• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 추계학술대회 논문집
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• pp.108-111
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• 2007

It's important to measure quantitative properties about thermal-nano variation conduct of polymer for producing high quality components using NIL process. NanoScale indents can be used ad cells for molecular electronics and drug deliver, slots for integration into nanodevices, and defects for tailoring the structure and properties. In this study, it's to evaluate mechanical characteristic of polymer such as PMMA and PC at high temperature for manufacture of nano/micro size of polymer using indenter at high temperature. At high temperature mechanical properties of polymer have extreme variation. Because heating the polymer, it becomes softer than room temperature. In this case it is especially important to study for mechanical properties of polymer at high temperature.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2003년도 춘계학술대회논문집
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• pp.23-26
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• 2003

This paper explains the die cooling method for improving tool life in the hot forging process. In continuous forming operation such as hot forging process, performed at high speeds, temperature increases of several hundred degrees may be involved. Die hardness was reduced due to thermal softening. Factor of die fracture are wear and plastic deformation of die due to hardness reduction by high temperature. Because die service life was reduced due to this phenomenon during hot forging, quantified data for optimal die cooling method is required. The new developed techniques for predicting tool life applied to estimate the production quantity for a spindle component and these techniques can be applied to improve the tool life in hot forging process

• 한국분말재료학회지
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• 제4권3호
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• pp.222-229
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• 1997

A P/M high speed steel of ASP 30 grade was austenitized, gas quenched and tempered at various conditional. The mechanical properties such as hardness, bend strength and fracture toughness were evaluated after heat treatment. The microstructure and the type and volume fraction of carbides were analyzed by an optical microscope, image analyzer and XRD. The primary carbides after the heat treatment were MC and $M_6C$ type. The volume of the total carbide varied from 10 to 15% depending on the austenitizing and tempering temperature. The tempering temperature for maximum hardness was at around 52$0^{\circ}C$. But the maximum bend strength was obtained at about 55$0^{\circ}C$. The fracture toughness was largely affected by the presence of retained austenite after gas quenching and secondary hardening during tempering.

• International Journal of Advanced Culture Technology
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• 제7권4호
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• pp.260-267
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• 2019

Harvested de-astringent persimmon 'Fuyu' were treated with various lighting sources under low (3℃) and high (22℃) temperatures. The weight loss rate of fruits was lower in those with Red LED than Fluorescence and Blue LED under both temperature conditions. Hardness and soluble solid content of fruits were higher in those with 3℃ / Blue LED or mixed LED (Blue+Red LEDs). Beta-carotene and lycopene content of fruit peel were higher in those with 3℃ than 22℃ and with Red LED or light sources with mixed red wavelength under both temperatures. When the fruits treated with light and temperature were stored for 4 days under 3℃ / dark condition, the hardness of the fruits did not significant difference among the treatments. Taken together all the results, it would be best to treat it light sources mixed red wavelength under 3℃.

• 한국표면공학회지
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• 제50권6호
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• pp.492-497
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• 2017

In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

• 한국세라믹학회지
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• 제50권1호
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• pp.37-42
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• 2013

Tristructural-isotropic (TRISO)-coated particles were fabricated by a fluidized-bed chemical vapor deposition (FBCVD) method for use in a very high temperature gas-cooled reactor (VHTR). ZrC as a constituent layer of TRISO coating layers was deposited by a chloride process using $ZrCl_4$ and $CH_4$ source gases in a temperature range of $1400^{\circ}C$ and $1550^{\circ}C$. The change in the microstructure of ZrC depending on the deposition temperature and its effect on the hardness were evaluated. As the deposition temperature increased to $1500^{\circ}C$, the grain size of the ZrC increased and the hardness of the ZrC decreased according to the Hall-Petch relationship. However, at $1550^{\circ}C$, the ZrC layer was highly non-stoichiometric and carbon-rich and did not obey the Hall-Petch relationship in spite of the decrease of the grain size. A considerable amount of pyrolytic carbon at the grain boundaries of the ZrC as well as coarse granular pyrolytic carbon were locally distributed in the ZrC layer deposited at $1550^{\circ}C$. Therefore, the hardness decreased largely due to the formation of a large amount of pyrolytic carbon in the ZrC layer.

