• 한국세라믹학회지
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• 제43권9호
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• pp.527-531
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• 2006

In order to study the influence of post-annealing treatment on the frequency characteristics of the Li doped ZnO(Li:ZnO) FBAR(Film Bulk Acoustic Resonator) device, we investigated the material and electrical properties of Li:ZnO films in the annealing temperature range from 300 to $500^{\circ}C$. In our samples, as annealing temperature was increased, Li:ZnO films showed the improvement of high c-axis orientation and resistance value with relieved stress and low surface roughness. In addition to, the return loss in the frequency property of fabricated FBAR was improved by annealing treatment from 24.9 to 29.8dB. From experimental results, the optimum post-annealing temperature for FBAR is $500^{\circ}C$ and it can obtain excellent Li:ZnO FBAR performance with stronger c-axis orientation, smoother surface, relieved stress, and lower loss factor.

• 한국분말재료학회지
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• 제22권2호
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• pp.111-115
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• 2015

This study investigates the microstructure and thermal shock properties of polycrystalline diamond compact (PDC) produced by the high-temperature, high-pressure (HPHT) process. The diamond used for the investigation features a $12{\sim}22{\mu}m$- and $8{\sim}16{\mu}m$-sized main particles, and $1{\sim}2{\mu}m$-sized filler particles. The filler particle ratio is adjusted up to 5~31% to produce a mixed particle, and then the tap density is measured. The measurement finds that as the filler particle ratio increases, the tap density value continuously increases, but at 23% or greater, it reduces by a small margin. The mixed particle described above undergoes an HPHT sintering process. Observation of PDC microstructures reveals that the filler particle ratio with high tap density value increases direct bonding among diamond particles, Co distribution becomes even, and the Co and W fraction also decreases. The produced PDC undergoes thermal shock tests with two temperature conditions of 820 and 830, and the results reveals that PDC with smaller filler particle ratio and low tap density value easily produces cracks, while PDC with high tap density value that contributes in increased direct bonding along with the higher diamond content results in improved thermal shock properties.

• 한국지반공학회논문집
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• 제22권8호
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• pp.99-106
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• 2006

본 연구는 액상화에 대한 고로 수쇄슬래그의 잠재수경성의 영향을 명확히 조사하기 위해 고로 수쇄슬래그를 고온알칼리 수(수산화칼슘 첨가, pH=12, 수온 약 $80^{\circ}C$)로 양생한 후에 반복 및 정적 삼축압축시험을 실시하였다. 삼축시험을 통해 얻어진 결과는 일본의 표준사인 Toyoura sand와 천연사인 Genkai sand의 결과와 비교하였다. 시험결과 고로수쇄슬래그의 액상화 강도는 양생기간의 증가와 더불어 잠재수경성에 의한 경화에 의해 증가함을 알았다. 또한, 담수조건에서 189일간 양생한 상대밀도 50%및 80%의 고로 수쇄슬래그에서 잠재수경성의 발현에 의해 점착력이 나타난다. 더욱이 경화과정에 있어서 고로 수쇄슬래그의 액상화 강도는 반복전단횟수 n=20회에서의 반복응력비 $R_{20}$과 점착력 $C_{d}$사이에 선형 관계가 관찰되었다. 또한, 고온 알칼리 수로 양생된 고로 수쇄슬래그에 대한 액상화 강도는 점착력이나 일축압축강도에 의해 예측이 가능함을 알았다.

• 분석과학
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• 제13권6호
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• pp.775-780
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• 2000

고온에서 용융된 유리의 전기 전도도를 측정하였다. 유리의 전기 전도도는 유리의 물성 연구와 유리 제조 공정에서 공정 조건을 조절하기 위하여 중요하게 사용되는 용융물의 물리적 성질이다. 그러나 고온의 용융물은 수용액에서 사용하는 전도도 셀을 사용할 수 없기 때문에 고온의 전도도를 직접 측정할 수 있는 백금 도가니와 막대로 구성된 전도도 셀을 구성하고 유리 용융액의 전도도를 측정하였다. 전도도 셀의 상수를 구하기 위하여 융융 유리와 전도도가 유사하도록 KCl의 수용액을 사용하였다. 교류 1 kHz의 사인파 발생기와 연산증폭기로 구성된 회로를 사용하고 용액의 전도도에 따른 출력 전위를 측정하여 전기 전도도와 셀 상수를 구하였으며, 고온에서 사용하기에 적합한 전도도 셀 형태를 결정하였다. 측정하는 Cell의 크기와 용기의 크기, Cell이 들어가는 깊이, 전극의 형태를 달리하여 측정한 결과를 비교하였다. 시험 측정한 붕규산염 유리의 고온 용융물의 전기 전도도는 $1,450^{\circ}C$에서 $0.053{\Omega}^{-1}cm^{-1}$이었다.

