• The Journal of Advanced Prosthodontics
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• 제12권5호
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• pp.265-272
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• 2020

PURPOSE. The aims of this study were to investigate mechanical properties and hydrothermal degradation behaviour of the cubic-containing translucent yttrium oxide stabilized tetragonal zirconia polycrystal (Y-TZP). MATERIALS AND METHODS. Four groups of Y-TZP (T, ST, XT, and P), containing different amount of cubic crystal, were examined. Specimens were aged by autoclaving at 122℃ under 2 bar pressure for 8 h. Phase transformation was analyzed using X-ray diffraction (XRD) to measure phase transformation (t→m). Kruskal-Wallis test was used to determine the difference. Surface hardness, biaxial flexural strength, and fracture toughness in values among the experimental groups and verified with Wilcoxon matched pairs test for hardness values and Mann Whitney U for flexural strength and fracture toughness. RESULTS. XRD analysis showed no monoclinic phase in XT and P after aging. Only Group T showed statistically significant decreases in hardness after aging. Hydrothermal aging showed a significant decrease in flexural strength and fracture toughness in group T and ST, while group XT and P showed no effect of aging on fractural strength and fracture toughness with P<.05. CONCLUSION. Hydrothermal aging caused reduction in mechanical properties such as surface hardness, biaxial flexural strength, and fracture toughness of Y-TZP zirconia. However, cubic-containing zirconia (more than 30% by volume of cubic crystal) was assumed to have high resistance to hydrothermal degradation. Clinical significance: Cubic-containing zirconia could withstand the intraoral aging condition. It could be suggested to use as a material for fabrication of esthetic dental restoration.

• 대한기계학회논문집A
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• 제21권3호
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• pp.519-527
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• 1997

AISI 316 steel has been used extensively for heater and boiler tube of the structural plants such as power, chemical and petroleum plants under severe operating conditions. Usually, material degradation due to microcrack or precipitation of carbides and segregation of impurity elements, is occured by damage accumulated for long-term service at high temperature in this material. In this study, the effect of aging time on fracture toughness was investigated to evaluate the measurement of material degradation. The elastic-plastic fracture toughness behaviour of AISI 316 steel pipe aged at $550^{\circ}C$for 1h-10000h (the aged material) was characterized using the single specimen J-R curve technique and eletric potential drop method at normal loading rate(load-line displacement speed of 0.2mm/min) in room temperature and air environment. The fracture toughness data from above experiments is compared with the $J_{in}$ obtained from predicted values of crack initiation point using potential drop method.

• Restorative Dentistry and Endodontics
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• 제23권2호
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• pp.690-700
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• 1998

Rubber-toughened particles which are used in the field of chemical engineering are used to increase the fracture toughness of thermoset resin. The application of Core-Shell particles, one of rubber-toughened particles, as a filler for dental composite or restoration have not been examined. The purpose of this study was to evaluate possible use of Core-Shell particles for dental composite, and the hypothesis was that additional toughening mechanisms are activated by the addition of Core-Shell particles. After blending 50vol% quartz with Bis-GMA/TEGDMA resin matrix, the experimental resins were made by the addition of Core-Shell particles with varied content level as 0, 2.5, 5, 7.5, 10, 12.5, 15, and 20wt%. Fracture toughness was determined on three-point bending specimen with single-edge notch according to ASTM-E 399. Also, flexural properties, that is, strength and modulus were measured by three-point bending testing. Fractogragh of fracture toughness specimen was observed using SEM (JEOL 6400 SEM, MA). The following results from this study were obtained ; 1. Fracture toughness of composite resin added 2.5wt% Core-Shell particles was significantly higher than control group ($p{\leq}0.05$). 2. Flexural properties were decreased with increasing Core-Shell particle content, which showed a correlation statistically ($p{\leq}0.05$). 3. A toughening mechanism such as lamination and microcrack was observed in specimen determined high fracture toughness. 4. The dispersion of Core-Shell itself and quartz filler particles was limited present high content of Core-Shell particles, which decreased a resulting mechanical properties of composites. These results suggest that adequate Core-Shell particles can be used to enhance mechanical properties included toughening for dental composites.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2002년도 추계학술대회 논문집
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• pp.373-378
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• 2002

