• Journal of the Korean Society for Heat Treatment
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• v.12 no.4
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• pp.327-337
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• 1999

A series of Ni-Cr-Mo alloy steels were austenitized, quenched to martensite, and tempered at various temperature and time conditions. Tensile testing was conducted at room temperature with cylindrical specimens, and hardness was measured using Rockwell hardness tester. In the tempering stage I, high strain hardening and yield strength accounted for the high ultimate strength and hardness. In the tempering stage II, strengths and hardness linearly decreased with increasing tempering temperature. Specimens tempered in the temperin stage III showed incipient discontinuous yielding and tensile strengths only slightly higher than yield strengths. Ductilities decreased slightly in specimens tempered in the tempered martensite embrittlement range, and severely decreased in specimens tempered for 10 hours at $500^{\circ}C$ in the temper embrittlement range. Specimens tempered at $600^{\circ}C$ for 10 hours showed recrystallized microstructures, a number of fine dimples, and increased strain hardening, probably due to the precipitation of alloy carbides. The simple formulae for the mechanical properties of these steels were suggested as a function of carbon content and Hollomon-Jaffe tempering parameter.

• Korean Journal of Poultry Science
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• v.17 no.2
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• pp.127-133
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• 1990

This study was undertaken to find out the effect of heating time and temperature, pH and NaCl concentration on the heat stability of egg albumen gel during heat treatment. With the transient decrease at 110-$130^{\circ}C$, hardness of heat-set albumen gel was increased as the heating temperature increased. The cohesiveness showed similar trend as well. The lightness was decreased while the yellowness was increased as the heating time and temperature increased. Heat-set albumen gel showed maximum hardness at pH 4.5-5.0 and pH 9.0 High heat treatment($120^{\circ}C$, 30min) showed higher hardness at alkaline range compared to low heat treatment($96^{\circ}C$, 30min.). Color of the albumen gel was relatively dark at acidic range and bright at alkaline range. High heat treatment caused darker albumen gel at alkaline range and brighter albumen gel at acidic range. The addition of NaCl increased hardness and cohesiveness of the albumen gel and improved the lightness after high heat treatment regardless of NaCl concentration.

• Archives of Metallurgy and Materials
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• v.66 no.4
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• pp.971-975
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• 2021

This study investigates the effects of grain boundary structures on mechanical properties of nanocrystalline Al-0.7Mg-1.0Cu alloy using nanoindentation system. Grain boundary structure transforms to high angle grain boundaries from low angle ones with increase of heat treatment temperature and the transformation temperature is about 400℃. Young's modulus and hardness are higher in sample with low angle grain boundaries, while creep length is larger in sample with high angle ones. These results indicate that progress of plastic deformation at room temperature is more difficult in sample with low angle ones. During compression test at 200℃, strain softening occurs in all samples. However, yield strength in sample with low angle grain boundaries is higher twice than that with high angle ones due to higher activation energy for grain boundary sliding.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.5
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• pp.261-269
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• 2023

This study aims to investigate the effects of tungsten additions on the microstructure, corrosion characteristics, and hardness of super duplex stainless steel heat-treated at two different annealing temperatures. Under the annealing temperature of 1100℃, the microstructure of the stainless steels consisted mainly of ferrite, while under the annealing temperature of 1000℃, significant amounts of austenite and secondary phases were also observed. In terms of corrosion characteristics in 3.5 wt%NaCl solution, there was not a significant difference due to W addition at the 1100℃ conditions. However, at the 1000℃, a tendency of decreased corrosion resistance was observed with increasing the tungsten content. On the other hand, the micro-hardness of the stainless steel heat-treated 1000℃ showed an increasing trend with tungsten addition. This increase can be mainly attributed to the higher fraction of secondary phases, primarily sigma, known for their high hardness.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.362-365
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• 2009

Microstructural evolution and the mechanical properties of various carbon steels were investigated with the variation deformation temperature to explore the optimum microstructure with excellent combination of strength and ductility. For this purpose, three carbon steels containing different carbon contents were deformed using Gleeble 3500 at temperatures including austenitic, austenitic/ferritic, austenitic/cementitic, ferritic/cementitic regions. The results showed that in the medium and high carbon steels, cementite particles became finer with decreasing deformation temperature resulting higher hardness but lower ductility. Further effort is needed to find out optimum microstructures with enhanced mechanical properties.

• Nuclear Engineering and Technology
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• v.55 no.4
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• pp.1468-1475
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• 2023

Enhancement of wear resistance of components used in fast reactors is necessary for long service life of the components. Plasma nitriding is a promising surface modification technology to impart high hardness and improved wear resistance of various steel components. This study discusses the characterization of chrome nitrided SS316L casing ring used in secondary sodium pump of fast breeder reactor and its stability under long term sodium exposure. Microstructural and hardness analysis showed that stress relieved component could be chrome nitrided successfully to a thickness of about 100 ㎛. Assessment of in-sodium performance of the chrome nitrided casing ring subjected to long term exposure up to 5000h at 550℃, showed retention of chrome nitrided layer with a case depth almost similar to that before sodium exposure. A slight decrease in the hardness was observed due to prolonged high temperature sodium exposure. Tribological studies indicate very low coefficient of friction indicating the retention of good wear resistance of the coating even after long term sodium exposure.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.105-110
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• 2001

