• 제목/요약/키워드: Homogeneous group

검색결과 396건 처리시간 0.025초

방전 플라즈마 소결법으로 제작한 Mo-Cu 합금의 열적, 전기적 특성 (A Study on the Thermal and Electrical Properties of Fabricated Mo-Cu Alloy by Spark Plasma Sintering Method)

  • 이한찬;이붕주
    • 전기학회논문지
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    • 제66권11호
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    • pp.1600-1604
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    • 2017
  • Mo-Cu alloys have been widely used for heat sink materials, vacuum technology, automobile and many other applications due to their excellent physical and electronic properties. Especially, Mo-Cu composites with 5~20 wt% copper are widely used for the heavy duty service contacts due to their excellent properties like low coefficient of thermal expansion, wear resistance, high temperature strength and prominent electrical and thermal conductivity. In most of the applications, high dense Mo-Cu materials with homogeneous microstructure are required for high performance, which has led in turn to attempts to prepare ultra-fine and well-dispersed Mo-Cu powders in different ways, such as spray drying and reduction process, electroless plating technique, mechanical alloying process and gelatification-reduction process. However, most of these methods were accomplished at high temperature (typically degree), resulting in undesirable growth of large Cu phases; furthermore, these methods usually require complicated experimental facilities and procedure. In this study, Mo-Cu alloying were prepared by planetary ball milling (PBM) and spark plasma sintering (SPS) and the effect of Cu with contents of 5~20 wt% on the microstructure and properties of Mo-Cu alloy has been investigated.

경수로에 대한 다차원 노심 동특성 방정식의 해를 구하기 위한 새로운 방법 개발 (A New Approach for the Solution of Multi-Dimensional Neutron Kinetics Equations in LWR's)

  • Song, Jae-Woong;Kim, Jong-Kyung
    • Nuclear Engineering and Technology
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    • 제24권3호
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    • pp.252-262
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    • 1992
  • 시간 및 공간 종속형 중성자 수송 방정식으로부터 비균질 원자로 노심해석의 효율적인 방법을 개발하였다. 이를 위해 계산 시간을 단축하고 각 집합체 크기의 소격격자(coarse mesh)에 대한 평균 중성자속을 정확히 예측할 수 있도록 노달방법(nodal method)을 도입하였고, 노드 별 평균 중성자속과 노드 각 경계면의 평균 중성자속 및 유속(flux and current)과의 관계식을 얻기 위하여 조정 인자( correction factor)로서 불연속인자(discontinuity factor)를 사용하였으며, 이 인자는 이전 시간대(previous time step)의 노드 평균 중성자속, 확산계수, 그리고 불연속인자 등에 따라 새로이 계산(updating)된다. 본 논문에서 개발된 방법을 시간에 따라 비교적 단순히 변하는 과도 노심(TWIGL)과 급격한 중성자 거동의 변화를 모사하는 과도 노심(LRA)에 적용한 결과 정확성 및 효율성이 입증되었 다.

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백색소음이 대학생의 수면의 질, 우울 및 스트레스에 미치는 영향 (The Effects of White Noise on Sleep Quality, Depression and Stress in University Students)

  • 김근면;김은주
    • 가정∙방문간호학회지
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    • 제24권3호
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    • pp.316-324
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    • 2017
  • Purpose: This study was conducted to investigate the effect of white noise on sleep quality, depression, and stress in college students. Method: This study was designed a randomized controlled design to measure the effect of white noise on college students' sleep quality, depression, and stress. Data collection was conducted from May 15, 2017 to June 5, 2017. The subjects were randomly assigned to 27 college students and 28 control volunteers. Data analysis was done using SPSS 23.0 Windows program. Results: The experimental and control groups were homogeneous in general characteristics and study variables. The white noise group showed statistically significant effects on stress(t=-2.25, p=.015) and sleep quality(t=0.65, p<.001). Conclusion: This study confirms that white noise has a positive effect on stress and sleep of college students. Based on these results, it is expected that further research will be conducted on systematic and differentiated white noise mediation.