Metal matrix composites have a great interest in recent years because high specific strength, high specific stiffness characteristics, and application ranges of the composites are extend to variety industry. In this paper, an investigation was performed on the plane strain fracture toughness and slinding wear properties of AC4CH alloy(Al-Si-Mg line) reinforced with 20wt% aluminum borate whisker expect one, which contained a inorganic binder($TiO_2$). the binder led to the formation of strengthen the whisker each other. The test of fracture toughness was using CT(half size) specimen of thickness 12.5mm, width 25mm. and test of slinding wear of using tribo a pin-on-disk machine and lubricant is used without paraffine 8.2CST at room temperature. As results, Fracture toughness $K_{IC}$ is $8.7MPa-m^{05}$ for ABOw/AC4CH, $9.28MPa-m^{05}$ for ABOw/AC4CH added $TiO_2$. but AC4CH alloy was violated the critical stipulated by ASTM standard for valid measurement of $K_{IC}$. In case of, it was performed $J_{IC}$ test instead of $K_{IC}$ based on ASTM E 1820.

• 한국정밀공학회지
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• 제16권5호통권98호
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• pp.175-185
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• 1999

Acoustic emission(AE) measurement was carried out to evaluate the fracture behavior of high tension steel. Fracture toughness $K_{AE}$ could be determined reasonably by using the load value corresponding to an abrupt change of the accumulated AE counts AE emitted from the test specimens. AE characteristics of the base metal, the weld metal and the heat-affected zone could be distinguished using a constant value b which represented the AE amplitude distribution, Consequently the structure integrity can be evaluated by variation of the constant b at the load level. In addition it was found that AE signals due to crack growth have high amplitude but low rise time and duration.

• 열처리공학회지
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• 제36권4호
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• pp.206-214
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• 2023

Tungsten carbide has many industrial applications due to its high electrical and thermal conductivity, high melting temperature, high hardness and good chemical stability. Because tungsten carbide is difficult to sinter, it is sintered with nickel or cobalt as a binder and is currently used in nozzles, cutting tools, and molds. Alumina is reported to be a viable binder for tungsten carbide due to its higher oxidation resistance and lower cost than nickel and cobalt. The ultrafine tungsten carbide-graphene-alumina composites were rapidly sintered in a high frequency induction heating active sintering unit. The microstructure and mechanical properties (fracture toughness and hardness) of the composites were investigated and analyzed by Vickers hardness tester and electron microscope. Since the high-frequency induction heating sintering method enables high-speed sintering, ultrafine composites can be prepared by preventing grain growth. In the tungsten carbide-graphene-alumina composites, the grain size of tungsten carbide increased with the amount of alumina participation. The hardness and fracture toughness of the tungsten carbide-5% graphene- x% alumina (x = 0, 5, 10,15) composites were 5.1, 8.6, 8.6, and 8.4 MPa-m^1/2 and 2384, 2168, 2165, and 2102 kg/mm², respectively. The fracture toughness increased without a significant decrease in hardness. Sinterability was improved by adding alumina to tungsten carbide-graphene.

• Journal of Welding and Joining
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• 제33권1호
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• pp.35-40
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• 2015

