• 제목/요약/키워드: High Temperature/High Pressure Spray Water

검색결과 24건 처리시간 0.02초

질산염 전구체 원료로 Ex-situ 공정에 의한 GdBCO 박막 제조 (Preparation of GdBCO Thin Film by Ex-situ Process using Nitrate Precursors)

  • 김병주;이철선;이종범;이재훈;문승현;이희균;홍계원
    • Progress in Superconductivity
    • /
    • 제13권2호
    • /
    • pp.127-132
    • /
    • 2011
  • Many research groups have been manufacturing coated conductor by various processes such as PLD, MOD, and MOCVD, but the methods with production cost suitable for wide and massive application of coated conductor did not develop yet. Spray pyrolysis method adopting ultrasonic atomization was tried as one of the possible option. GdBCO precursor films have been deposited on IBAD substrate by spray pyrolysis method at low temperature and converted to GdBCO by post heat treatment. Ultrasonic atomization was used to generate fine droplets from precursor solution of Gd, Ba, and Cu nitrate dissolved in water. Primary GdBCO films were deposited at $500^{\circ}C$ and oxygen partial pressure of 1 torr. After that, the films were converted at various temperatures and low oxygen partial pressures. C-Axis oriented films were obtained IBAD substrates at conversion temperature of around $870^{\circ}C$ and oxygen partial pressures of 500 mtorr ~ 1 torr in a vacuum. Thick c-axis epitaxial film with the thickness of 0.4 ~ 0.5 ${\mu}m$ was obtained on IBAD substrate. C-axis epitaxial GdBCO films were successfully prepared by ex-situ methods using nitrate precursors on IBAD metal substrate. Converted GdBCO films have very dense microstructures with good grain connectivity. EDS composition analysis of the film showed a number of Cu-rich phase in surface. The precursor solution having high copper concent with the composition of Gd : Ba : Cu = 1 : 2 : 4 showed the better grain connectivity and electrical conductivity.

합성가스/디젤 혼소압축착화 엔진의 합성가스 혼합비와 압축비에 따른 연소 및 배출가스 특성 (Syngas/Diesel Dual Fuel Combustion in a Compression Ignition Engine with Different Composition Ratios of Syngas and Compression Ratios)

  • 이준순;정탄;이용규;김창업;오승묵
    • 한국분무공학회지
    • /
    • 제24권1호
    • /
    • pp.35-42
    • /
    • 2019
  • Syngas is widely produced by incomplete combustion of coal, water vapor, and air (oxygen) in a high-temperature/high-pressure gasifier through a coal-gasification process for power generation. In this study, a simulation syngas which was mainly composed of $H_2$, CO, $CO_2$, and $N_2$ was fueled with diesel. A modified single cylinder compression ignition (CI) engine is equipped with intake port syngas supply system and mechanical diesel direct injection system for dual fuel combustion. Combustion and emission characteristics of the engine were investigated by applying various syngas composition ratios and compression ratios. Diesel fuel injection timing was optimized to increase indicated thermal efficiency (ITE) at the engine speed 1,800 rpm and part load net indicated mean effective pressure ($IMEP_{net}$) 2 to 5 bar. ITE of the engine increased with the $H_2$ concentration, compression ratio and engine load. With 45% of $H_2$ concentration, compression ratio 17.1 and $IMEP_{net}$ 5 bar, ITE of 41.5% was achieved, which is equivalent to that of only diesel fuel operation.

