• 제목/요약/키워드: Homogeneous Grain

검색결과 162건 처리시간 0.033초

MgO가 첨가된 $(Ba_{0.5}Sr_{0.5})TiO_3$ 후막의 유전특성 (Dielectric properties of MgO doped $(Ba_{0.5}Sr_{0.5})TiO_3$ thick films)

  • 강원석;남성필;이성갑;배선기;이영희
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 C
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    • pp.1353-1354
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    • 2006
  • The dielectric properties of $Ba_{0.5}Sr_{0.5}TiO_3$(BST) and MgO-doped BST ceramics were investigated for tunable microwave applications by sol-gel method. The effects of MgO mixing with BST. It is observed that Mg substitution into BST causes a shift in the cubic-tetragonal BST Phase transition peak to a lower temperature. MgO-substituted BST and MgO-mixed phases exhibit homogeneous and broadened BST phase transition peaks. Mg substitution into BST has a significant effect on the grain sife reduction. Dielectric constant and loss is inhanced with decrease MgO dopant.

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기계적 합금화한 W-Cu 복합분말 소결체의 열물성 평가 (The Evaluation of Thermal Properties for W-Cu Composite Sintered from Mechanically Alloyed Powders)

  • 오낭렴;김대건;석명진;김영환;김영도;문인형
    • 한국분말재료학회지
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    • 제7권3호
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    • pp.154-160
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    • 2000
  • In order to enhance sinterability of W-Cu composites used for heat sink materials, mechanical alloying process where both homogeneous mixing of component powders and fine dispersion of minor phase can be easily attained was employed. Nanostructured W-Cu powders prepared by mechanical alloying showed W grain size ranged of 20-50 nm and were able to be efficiently sintered owing to the fine particle size as well as uniform distribution of Cu phase. The thermal properties such as electrical resistivity, coefficient of thermal expansion and thermal conductivity were evaluated as functions of temperature and Cu content. It was found that the coefficient of thermal expansion could be controlled by changing Cu content. The measured electrical resistivities and thermal diffusivities were also varied with Cu content. The thermal conductivities calculated from the values of resistivities and diffusivities showed similar tendency as a function of temperatures. However, this is in contradiction with thermal conductivities of pure W and Cu which decrease with increasing temperature.

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Photoluminescence of the Mn-doped ZnGa₂O₄ Phosphors Prepared by Coprecipitation of Metal Salts

  • 고중곤;박희동;김동표
    • Bulletin of the Korean Chemical Society
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    • 제20권9호
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    • pp.1035-1039
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    • 1999
  • Manganese-activated zincgallate (Zn1-xMnxGa2O4) phosphor as a green phosphor was readily prepared by coprecipitation in aqueous basic solution of metal salts. The obtained product converted to amorphous zincgallate even at 300℃, followed by crystallization at 1000 ℃. The pyrolyzed phosphor showed fine particle, then reduction treatment at 900 ℃ changed into homogeneous shape with slight grain growth(particle size less than 0.5 mm). The photoluminescence characteristics of the zincgallates have been investigated as a function of dopant concentrations, reducing atmospheres and temperatures. Under UV excitation the phosphors displayed the highest green emission efficiency at 504 nm when the specimen oxidized at 1000 ℃ was reduced at 900 ℃ in a mild hydrogen atmosphere (97% N2, 3% H2) with a flow rate of 100 ml/min.

동해남부해역과 울릉분지의 퇴적상과 퇴적작용 (Sedimentary Facies and Processes in the Ulleung Basin and Southern East Sea)

  • 이병관;김석윤
    • 한국수산과학회지
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    • 제40권3호
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    • pp.160-166
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    • 2007
  • The coarse deposit with a lower mud content adjacent to the shelf of the southern East Sea is probably a "relict" sediment deposited in response to a lower stand of sea level during the Pleistocene. The sediment that developed on the slope and in the deep sea was river-borne primarily and was secondarily reworked or redistributed by the Tsushima Warm Current from the East China Sea. The clay mineralogy of the area suggests various sources of fine-grained sediment from adjacent rivers, the Korea Strait, volcanic material from Ulleung Island, and the Japan coast. Massive sand, bioturbated mud, homogeneous mud, and laminated mud were the dominant facies found in the core sediments from the study area. The massive sand was mainly volcanic ash from an eruption on Ulleung Island (9300 yr BP) and consisted of colorless pumiceous glass and a black scoriaceous type. The sedimentation rates on the slope, based on the Ulleung-Oki ash layer, were about 10cm/ky higher than in the basin. Other than the coarse-grain sediment, the mean size of the fine sediment dominating the bioturbated and homogeneous muds in the basin and the laminated mud on the slope was 6-10 phi. This indicates a difference in the major sedimentary process: hemipelagic sedimentation in the Ulleung Basin and mass flow deposition, such as turbidite, on the slope of the southern East Sea.