It has recently been raised main issue how solve the problem of insufficient energy. One of the solution is to increase the thermal efficiency of power generation system. For the purpose of high efficiency, it is necessary to increase the steam temperature and pressure. So, the use of modified $9{\sim}12%Cr$ steel having superior creep rupture strength and oxidation resistance is required to endure such severe environment. The evaluation of creep properties of those heat resistance material is very important to secure the reliability of high temperature and pressure structural components. Since creep properties are determined by microstructural change such as carbide precipitation and coarsening, It is certain that there are some relationship between creep properties and hardness affected by microstructure. In this study, SP-Creep ruptured test for newly developed 9Cr steel being used as boiler valve material was performed, and creep properties of the material were evaluated. Also, hardness test were performed and hardness results were related to the creep properties such as LMP and creep strength to verify the availability of SP-Creep test as creep test method.

• Toxicological Research
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• v.33 no.2
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• pp.119-124
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• 2017

Hexavalent chromium is a bio accumulative toxic metal in water and fish. It enters aquaculture ponds mainly through anthropogenic sources. Hexavalent chromium concentrations and its effects on the morphology and behavior of Clarias gariepinus were investigated from four aquaculture ponds for 12 weeks. Chromium was measured using diphenyl carbohdrazide method; alkalinity and hardness were measured using colometric method and analyzed with Bench Photometer. Temperature and pH were measured using pH/EC/TDS/Temp combined tester. Temporal and spatial replications of samples were done with triplicates morphological and behavioural effects of the metal on fish were observed visually. Chromium ranged from no detection to 0.05 mg/L, alkalinity 105 to 245 mg/L, hardness 80 to 165 mg/L, pH 6.35 to 8.03 and temperature 29.1 to $35.9^{\circ}C$. Trend in the chromium concentrations in the ponds is natural > earthen > concrete > collapsible. There was a significant difference (P < 0.05) in chromium, alkalinity, water hardness, pH and temperature among the four ponds. Significant positive correlation also existed between alkalinity, water hardness, pH, with chromium. Morphological and behavioural changes observed in the fish include irregular swimming, frequent coming to the surface, dark body colouration, mucous secretion on the body, erosion of gill epithelium, fin disintegration, abdominal distension and lethargy. High chromium concentration in natural pond was due to anthropogenic run-off of materials in to the pond. Acidic pH, low alkalinity, low water hardness also contributed to the high chromium concentration. Morphological and behavioural changes observed were attributed to the high concentrations, toxicity and bio accumulative effect of the metal. Toxicity of chromium to fish in aquaculture could threaten food security. Watershed best management practices and remediation could be adopted to reduce the effects of toxicity of chromium on pond water quality, fish flesh quality and fish welfare.

• Korean Journal of Metals and Materials
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• v.46 no.9
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• pp.593-603
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• 2008

In this study, effects of alloying elements on the sticking occurring during hot rolling of five kinds of ferritic STS430J1L stainless steels were investigated by analyzing high-temperature hardness and oxidation behavior of the rolled steels. Hot-rolling simulation tests were conducted by a high-temperature wear tester which could simulate actual hot rolling. The simulation test results revealed that the sticking process proceeded with three stages, i.e., nucleation, growth, and saturation. Since the hardness continuously decreased as the test temperature increased, whereas the formation of Fe-Cr oxides in the rolled steel surface region increased, the sticking of five stainless steels was evaluated by considering both the high-temperature hardness and oxidation effects. The addition of Zr, Cu, or Si had a beneficial effect on the sticking resistance, while the Ni addition did not show any difference in the sticking. Particularly in the case of the Si addition, Si oxides formed first in the initial stage of high-temperature oxidation, worked as initiation sites for Fe-Cr oxides, accelerated the formation of Fe-Cr oxides, and thus raised the sticking resistance by about 10 times in comparison with the steel without Si content.

• Journal of the Korean Society for Heat Treatment
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• v.4 no.1
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• pp.1-12
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• 1991

This study has been performed to find out the effect of austenitizing temperature, austempering temperature and its holding time, and tempering cycle on the mechanical properties such as impact resistance, hardness etc. of AISI $M_2$ Mo series high speed tool steel austempered or tempered after austempering treatment. The results obtained from the experiment are as follows ; (1) Optical micrograph has revealed that the transformation rate of bainite is delayed as the austenitizing temperature increases and that bainite is most apparently transformed at an austempering temperature of $290^{\circ}C$. (2) The amount of retained austenite during austempering has been analysed to be increased by the X-ray diffraction technique as the transformation product of bainite is increased. It has also been shown that the longer the holding time of austempering, the more the transformation quantity of bainite is formed, exhibiting, however, that the rate of bainitic transformation is considerably retarded after a certain period of holding time elapses. (3) Hardness measurement has shown that hardness values obtained after austempering increase with decreasing the amount of retained austenite. (4) The austempering and then tempering cycle has been formed to give hardness values which are more greatly improved as austenitizing temperature is increased. (5) The mechanical property of the specimen primary-tempered for 1 hour at $550^{\circ}C$ after austempering for 2 hours at $290^{\circ}C$ from the austenitizing temperature range of $1180^{\circ}C$ to $1210^{\circ}C$ have been estimated to be good values.