• Title/Summary/Keyword: High-temperature compression test

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Microstructure and High Temperature Deformation Behavior of Heat Resistant Stainless Steel for a Retort (열환원반응관용 내열강의 미세조직과 고온변형거동)

  • Choi, G.S.;Ha, T.K.
    • Transactions of Materials Processing
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    • v.22 no.3
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    • pp.165-170
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    • 2013
  • High temperature deformation behavior of a heat-resistant duplex stainless steel, used as a retort in the Pidgeon process for Mg production, was investigated in this study. 25Cr-8Ni based duplex stainless steels were cast into rectangular ingots, with dimensions of $350mm{\times}350mm{\times}100mm$. Nitrogen and yttrium were added at 0.3wt.% each to enhance the heat-resistance of the steel. Phase equilibrium was calculated using the thermodynamic software FactSage$^{(R)}$ and the database of FSStel. For comparison, cast 310S steel, a widely used heat-resistant austenitic stainless steel, was also examined in this study. Dilatometry was conducted on the as-cast ingots for the temperature range from RT to $1200^{\circ}C$ and the thermal expansion coefficients were evaluated. The nitrogen addition was found to have an effect on the thermal expansion behavior for temperatures between 800 and $1000^{\circ}C$. High temperature tensile and compression tests were conducted on the ingots for temperatures ranging from 900 to $1230^{\circ}C$, which is the operation temperature employed in Mg production by the Silico-thermic reduction process. The steel containing both N and Y showed much higher strength as compared to 310S.

Room and High Temperature Deformation Behaviors and Estimation on Formability of Zr-based Bulk Metallic Glass Composite (Zr-Nb-Cu-Ni-Al 비정질 복합 재료의 변형거동과 성형성)

  • Jun, H.J.;Lee, K.S.;Kuhn, U.;Eckert, J.;Chang, Y.W.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.199-202
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    • 2008
  • In this study, we investigated the thermal properties of $Zr_{66.4}Nb_{6.4}Cu_{10.5}Ni_{8.7}Al_{8.0}$ by using a differential scanning calorimeter (DSC), and then analyzed the composition of dendrite phase by using X-ray diffraction (XRD). A series of uniaxial compression tests has been performed under the strain rates between $10^{-5}/s$ and $10^{-2}/s$ at room temperature and near SLR. This BMGC has higher high temperature strength than other Zr-based monolithic BMGs because in-situ formed crystalline phases hinder a feasible viscous flow of amorphous matrix. Warm formability is also estimated by laboratory-scale extrusion test within supercooled liquid region. It was found that BMGC has poor formability compared with nother Zr-based bulk metallic glass composite presumably due to large volume fraction of 'brittle' crystalline phases distributed within amorphous matrix.

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Study of Material Properties of High Strength Microalloyed Steel for Cold Forming by Controlled Rolling and Cooling Technology (제어압연.제어냉각기술로 제조된 냉간성형용 비조질강의 소재특성)

  • Kim, N.G.;Park, S.D.;Kim, B.O.;An, J.Y.;Choi, H.J.
    • Transactions of Materials Processing
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    • v.15 no.8 s.89
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    • pp.603-608
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    • 2006
  • The main purpose of the present study has been placed on investigating the mechanical properties and microstructures of C-Si-Mn-V steels for cold forming manufactured by controlled rolling and cooling technology. The steels were manufactured in electric arc furnace (EAF) and casted to $160{\times}160mm$ billet. The billets were reheated in walking beam furnace and rolled to coil, the stocks were rolled by Controlled Rolling and Cooling Technology (CRCT), so rolled at low temperature by water spraying applied in rolling stage and acceleratly cooled before coiling. Rolled coils were cold drawed to the degree of 16%, 27% of area reduction respectively without heat treatment. Microstructual observation, tensile test, compression test and charpy impact tests were conducted. The mechanical properties of the steels were changed by area reduction of cold drawing and it is founded that there are optimum level of cold drawing to minimize compression stress for these steels. From the result of this study, it is conformed that $80kg_{f}/mm^{2},\;90kg_{f}/mm^{2}$ grade high strength microalloyed steel for cold forming are developed by accelerated cooling and optimum cold drawing.