열간 압연한 AZ31 마그네슘합금 판재의 미세조직 발달에 관한 연구 (A Study on Microstructural Evolution of Hot Rolled AZ31 Magnesium Alloy Sheets)

  • 김수현;임창동;유봉선;서영명;정인상
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2004년도 제5회 압연심포지엄 신 시장 개척을 위한 압연기술
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    • pp.63-71
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    • 2004
  • Recently, a sheet forming process of Mg alloys is highlighted again due to increasing demand for Mg wrought alloys in the applications of casings of mobile electronics and outer-skins of light-weight transportation. Microstructure control is essential for the enhancement of workability and formability of Mg alloy sheets. In this research, AZ31 Mg alloy sheets were prepared by hot rolling process and the rolling condition dependency of the microstructure and texture evolution was studied by employing a conventional rolling mill as well as an asymmetric rolling mill. When rolled through multiple passes with a small reduction per pass, fine-grained and homogeneous microstructure evolved by repetitive dynamic and static recrystallization. With higher rolling temperature, dynamic recrystallization was initiated in lower reduction. However with increasing reduction per pass, deformation was locallized in band-like regions, which provided favorable nucleation sites f3r dynamic recrystallization. Through post annealing process, the microstructures could be transformed to more equiaxed and homogeneous grain structures. Textures of the rolled sheets were characterized by $\{0002\}$ basal plane textures and retained even after post annealing. On the other hand, asymmetrically rolled and subsequently annealed sheets exhibited unique annealing texture, where $\{0002\}$ orientation was rotated to some extent to the rolling direction and its intensity was reduced.

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Effects of Powder Property and Sintering Atmosphere on the Properties of Burnable Absorber Fuel : I. $UO_2-Gd_2O_3$ Fuel

  • K. W. Song;Kim, K. S.;H. S. Yoo;Kim, J. H.
    • 한국원자력학회:학술대회논문집
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    • 한국원자력학회 1997년도 춘계학술발표회논문집(2)
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    • pp.171-176
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    • 1997
  • UO$_2$-Gd$_2$O$_3$fuel has been sintered to study the effect of powder property and sintering atmospheres on densification and microstructure. Three types of powders have been used; AUC-UO$_2$ powder and ADU-UO$_2$ powder were mixed with Gd$_2$O$_3$ Powder, and co-milled AUC-UO$_2$ and Gd$_2$O$_3$ powder. UO$_2$-(2, 5, 10)wt% Gd$_2$O$_3$pellets have been sintered at 168$0^{\circ}C$ for 4 hours in the mixture of H$_2$ and $CO_2$ gases, of which oxygen potential has been controlled by the ratio of $CO_2$ to H$_2$ gas. Densities of UO$_2$-Gd$_2$O$_3$ fuel pellets are quite dependent on powder types, and UO$_2$-Gd$_2$O$_3$ fuel using co-milled UO$_2$ powder yields the highest density. A long range homogeneity of Gd is determined by powder mixing. As the oxygen potential of sintered atmosphere increases, the sintered densities of UO$_2$-Gd$_2$O$_3$ pellets decrease but grain size increases. In addition, (U, Gd)O$_2$ solid solution becomes more homogeneous. The UO$_2$-Gd$_2$O$_3$fuel having adequate density and homogeneous microstructure can be fabricated by co-milling powder and by high oxygen potential.

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유전 알고리즘을 이용한 다중프로세서 시스템에서의 선형 스케쥴링 알고리즘 구현 (An Implementation of the Linear Scheduling Algorithm in Multiprocessor Systems using Genetic Algorithms)

  • 배성환;최상방
    • 한국정보과학회논문지:시스템및이론
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    • 제27권2호
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    • pp.135-148
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    • 2000
  • 본 논문에서는 유전 알고리즘을 이용하여 다중프로세서 시스템을 위한 선형 스케쥴링 알고리즘을 제안하였다. 일반적으로 유전 알고리즘은 초기세대를 임의로 생성하기 때문에, 문제에 적합하지 않은 개체들의 영향으로 긴 천이시간과 느린 수렴속도를 갖는다. 제안된 알고리즘은 프로세서간의 통신비용을 고려하며, 초기세대를 생성할 때 현재 노드를 기준으로 직접 후임노드만을 동일 프로세서에 할당함으로써 선형 스케쥴링을 하게 되고, 교배연산과 변이연산에서도 기준 노드의 직접 전임노드나 직접 후임노드의 결합을 변화시킴으로써 선형성을 유지하게 된다. 선형 스케쥴링은 비선형에 비해 프로그램의 병렬성을 최대한 활용할 수 있을 뿐 아니라, 코오스 그레인(coarse grain) 방향성 비순환 그래프(directed acyclic graph: DAG)에서 항상 우수한 스케쥴ㄹㅇ 결과를 생성한다. 본 논문의 목적은 유전 알고리즘의 실시간 사용 가능성에 중점을 두었으며, 시뮬레이션 결과 제안된 알고리즘은 대부분의 DAG에서 50세대 내의 빠른 수렴속도를 나타내었다.