Multi-Nuclear NMR Investigation of Nickel(II), Palladium(II), Platinum(II) and Ruthenium(II) Complexes of an Asymmetrical Ditertiary Phosphine

  • Raj, Joe Gerald Jesu;Pathak, Devendra Deo;Kapoor, Pramesh N.
    • 대한화학회지
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    • 제57권6호
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    • pp.726-730
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    • 2013
  • Complexes synthesized by reacting alkyl and aryl phosphines with different transition metals are of great interest due to their catalytic properties. Many of the phosphine complexes are soluble in polar solvents as a result they find applications in homogeneous catalysis. In our present work we report, four transition metal complexes of Ni(II), Pd(II), Pt(II) and Ru(II) with an asymmetrical ditertiaryphosphine ligand. The synthesized ligand bears a less electronegative substituent such as methyl group on the aromatic nucleus hence makes it a strong ${\sigma}$-donor to form stable complexes and thus could effectively used in catalytic reactions. The complexes have been completely characterized by elemental analyses, FTIR, $^1HNMR$, $^{31}PNMR$ and FAB Mass Spectrometry methods. Based on the spectroscopic evidences it has been confirmed that Ni(II), Pd(II) and Pt(II) complexes with the ditertiaryphosphine ligand showed cis whereas the Ru(II) complex showed trans geometry in their molecular structure.

새로운 합성 펩티드에 대한 펩신 작용 1. Benzyloxycarbonyl-glycyl-L-tyrosyl-L-phenylalanyl-glycine 과 그의 에틸에스테르에 대한 펩신 작용 (Pepsin Action on the New Synthetic Peptides 1. Pepsin action on benzyloxycarbonyl-glycyl-L-tyrosyl-L-phenylalanyl-glycine and its ethyl ester)

  • 윤주억;신홍대
    • 대한화학회지
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    • 제13권3호
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    • pp.233-240
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    • 1969
  • The synthesis is described of new pepsin substrates of benzyloxycarbonyl-glycyl-L-tyrosyl-L-phenylalanyl-glycine ethyl ester and benzyloxycarbonyl-glycyl-L-tyrosyl-L-phenylalanyl-glycine for studies on the specificity of pepsin, and thin layer chromatographic examination of the peptides prepared showed the new substrates are homogeneous and also, same examination of the incubation mixtures showed that two synthetic substrates are cleaved by pepsin at the L-tyrosyl-L-phenylalanyl bond and hydrolysis of these substrates by pepsin is achieved without transpeptidation. It is found that synthetic peptides are moderately soluble with the amount of the substrate up to a concentration of 0.7 mM in aqueous sodium citrate buffers (0.04 M) in the pH range 1.8-4.0, thus obviating the necessity for the adding of an organic solvent in the assay mixture. The kinetic parameters for synthetic substrates are tabulated in the following table. The data in the table indicate that the susceptibility of synthetic peptides to peptic hydrolysis are relatively large and the change of the carboxyl-terminal group of synthetic substrate from glycine ethyl ester to glycine causes a small decrease in the susceptibility of the L-tyrosyl-L-phenylalanyl bond.

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Effect of the Environmental Conditions on the Structure and Distribution of Pacific Saury in the Tsushima Warm Current Region

  • Gong, Yeong;Suh, Young-Sang
    • 한국환경과학회지
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    • 제12권11호
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    • pp.1137-1144
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    • 2003
  • To provide evidence that the changes in oceanic environmental conditions are useful indices for predicting stock structure and distribution of the Pacific saury (Cololabis saira), the body length compositions and catch per unit fishing effort were examined in relation to the sea surface temperature(SST) anomalies in the Tsushima Warm Current(TWC) region. The size of the fish became larger(smaller) than the average in the same size category during the season of higher SST(lower SST) as opposed to the normal SST. The year-to-year changes in body size caused by the changes in the environmental conditions led the stock to be homogeneous during the period of high stock level from the late 1950s to early 1970s and in the 1990s. The changes in body size manifested by higher(lower) occurrence rates of larger (smaller) sized groups in relation to temperature anomalies suggest that the changes in the environmental conditions affect the distribution and the structure of the stock in the TWC region. Therefore, if the SST anomaly derived from satellite data is large enough in the early spring months(Mar. or Apr.), it is possible to predict whether or not sea temperature will be favorable for large sized groups of saury at normal or slightly earlier time of commencement of the fishery in spring(Apr.∼June).