Recently, there have been the increase of ship size and the development of oil and gas in arctic region. These trends have led to the requirements such as high strength, good toughness at low temperature and good weldability for prevent of brittle fracture at service temperature. There has been the key issue of crack arrestability in large size structure such as container ship. In this report for the first time, crack arrest toughness of thick steel plate welds was evaluated by large scale ESSO test for estimate of brittle crack arrestability in thick steel plate. For large structures using thick steel plates, fracture toughness of welded joint is an important factor to obtain structural integrity. In general, there are two kinds of design concepts based on fracture toughness: crack initiation and crack arrest. So far, when steel structures such as buildings, bridges and ships were manufactured using thick steel plates (max. 80~100mm in thickness), they had to be designed in order to avoid crack initiation, especially in welded joint. However, crack arrest design has been considered as a second line of defense and applied to limited industries like pipelines and nuclear power plants. Although welded joint is the weakest part to brittle fracture, there are few results to investigate crack arrest toughness of welded joint. In this study, brittle crack arrest designs were developed for hatch side coaming of large container ships using arrest weld, hole, and insert technology.

• Computers and Concrete
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• 제2권3호
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• pp.239-248
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• 2005

The article presents the results of examination of the fractal dimension D of concrete specimen fracture surfaces obtained in fracture toughness tests. The concretes were made from three different types of coarse aggregate: gravel, dolomite and basalt aggregate. Ordinary concretes (C40) and high-performance concretes (HPC) were subjected to testing after 7, 14, 28 and 90 days of curing, respectively. In fracture toughness and compressive tests, different behaviours of concretes were found, depending on the type of aggregate and class of concrete (C40, HPC). A significant increase in the strength parameters tested occurred also after a period of 28 days (up to the $90^{th}$ day of curing) and was particularly large for concretes C40. Fractal examinations performed on fracture replicas showed that the fractal dimension D was diverse, depending on the coarse aggregate type and concrete class being, however, statistically constant after 7 and 14 days for respective concretes during curing. The fractal dimension D was the greater, the worse strength properties were possessed by the concrete. A cross-grain crack propagation occurred in that case, due to weak cohesion forces at the coarse aggregate/mortar interface. A similar effect was observed for C40 and HPC made from the same aggregate. A greater dimension D was exhibited by concretes C40, in which case the fracture was easier to form compared with high-performance concretes, where, as a result of high aggregate/mortar cohesion forces, the crack propagation was of inter-granular type, and the resulted fracture was flatter.

• Restorative Dentistry and Endodontics
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• 제35권6호
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• pp.461-472
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• 2010

연구목적: 본 연구는 미세인장결합강도와 파괴인성을 통해 복합 레진 수복물의 수리 시기와 표면 처리 방법에 따른 파괴 거동을 알아보고자 시행되었다. 연구 재료 및 방법: Short rod 시편과 composite resin specimen block을 준비하여 표면 처리 방법에 따라 none-treated, sand blasting, bur roughening 군으로 나누고 이를 다시 즉시군과 2주 지연군으로 나누어 수리했다. 결과: 미세인장결합강도와 파괴인성을 측정한 결과, 두 실험 모두에서 즉시군이 지연군보다 높은 값을 보였다. 기계적 표면 처리군이 none-treated군보다 높은 값을 보였고, sand blasting과 bur roughening 사이에 유의한 차이는 없었다. 파괴인성과 미세인장결합강도는 상관 관계가 없었다. FE-SEM을 보아 수복물의 탈락은 균열 전도와 관계가 있는 것으로 보인다. 결론: 수리된 복합 레진의 파괴 거동 평가에는 파괴인성 실험이 적합하다.

• 한국기계가공학회지
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• 제12권4호
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• pp.123-130
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• 2013

Zirconia is well known in industrial applications for its mechanical characteristics. DLC (diamond-like carbon) have high elastic modulus, high electric resistivity, high dielectric constant, high wear resistance, low friction coefficient, bio compatibility, chemically inert and thermally stable. Because of all these physical and chemical properties these types of coatings have become key procedure for thin coating. Friction coefficient of DLC films is already evaluated and the current work is a further advancement by calculating the fracture toughness and wear resistance of these coatings. In the present study DLC thin film coatings are developed on $ZrO_2$ alloy surface using Plasma Enhanced Chemical Vapor Deposition (PECVD) method. Vicker hardness test is employed and it was concluded that, DLC coatings increase the Vickers hardness of ceramics.