구강내에서 임플랜트 지대주 형성 시 내부연결방식과 외부연결방식간의 열전달 효과 비교 (THE COMPARATIVE STUDY OF THERMAL INDUCTIVE EFFECT BETWEEN INTERNAL CONNECTION AND EXTERNAL CONNECTION IMPLANT IN ABUTMENT PREPARATION)

  • 허중보;고석민
    • 대한치과보철학회지
    • /
    • 제45권1호
    • /
    • pp.60-70
    • /
    • 2007
  • Statement of problem: The cement-type abutment would be needed for the reduction of its body in order to correct the axis and to assure occlusal clearance. In the case of intraoral preparation, there is a potential risk that generated heat could be transmitted into the bone-implant interface, where it can cause deterioration of tissues around the implant and failed osseointegration. Purpose: The purpose of this study was to assess the difference of the heat transmitting effect on external and internal connection implant types under various conditions. Material and method: For evaluating the effects of alternating temperature, the thermocoupling wires were attached on 3 areas of the implant fixture surface corresponding to the cervical, middle, and apex. The abutments were removed 1mm in depth horizontally with diamond burs and were polished for 30 seconds at low speed with silicone points using pressure as applied in routine clinical practice. Obtained data were analyzed using Mann-Whitney rank-sum test and Wilcoxon / Kruskal-Wallis Tests. Result: Increased temperature on bone-implant interface was evident without air-water spray coolant both at high speed reduction and low speed polishing (p<.05). But, the difference between connection types was not shown. Conclusion: The reduction procedure of abutment without using proper coolant leads to serious damage of oral tissues around the implant irrespective of external and internal connection type.

치과 교정용 자가중합형 Resin의 중합 온도 변화에 따른 굽힘 특성 (Flexural Properties according to Change of Polymerization Temperature of Autopolymerized Resin for Orthodontic)

  • 이규선
    • 치위생과학회지
    • /
    • 제15권3호
    • /
    • pp.259-264
    • /
    • 2015
  • 치과 교정용 자가중합형 레진의 중합 온도가 기계적 특성에 미치는 영향을 알아보기 위하여 폴리머와 모노머의 부피비는 2.5:1로 하고, 중합 온도를 $25^{\circ}C$, $40^{\circ}C$, $70^{\circ}C$의 세 group으로 나누었다. 실험을 위해 각 group 당 10개씩의 시편을 중합 시간 15분, 중합 압력 3 bar로 통일하여 제작하였다. 그 후 시편을 실험 전까지 $37^{\circ}C$의 증류수에 48시간 이상 보관한 다음, Intron (3344)을 이용하여 각 시편의 FS 및 EM을 측정하였다. 이렇게 하여 얻어진 값들은 SPSS ver. 16.0을 사용하여 일원 배치 분산 분석을 하였으며 Scheffe의 사후 검정을 실시하여 다음과 같은 결과를 얻었다. 치과 교정용 자가중합형 레진의 FS 평균값을 비교해 보았을 때 $25^{\circ}C$ group은 $71.500{\pm}5.546MPa$, $40^{\circ}C$ group은 $74.920{\pm}4.237MPa$, $70^{\circ}C$ group은 $76.880{\pm}4.304MPa$의 범위였으며, $25^{\circ}C$ group<$40^{\circ}C$ group<$70^{\circ}C$ group 순으로 차이가 있었으나 통계적으로 유의한 차이는 없었다(p=0.052). 치과 교정용 자가중합형 레진의 EM 평균값은 $25^{\circ}C$ group이 $2.164{\pm}0.073MPa$, $40^{\circ}C$ group은 $2.258{\pm}0.069MPa$, $70^{\circ}C$ group은 $2.282{\pm}0.147MPa$의 범위였으며, $25^{\circ}C$ group<$40^{\circ}C$ group<$70^{\circ}C$ group 순으로 중합 온도가 높을수록 유의한 차이를 보였다(p<0.039). 이상의 실험 결과로 미루어 볼 때 EM 값은 $25^{\circ}C$ group<$40^{\circ}C$ group<$^70{\circ}C$ group 순으로 통계적 유의성이 인정되는 수준의 상승이 있었던 반면, FS 값은 통계적 유의성은 보이고 있지 않으나 강도의 증가에 영향을 미치고 있으므로, 치과 교정 장치 제작 시 일정 수준의 중합 온도 상승은 장치의 기계적 물성을 증가시킬 것이라고 판단된다.