• 한국식품과학회지
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• 제25권6호
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• pp.698-702
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• 1993

온도 증가에 따라 용출되는 soluble carbohydrate는 온도가 증가할수록 더 큰 분자들이 많이 용출되었고 동부나 녹두는 아주 유사한 용출 양상을 보였다. 그리고 팥은 동부나 녹두보다는 분자량이 작지만 강낭콩보다는 큰 분자들이 용출되었고 $95^{\circ}C$에서의 용출양상이 동부나 녹두의 $85^{\circ}C$에서의 용출양상과 비슷해지는 것을 알 수 있었다. 그러나 강낭콩은 온도가 증가되어도 아주 작은 분자들이 계속 많이 용출되어 강낭콩 아밀로오스가 작은 분자들로 이루어져 있다는 것을 시사했다. 텍스쳐실험결과 전분겔의 특성은 녹두가 가장 견고성이 크고 동부는 응집성이 가장 컸다. 팥이나 강낭콩은 견고성과 응집성 모두 동부나 녹두에 비해 낮았다. 15분간 가열하여 제조한 전분겔의 경우 가열온도가 증가할수록 견고성과 응집성이 증가하였다. 1시간 가열하여 제조한 전분겔의 경우 동부와 녹두는 $85^{\circ}C$에서보다 $95^{\circ}C$에서 견고성이 감소하였으나 팥이나 강낭콩은 가열온도 증가에 따라 견고성이 증가하였고 시료 전분겔 모두 응집성은 증가 하는 양상을 보였다.

• 동력기계공학회지
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• 제17권4호
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• pp.109-114
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• 2013

In this study, the microstructure, mechanical properties and high temperature oxidation characteristics of HiSiMo and HiSiMoM ductile iron for exhaust manifold were investigated. The HiSiMoM ductile iron was developed by optimization of alloying element addition and casting design. The exhaust manifold prototype was fabricated using the HiSiMoM iron and this resulted in the weight saving of 0.73kg. The microstructures of the HiSiMo and HiSiMoM irons were similar each other and graphite nodularity was 89% and 93% respectively. Tensile strengths of them were 663.5 and 674.4 MPa and Brinell hardness were 235.3 and 243.9 respectively. Both irons showed parabolic weight gain behavior in high temperature oxidation atmosphere. Oxidation layer was divided into external and internal layers. The weight gain of the HiSiMoM iron was lower than that of the HiSiMo iron after isothermal oxidation test at $900^{\circ}C$. This should be rationalized by higher Si enrichment at the interface of the matrix and internal layer of the HiSiMoM iron.

• Advances in materials Research
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• 제7권1호
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• pp.17-28
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• 2018

Niobium is a candidate base for new alloys devoted to applications at especially elevated temperatures. Elaborating and shaping niobium-based alloys by conventional foundry may lead to mechanically interesting microstructures. In this work a series of charges constituted of pure elements were subjected to high frequency induction melting in cold crucible to try obtaining cast highly refractory Nb-xCr and Nb-xCr-0.4 wt.%Calloys(x=27, 34 and 37 wt.%). Melting and solidification were successfully achieved. The as-cast microstructures of the obtained alloys were characterized by electron microscopy and X-ray diffraction and their hardness were specified by Vickers macro-indentation. The obtained as-cast microstructures are composed of a body centered cubic (bcc) niobium dendritic matrix and of an interdendritic eutectic compound involving the bcc Nb phase and a $NbCr_2$ Laves phase. The obtained alloys are hard to cut and particularly brittle at room temperature. Hardness is of a high level (higher than 600Hv) and is directly driven by the chromium content or the amount of {bcc Nb - $NbCr_2$} eutectic compound. Adding 0.4 wt.% of carbon did not lead to carbides but tends to increase hardness.

• 열처리공학회지
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• 제3권2호
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• pp.10-19
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• 1990

The tempering behavoirs of 0.45% carbon steel treated by automatic progressive high frequency induction hardening equipment have been investigated. In order to examine the correlation of hardness with both tempering temperature and time, simple regression analysis has been made using the statistical quality control package. The maximum surface hardness value of induction hardened zone and its effective hardening depth have been determined to be Hv 810 and 0.76mm, respectively. The hardness obtained after tempering has been shown to vary lineary with tempering time at six different temperatures. The activation energies during tempering have been calculated to be 25.34kcal/mole, 32.73kcal/mole and 49.24kcal/mole for HRcs 60, 50 and 40, respectively, showing that tempering process occurs by a complex mechanism, The tempering hardness equation of $H=90.113{\sim}4.531{\times}10^{-3}$ [T(11.996+log t)] has proved to be in a reasonably good agreement with experimently determined data and it is also expected to be useful for the determination of tempering treatment conditions to obtain a required hardness value.