Development of a 1.8T HTS Insert Coil for High Field Magnet (고자장 자석용 1.8T HTS insert 코일 개발)

  • Bae, Joon-Han;Seong, Ki-Chul
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.6
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    • pp.1035-1038
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    • 2007
  • We designed and manufactured a 1.8T high temperature superconducting(HTS) insert coil for a NMR magnet operated at 4.2 K. Suitable HTS superconductor and HTS coil were carefully designed and developed. We have selected multi-filamentary Bi2223 conductor fabricated by American Superconductor Corporation(AMSC). The selected conductor consists of Bi2223 filaments of 55, silver stabilizer and stainless steel reinforcement tapes. Therefore, it shows good hoop strength as well as compression tolerance. The conductor has a tape cross-section of 0.31mm x 4.8mm. the Bi2223 conductor shows large anisotropy of critical current. The critical current of conductor in magnetic field parallel to the flat surface are much higher than that in magnetic field perpendicular. The HTS coil has an inner diameter of 78 mm, an outer diameter of 127 mm and a coil length of 600 mm. In this paper, the detailed design, fabrication and test results on the HTS insert coil are presented.

Effect of Elevated Temperature on Mechanical Properties of Limestone, Quartzite and Granite Concrete

  • Tufail, Muhammad;Shahzada, Khan;Gencturk, Bora;Wei, Jianqiang
    • International Journal of Concrete Structures and Materials
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    • v.11 no.1
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    • pp.17-28
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    • 2017
  • Although concrete is a noncombustible material, high temperatures such as those experienced during a fire have a negative effect on the mechanical properties. This paper studies the effect of elevated temperatures on the mechanical properties of limestone, quartzite and granite concrete. Samples from three different concrete mixes with limestone, quartzite and granite coarse aggregates were prepared. The test samples were subjected to temperatures ranging from 25 to $650^{\circ}C$ for a duration of 2 h. Mechanical properties of concrete including the compressive and tensile strength, modulus of elasticity, and ultimate strain in compression were obtained. Effects of temperature on resistance to degradation, thermal expansion and phase compositions of the aggregates were investigated. The results indicated that the mechanical properties of concrete are largely affected from elevated temperatures and the type of coarse aggregate used. The compressive and split tensile strength, and modulus of elasticity decreased with increasing temperature, while the ultimate strain in compression increased. Concrete made of granite coarse aggregate showed higher mechanical properties at all temperatures, followed by quartzite and limestone concretes. In addition to decomposition of cement paste, the imparity in thermal expansion behavior between cement paste and aggregates, and degradation and phase decomposition (and/or transition) of aggregates under high temperature were considered as main factors impacting the mechanical properties of concrete. The novelty of this research stems from the fact that three different aggregate types are comparatively evaluated, mechanisms are systemically analyzed, and empirical relationships are established to predict the residual compressive and tensile strength, elastic modulus, and ultimate compressive strain for concretes subjected to high temperatures.

Effect of Microstructure on the High Deformation Stability of Incoloy 825 Alloy (Incoloy 825 합금의 고온 변형 안정성에 미치는 미세조직의 영향)

  • Kang, Chang-Yong;Kim, Seong-Hwi;Park, Young-Tae
    • Journal of Power System Engineering
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    • v.21 no.2
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    • pp.20-26
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    • 2017
  • This study was carried out to investigate the effect of precipitate on the high temperature deformation stability of incoloy 825 alloy. $Cr_{23}C_6$ carbide was precipitated under $950^{\circ}C$, but was not detected over $1,000^{\circ}C$. Most of the precipitation consist of $Cr_{23}C_6$ carbide. Strain-rate sensitivity was the highest in 0.01/s and the lowest in 10/s. Strain-rate sensitivity was decreased sharply below $950^{\circ}C$. In the temperature between $850^{\circ}C{\sim}1,150^{\circ}C$, plastic instable area did not exist. It showed the lowest Ziegler Parameter value of 0.06 Ziegler Parameter was the lowest as 0.06 at $850^{\circ}C$ with 10s-1 of strain. The highest Ziegler Parameter value(0.43) was found in plastic deformation at $1,050^{\circ}C$ with 0.01s-1 of strain. It tends to have an higher resistance to the high temperature deformation under $950^{\circ}C$, due to the precipitation.