• 한국재료학회지
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• 제18권5호
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• pp.266-271
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• 2008

Magnesium alloys are alloyed with rare earth elements (Re, Ca, Sr) due to the limited use of magnesium in high-temperature conditions. In this study, the influences of Zr and Zn on the aging behavior of a Mg-Nd-Y alloy were investigated. magnesium alloys containing R.E elements require aging treatments Specifically, Nd, Y and Zr are commonly used for high-temperature magnesium alloys. Various aging treatments were conducted at temperatures of 200, 250 and $300^{\circ}C$ for 0.5, 1, 3, 6, and 10 hours in order to examine the microstructural changes and mechanical properties at a high temperature ($150^{\circ}C$). Hardness and high-temperature ($150^{\circ}C$) tensile tests were carried out under various aging conditions in order to investigate the effects of an aging treatment on the mechanical properties of a Mg-3.05Nd-2.06Y-1.13Zr-0.34Zn alloy. The maximum hardness was 67Hv; this was achieved after aging at $250^{\circ}C$ for 3 hours. The maximum tensile, yield strength and elongation at $150^{\circ}C$ were 237MPa, 145MPa and 13.6%, respectively, at $250^{\circ}C$ for 3 hours. The strengths of the Mg-3.05Nd-2.06Y-1.13Zr-0.34Zn alloy increased as the aging time increased to 3 hours at $250^{\circ}C$ This is attributed to the precipitation of a Nd-rich phase, a Zr-rich phase and $Mg_3Y_2Zn_3$.

• Journal of Electrical Engineering and Technology
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• 제7권5호
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• pp.765-771
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• 2012

$SF_6$ gas has been used as arc quenching and insulating medium for high and extra high voltage switching devices due to its high dielectric strength, its excellent arc-quenching capabilities, its high chemical stability and non toxicity. Despite of its significant contributions, the gas was classified as one of the greenhouse gas in the Kyoto Protocol. Thus, many researches are conducted to find out the replacement materials and to develop the $SF_6$ gas useless electrical equipment. This paper describes experiments on the temperature change-related breakdown characteristics of $SF_6$ gas ($SF_6$) and $SF_6$ liquid ($LSF_6$) in a model GIS(Gas-Insulated Switchgear) chamber in order to show the possibility of more stable and safe usages of $SF_6$ gas. The breakdown characteristics are classified into three stages, namely the gas stage of $SF_6$ according to Paschen's law, the coexisting stage of $SF_6$ gas with liquid in considerable deviation at lower temperature, and the stage of $LSF_6$ and remaining air. The result shows that the ability of the $LSF_6$ insulation is higher than the high-pressurized $SF_6$. Moreover, it reveals that the breakdown characteristics of $LSF_6$ are produced by bubble-formed $LSF_6$ evaporation and bubbles caused by high electric emission and the corona. In addition, the property of dielectric breakdown of $LSF_6$ is determined by electrode form, electrode arrangement, bubble formation and movement, arc extinguishing capacity of the media, difficulty in corona formation, and the distance between electrodes. The bubble formation and flow separation phenomena were identified for $LSF_6$. It provides fundamental data not only for $SF_6$ gas useless equipment but also for electric insulation design of high-temperature superconductor and cryogenic equipment machinery, which will be developed in future studies.