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Fabrication and Electrical Properties of PZT/BFO Multilayer Thin Films

  • Jo, Seo-Hyeon;Nam, Sung-Pil;Lee, Sung-Gap;Lee, Seung-Hwan;Lee, Young-Hie;Kim, Young-Gon
    • Transactions on Electrical and Electronic Materials
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    • 제12권5호
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    • pp.193-196
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    • 2011
  • Lead zirconate titanate (PZT)/ bismuth ferrite (BFO) multilayer thin films have been fabricated by the spin-coating method on Pt(200 nm)/Ti(10 nm)/$SiO_2$(100 nm)/p-Si(100) substrates using $BiFeO_3$ and $Pb(Zr_{0.52}Ti_{0.48})O_3$ metal alkoxide solutions. The PZT/BFO multilayer thin films show a uniform and void-free grain structure, and the grain size is smaller than that of PZT single films. The reason for this is assumed to be that the lower BFO layers play an important role as a nucleation site or seed layer for the formation of homogeneous and uniform upper PZT layers. The dielectric constant and dielectric losses decreased with increasing number of coatings, and the six-layer PZT/BFO thin film has good properties of 162 (dielectric constant) and 0.017 (dielectric losses) at 1 kHz. The remnant polarization and coercive field of three-layer PZT/BFO thin films were 13.86 ${\mu}C/cm^2$ and 37 kV/cm respectively.

SPS법을 이용한 CuZnAl계 형상기억합금의 제조 (Manufacturing of Cu-Zn-Al shape memory alloy using spark plasma sintering)

  • 박노진;이인성;조경식;김성진
    • 한국결정성장학회지
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    • 제12권4호
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    • pp.172-177
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    • 2002
  • CuZnAl계 형상기억합금은 경제성, 열간 가공성 등이 우수하며 변태온도의 조절이 쉬운 등 여러 장점을 가지고 있으나, 열간 가공 중에 결정립이 쉽게 커지며, 취성이 심하고, 열이력에 대해서 형상기억 효과가 빨리 감소되는 등의 단점이 있다. 이러한 단점들은 결정립크기를 미세화함으로써 어느 정도 해소할 수 있다고 알려져 있다. 본 연구에서는 Cu-24.78Zn-9.11Al(at.%)과 Cu-13.22Zn-17.24Al(at.%)의 조성을 갖으며 비교적 작은 결정립크기를 갖는 형상기억합금을 99.9% 이상의 순도를 갖는 Cu, Zn 및 Al원소분말을 이용하여 SPS(spark plasma sintering) 방법으로 제조하였다. SPS 공정을 통하여 원소분말을 이용한 합금화가 가능함을 확인하였으며, 75-150 $\mu \textrm{m}$ 크기의 원소분말을 이용하여 제조한 경우, 두 조성 모두에서 약 70$\mu$m 의 결정립크기를 얻을 수 있었으며, 조성에 따라 상온에서 오스테나이트 단상 혹은 마르텐사이트 단상을 나타냄을 확인하였다.

Sinterability of Low-Cost 3Y-ZrO2 Powder and Mechanical Properties of the Sintered Body

  • Kim, Min-Sung;Go, Shin-Il;Kim, Jin-Myung;Park, Young-Jo;Kim, Ha-Neul;Ko, Jae-Woong;Jung, Seung-Hwa;Kim, Jae-Yuk;Yun, Jon-Do
    • 한국세라믹학회지
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    • 제54권4호
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    • pp.285-291
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    • 2017
  • This study investigated the effects of grain size and phase constitution on the mechanical properties of $3Y-ZrO_2$ by varying the sintering conditions. The raw powder prepared by a low-cost wet milling using the coarse solid oxide powders was sintered by both pressureless sintering and hot-pressing, respectively. As increasing holding time at $1450^{\circ}C$ for pressureless sintering, it promoted the microstructural coarsening of matrix grains and the phase transformation to tetragonal phase, whereas the bimodal microstructure embedded with abnormal $cubic-ZrO_2$ grains was observed regardless of sintering time. On the other hand, the specimens hot-pressed at $1300^{\circ}C$ for 2 h reached ~ 97% of relative density with homogeneous fine microstructure and mixed phase constitution. It was found that the proportion of untransformed monoclinic zirconia had the most adverse effect on the biaxial strength compared to the impacts of grain size and density. The pressureless sintering of the low-cost powder for prolonged sintering time to 8 h led to a decent combination of mechanical properties ($H_V=13.2GPa$, $K_{IC}=8.16MPa{\cdot}m^{1/2}$, ${\sigma}=981MPa$).