce₃ were observed in all alloys, while the β-phase of Al₃Mg₂ was observed in alloys containing 6 wt% of Mg. In the extruded material, with increasing Mg content the average grain size decreased to 84.8, 71.6 and 36.2 ㎛, and the fraction of high-angle grain boundaries (greater than 15°) increased to 82.8 %, 88.6 %, and 91.8 %, respectively. This occurred because the increased Mg content promotes dynamic recrystallization during hot extrusion. Tensile test results showed that as the Mg content increased, both the yield strength and tensile strength increased. The yield strength reached 86.1, 107.3, and 186.4 MPa, and the tensile strength reached 215.2, 285, and 360.5 MPa, respectively. However, it is worth noting that the ductility decreased to 27.78 %, 25.65 %, and 20.72 % as the Mg content increased. This reduction in ductility is attributed to the strengthening effect resulting from the increased amount of dissolved Mg, and grain refinement due to dynamic recrystallization.

• 한국재료학회지
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• 제9권9호
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• pp.865-871
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• 1999

지르콘 쉘 몰드를 제조하여 소결 온도 및 시간에 따른 소결거동이 기계적특성에 미치는 영향을 관찰하였다. $1000^{\circ}C$에서 1.5시간동안 소결 한 쉘 몰드의 1차 코팅 표면층에서 미세균열의 크기 및 수가 극대화되었으며 소결온도 및 시간이 증가할수록 상온강도와 기공의 비표면은 감소하였다. 1차 소결 후 $1500^{\circ}C$에서 4시간동안 소결 처리한 주형의 고온변형거동은 백업층과 하중의 역방향으로 스터코와 지르콘 슬러리의 경계면을 따라 변형이 발생하였다. 1차 코팅층에서 알루미나 스터코와 지르콘 슬러리의 열팽창계수 차이와 백업 코팅층에서 지르콘 슬러리간의 입도 차이가 고온변형시험 중 역변형을 일으킨 것으로 판단된다.

• 한국정밀공학회지
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• 제26권5호
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• pp.48-56
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• 2009

In this paper, laser-assisted machining(LAM) has been employed to machine hot isostatically pressed (HIPed) Si3N4 work pieces. Due to little residual flaws and porosity, HIPed $Si_3N_4$ work pieces are more difficult to machine compared to normally sintered $Si_3N_4$ workpieces. In LAM, the intense energy of laser was used to enhance machinability by locally heating the workpiece and thus reducing yield strength. In experiments, the laser power ranges from 200W to 800W and the diameter of work pieces is 16mm. While machining, the surface temperature was kept nearly constant by laser heating except for a short period of rise time of max. 58 seconds. Results showed as feed rate increases the surface temperature of $Si_3N_4$ workpieces decreases slightly, whereas the effect of depth of cut is disregardable. With a laser power of 800W, achievable maximal depth of cut as 0.7mm and feed rate was 0.03mm/rev.

• 대한기계학회논문집A
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• 제20권7호
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• pp.2257-2265
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• 1996

In the cold rolling mill, it is very important that a constrained static flow stress of rolled strip and rolling force calculation model be exactly considered to improve an prediction accuracy for rolling forces. Therefore, in this study, the values of the constrained static flow stress are used by deriving the regression equation which is a function of rolling conditions(FDT, CT) and chemical compositions(C, Si, Mn), previously applied by making the tables of yield strength for hot coils with size. And with the consideration that an elastic deformation part of an rolled strip appears at the entry and delivery side of the contacting area between the work roll and rolled strip is calculated. By applying these methods, the more accurate prediction for rolling force is obtained. As a results, the deviation of thickness is significantly reduced in the rolling direction.

• Journal of the Korean Wood Science and Technology
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• 제26권1호
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• pp.29-37
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• 1998

Alkali-soluble extracts were prepared from medium-sized barks of Radiata pine(Pinus radiata). There are difficulties in the production of extracts with uniform quality and in the preparation of adhesives with suitable viscosity. Ultrafiltration using an Amicon cell was subjected to fractionate extracts according to molecular sizes in order to overcome the above problem. The filtration efficiency was studied by using thin channel filtration systems. Adhesive manufacturing was also examined. Removal of particles greater than 0.45m from the extracts increased both filtration speed (flux) and yields of solids in the filtrates. Ultrafiltration with PM 10 membrane was very effective to fractionate and concentrate the extracts. Stiasny precipitates from the filtrates obtained by PM 10 membrane were very lower than that(83%) of the retentates. This ultrafiltration method was efficient for obtaining high yield purified phenolic compounds(mainly polyflavanoids) and thus important for preparing wood adhesives from barks. The extracts were shown excessive high viscosities at the concentrations required for adhesive formulation, but this high viscosity and short gelation time was reduced by lowering pH of the extracts and addition of urea. The highest bonding strength of plywoods(340g/$m^2$ of adhesive spreads) was achieved with adhesive formulated by 100parts of mixed alkali extracts and urea(70/30,w/w), 10parts of p-formaldehyde and 3.5parts of wheat flour at pH 6, and by hot pressing at the conditions of 12kg/$cm^2$ at $120^{\circ}C$ for 10 minutes.