국내 28개 국공립대학교의 연구성과에 대한 평가 (Evaluation of research performances for 28 national universities)

  • 정동빈
    • Journal of the Korean Data and Information Science Society
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    • 제25권6호
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    • pp.1241-1251
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    • 2014
  • 국내 28개 국공립대학교를 대상으로 대학정보공시제에 근거하여 제시된 교육지표 중 연구성과에 관련된 4개의 양적평가 우량성속성 (1인당 연구비 수혜금액, 1인당 연구재단등재지 (KCI) 실적, 1인당 SCI/SCOUP급 실적, 1인당 저역서 실적)에 대해, 유사한 속성을 지닌 대학들을 유사성있는 군집끼리 분류 및 세분화하고 다차원 공간상에 시각적으로 배치시켰다. 이를 통해서 국내 28개 국공립대학은 4개 군집으로 유형화가 가능하며, 각 군집간 또는 군집내에 속한 대학들 간의 유형 및 특성을 평가할 수 있다.

피도금 탄소재의 산처리가 무전해 동도금에 미치는 영향 (Effects of Acid Treatment of Carbon on Electroless Copper Plating)

  • 신아리;한준현
    • 한국표면공학회지
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    • 제49권3호
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    • pp.265-273
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    • 2016
  • The effects of surface modification by nitric acid on the pre-treatment of electroless copper plating were investigated. Copper was electroless-plated on the nitric acid treated graphite activated by a two-step pre-treatment process (sensitization + activation). The chemical state and relative quantities of the various surface species were determined by X-ray photoelectron spectroscopy (XPS) after nitric acid modification or pre-treatment. The acid treatment increased the surface roughness of the graphite due to deep and fine pores and introduced the oxygen-containing functional groups (-COOH and O-C=O) on the surface of graphite. In the pre-treatment step, the high roughness and many functional groups on the nitric acid treated graphite promoted the adsorption of Sn and Pd ions, leading to the uniform adsorption of catalyst ($Pd^0$) for Cu deposition. In the early stage of electroless plating, a lot of tiny copper particles were formed on the whole surface of acid treated graphite and then homogeneous copper film with low variation in thickness was formed after 30 min.

불안에 대한 운동요법 중 요가, 기공, 태극권 연구 고찰: 2009년부터 2015년까지 국내학술지 논문을 중심으로 (The Review Study on Yoga, Qigong, and Taichi Interventions for Anxiety: Based on Korean Journal Articles from 2009 to 2015)

  • 안영준;조상호;이승환;임정화
    • 동의신경정신과학회지
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    • 제27권1호
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    • pp.23-31
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    • 2016
  • Objectives: This study was performed to investigate the research trends of physical activities interventions such as yoga, taichi, and qigong to reduce anxiety. Methods: Korean databases were searched for articles related to survey of physical activity interventions (yoga, taichi, qigong) to reduce anxiety from 2009 to 2015. Results: Fifteen articles published in Korean journals from 2009 to 2015 were retrieved. The quality of studies were generally low and characteristics of subject were not homogeneous. Spielberger State Trait Anxiety Inventory (STAI) was used most frequently as an assessment tool. The included publications included 9 articles on yoga, 4 articles on qigong, and 2 articles on taichi. Of these, 8 of 9 articles on yoga, 2 of 4 articles on qigong, and 2 of 2 articles on taichi reported that intervention group showed statistically significant decrease of anxiety symptoms. Conclusions: In this study, physical activity interventions such as yoga, taichi and qigong might be beneficial for reducing anxiety. However, more scientifically designed research on physical activity- based treatments are needed to prove the efficacy and effectiveness.

AZ91 마그네슘 합금에서 노냉으로 생성된 불연속 석출물의 미세조직 특징 (Microstructural Feature of Discontinuous Precipitates Formed by Furnace Cooling in AZ91 Magnesium Alloy)

  • 전중환
    • 열처리공학회지
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    • 제31권5호
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    • pp.231-236
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    • 2018
  • The purpose of this study was to investigate the microstructural characteristics and hardness distribution of AZ91 magnesium alloy furnace-cooled to room temperature after solution treatment, and to compare the results with those of as-cast condition. The as-cast alloy showed a partially divorced eutectic ${\beta}(Mg_{17}Al_{12})$ phase and discontinuous precipitates (DPs) with a lamellar morphology, while only DPs were observed in the furnace-cooled alloy. The DPs in the furnace-cooled AZ91 alloy had various apparent interlamellar spacings, which would be ascribed to the different transformation temperatures during the furnace cooling. The average hardness for the furnace-cooled alloy is similar to that for the as-cast alloy. It is interesting to note that the hardness values of the furnace-cooled alloy were distributed over a narrower range than those of the as-cast alloy. This is likely to be caused by the relatively more homogeneous microstructure of the furnace-cooled alloy in comparison with the ascast one.