High Temperature Deformation Behavior of SiCp/2124Al Metal Matrix Composites

  • Tian, Y.Z.;Cha, Seung I.;Hong, Soon H.
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.05a
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    • pp.69-72
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    • 2002
  • The high temperature deformation behavior of SiCp/2124Al composite and 2124Al alloy was investigated by hot compression test in a temperature ranged $400~475^{\circ}C$ over a strain rate ranged $10^{-3}~1s^{-1}$. The billets of 2124Al alloy and SiCp/2124Al composite were fabricated by vacuum hot pressing process. The stress-strain curve during high temperature deformation exhibited a peak stress, and then the flow stress decreased gradually into a steady state stress with increasing the strain. It was found that the flow-softening behavior was attributed to the dynamic recovery, local dynamic recrystallization and dynamic precipitation during the deformation. The precipitation phases were identified as S' and S by TEM diffraction pattern. Base on the TEM inspection, the relationship between the Z-H parameter and subgrain size was found based on the experiment data. The dependence of flow stress on temperature and strain rate could be formulated well by a hyperbolic-sinusoidal relationship using the Zener-Hollomon parameter.

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A Basic Study on Borehole Breakout under Room Temperature and High Temperature True Triaxial Compression (상온 및 고온 하 진삼축압축실험을 이용한 시추공의 파괴 거동 기초 연구)

  • Yoon, Jeonghwan;Min, Ki-Bok;Park, Eui-Seob;Jung, Yong-Bok
    • Tunnel and Underground Space
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    • v.30 no.6
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    • pp.559-572
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    • 2020
  • This paper performs laboratory experiments for borehole stability considering temperature and true triaxial stress condition, and observes a thermo-mechanical behavior of the rock under stress and temperature conditions of deep underground. China yellow sandstone and Hwangdeung granite specimens were used to perform a true triaxial compression test. Mechanical tests were carried out under nine confining pressure conditions, and thermo-mechanical tests using granite samples were carried out under six confining pressure conditions at 60-100℃. In the mechanical tests, maximum principal stress at borehole breakout was proportional to intermediate principal stress. In the thermo-mechanical tests, it was confirmed that thermal stress is added to the stress field of the borehole with the increase in temperature, resulting in additional breakout progress. To analyze the results of the laboratory experiment, Mogi-Coulomb failure criterion was used. The results of traditional triaxial compression test on cylindrical specimens and borehole breakout under true triaxial compressions matched well with Mogi-Coulomb failure criterion.

A Study on Buckling Strengths for Steel Compression Members at High Temperatures (고온 강구조 압축재의 좌굴 강도에 관한 연구)

  • Choi, Hyun-Sik
    • Journal of Korean Association for Spatial Structures
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    • v.19 no.2
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    • pp.73-81
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    • 2019
  • The high-temperature properties of mild steels were studied by comparing the test results of Kwon and the yield strength, tangent modulus predicted by the design provisions of ASCE and Eurocode(EC3). The column strengths for steel members at high temperatures were determined by the elastic and inelastic buckling strengths according to elevated temperatures. The material properties at high temperatures should be used in the strength evaluations of high temperature members. The buckling strengths obtained from the AISC, EC3 and approximate formula proposed by Takagi et al. were compared with ones calculated by the material nonlinear analysis using the EC3 material model. The newly simplified formulas for yield stress, tangent modulus, proportional limit and buckling strength which were proposed through a comparative study of the material properties and buckling strengths. The buckling strengths of proposed formulas were approximately equivalent to ones obtained from the formulas of Takagi et al. within 4%. They were corresponded to the lower bound values among the buckling strengths calculated by the design formulas and inelastic buckling analysis.

Finite Element Analysis of H-Shaped Compressive Member Exposed High Temperatures (고온에 노출된 H-형강 압축재의 유한요소해석)

  • Lee, Swoo-Heon;Lee, Hee-Du;Choi, Jun-Ho;Shin, Kyung-Jae
    • Fire Science and Engineering
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    • v.30 no.5
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    • pp.54-59
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    • 2016
  • Steel is a structural material that is inherently noncombustible. On the other hand, it has high thermal conductivity and the strength and stiffness of the material are reduced significantly when exposed to fire or high temperatures. Because the yield strength and modulus of elasticity of steel are reduced by 70% at $350^{\circ}C$ and less than 50% at $600^{\circ}C$, the load-carrying capacity of steel structure at high temperature rapidly lose. To be accepted as a fire-resisting construction, the fire test should be performed at the certificate authority. On the other hand, the fire test on a full-scale structure is limited by time, space, and high-cost. The analytical method was verified by a comparison with the fire test of H-section columns under compression and thermal analysis based on a finite element method using the ABAQUS program, and the numerical analysis method reported in this study was suggested as a complement of an actual fire test.