• Fibers and Polymers
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• 제6권1호
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• pp.35-41
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• 2005

Research and development of nano fiber products is very active over the world. Physical characteristics and dyeing properties of nylon 66 nano fiber were investigated in this study. X-ray diffraction, DSC, analysis of amino end group, and water absorption were performed to get information concerning physical properties of nano fiber. Nylon 66 nano fiber was dyed with high molecular mass acid dyes. Effects of dyeing temperature, pH of dyeing solution, and concentration of acid dyes on dyeing properties such as rate of dyeing and the extent of exhaustion, were examined and compared to those of regu­lar fiber. It was found that nano fiber adsorbed acid dyes at lower temperature, got rapidly dyed, and its extents of exhaustion at specific dyeing temperature were higher than regular fiber. It was also observed that nano fiber could adsorb a large amount of acid dye without a significant loss in the extent of exhaustion. Washing fastness of the dyed nano fiber was lower by $1/2\~1$ grade, light fastness by 1 grade than the dyed regular fiber.

• Journal of Advanced Marine Engineering and Technology
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• 제33권6호
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• pp.860-866
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• 2009

It is very important to choose optimal material having good corrosion resistance and capabilities for the part materials such as the automotive exhaust system under a hot salt corrosion atmosphere. Generally, two types of corrosion come into the automotive exhaust system. One is 'Condensate Corrosion', which is occurred by exhaust gas condensate formed at the inner surface of exhaust system heated up during driving, which results in the acid condensate pitting. The other is 'High Temperature Salt Corrosion' occurring from the interaction between the chloride ion coming from salt at the seaside district or snow salt and the outer surface of exhaust system. By the corrosion attack, the main muffler is firstly damaged and the life cycle of an automobile is significantly decreased. It has been investigated that the hot salt corrosion properties of a STS 409L and 436L ferritic stainless steels which are well-known for the materials of the automotive exhaust system. In addition, the corrosion properties of hot dip aluminum coated STS 409L have been compared with uncoated steels. Aluminum coated STS 409L showed a superior corrosion resistance than uncoated STS 409L, and futhermore showed a better corrosion resistance than a STS 436L, which is an expensive ferritic stainless steel having a excellent corrosion resistance caused from more chromium content of an alloying element.

• 대한치과기공학회지
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• 제28권1호
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• pp.27-41
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• 2006

The physical property and phase transformation in a commercial dental casting high gold alloy was investigated as a function of ageing temperature and time using microvickers hardness tester, X-ray diffraction, optical and electron microscopy and EPMA analyser. 1. With increasing ageing time, the hardness of solution-treated gold alloys increased slowly at the initial stage of ageing treatment at an ageing temperature of $300{\sim}400^{\circ}C$, and it reached a maximum value of hardness at the medium stage. Finally, it decreased gradually during further ageing. The maximum value of hardness at was similar with that of the conventional materials and suitable for using as the crown & bridge. 2. During isothermal ageing at a temperature range of $300{\sim}400^{\circ}C$, three phases consisting of the Au-rich ${\alpha}_1$phase with a face-centered cubic structure, the Pt3Zn ${\alpha}_2$phase with an ordered AuCu3(L12) type(f.c.c.) and the Pt-rich ${\alpha}_3$phase with face-centered cubic structure in solution-treated gold alloys were transformed into different three phases consisting of the ${\alpha}_1$phase, the ${\alpha}_3$phase and the PtZn $\beta$phase with an ordered AuCu I(L10) type. 3. The hardening of gold alloys was attributed to the lattice strains of the matrix resulting from the transformation of the ${\alpha}_2$phase to the $\beta$phase. 4. The softening of gold alloys during over-ageing was attributed to the coarsening of the nodules consisting of the $\beta$phase and ${\alpha}_1$matrix.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2020년도 봄 학술논문 발표대회
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• pp.132-133
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• 2020

The aim of this study is to evaluate the combination effect of amorphous steel fiber and polypropylene fiber on spalling of the 150MPa level ultra high strength concrete. Considering spalling has a great relationship with water vapor pressure, this paper is focusing on water vapor pressure. The test specimens were heated accordance with ISO-834 Standard Curve using electric heating furnace, the depth of 10mm water vapor pressure formation was tend to get faster and spalling damage become severe when the mixing proportion of amorphous steel fiber increase. When using ultra high strength concrete reinforced with amorphous steel fiber, further research about proper mixing proportion of polypropylene fiber.