• Title/Summary/Keyword: HgS

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Experimental method and evaluation of the calibration capability for the national calibration centers using the platinum resistance temperature sensors (백금저항온도센서를 이용한 국가교정기관의 교정능력 평가 및 실험방법)

  • Gam, Kee-Sool;Yoo, Sung-Ho;Kim, Sung-Min;Lee, In-Sick
    • Journal of Sensor Science and Technology
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    • v.14 no.4
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    • pp.231-236
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    • 2005
  • Calibration capability was evaluated using the reference-grade platinum resistance thermometer (PRT) in the temperature range of $-50^{\circ}C$ to $250^{\circ}C$ for the national calibration centers. The reference-grade PRT was calibrated at the several fixed points, which was composed by the freezing points of Sn, In, the melting point of Ga and the triple point of water and Hg, before and after the round-robin test (RRT) experiments. The temperature scale of reference-grade PRT was compared to the local standard PRT's using the system of the national calibration centers. $E_{n}$ values was calculated by the temperature difference between the reference-grade PRT and the local standard PRT, and the best measurement capability. Finally, the capability of the national calibration centers was evaluated by the $E_{n}$ values.

Conservation of Lacquer-wares (수침칠기의 보존)

  • Yi, Yong-Hee;Kim, Chang-Suk;Jung, Kwang-Yong;Han, Sung-He
    • 보존과학연구
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    • s.14
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    • pp.77-93
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    • 1993
  • In order to study for the production techniques and the materials of using in Korean Lacquer Antiques, we examined the section structure by SEM and Microscope, the qualitative analysis of lacquer layer by XRF and XRD, the qualitative analysis of Golhae layer by XRF and XRD, the qualitative analysis of Golhae by EDS on the locquer-wares which was excavated from Anapchi Pond Site in Kyungju and Miruksa Temple Site in Iksan. In the lacquer-wares excavated from Anapchi Pond Site, the lacuqer-wares layers made by a cloth attached on the surface of wooden vessel and Golhae-a mixture of clay and lacquer-covered on the cloth and finally finished with the red lacqure, being mixed with pure mercury sulfide(HgS) and lacquer. And raw materials of Golhae made of clay. The lacquer-wares excavated from Miruksa Temple Site in Iksan, we presumed that the lacquer-wares used fine born grains in place of clay for the raw materials of Golhae. Expecially in case of black lacquer-tray, we found that lacquer put on the surface of wooden vessel without cloth attaching and Golhae covering and the production of wooden vessel was used power-driven machine.

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Fabrication of High Permeable Nanoporous Carbon-SiO$_2$ Membranes Derived from Siloxane-containing Polyimides

  • Kim, Youn Kook;Han, Sang Hoon;Park, Ho Bum;Lee, Young Moo
    • Korean Membrane Journal
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    • v.6 no.1
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    • pp.16-23
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    • 2004
  • The silica containing carbon (C-SiO$_2$) membranes were fabricated using poly(imide siloxane) (PIS) having -CO- swivel group. The characteristics of porous C-SiO$_2$ structures prepared by the pyrolysis of poly(imide siloxane) were related with the micro-phase separation between the imide block and the siloxane block. Furthermore, the nitrogen adsorption isotherms of the CMS and the C-SiO$_2$ membranes were investigated to define the characteristics of porous structures. The C-SiO$_2$ membranes derived from PIS showed the type IV isotherm and possessed the hysteresis loop, which was associated with the mesoporous carbon structures, while the CMS membranes derived from PI showed the type I isotherm. For the molecular sieving probe, the C-SiO$_2$ membranes pyrolyzed at 550, 600, and 700$^{\circ}C$ showed the O$_2$ permeability of 924, 1076, and 367 Barrer (1 ${\times}$ 10$\^$-10/㎤(STP)cm/$\textrm{cm}^2$$.$s$.$cmHg) and O$_2$/N$_2$ selectivity of 9, 8, and 12.

Measurement of Leg Arterial Compliance of Normal and Diabetics (정상인과 당뇨병 환자의 다리 동맥의 Compliance 측정)

  • 김덕원;김상수
    • Journal of Biomedical Engineering Research
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    • v.13 no.3
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    • pp.189-194
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    • 1992
  • As people's income and intake of animal fat rapidly increase, so does choresterol concentration in blood. Thus diseases such as non-insulin-dependent diabetes mellitus(NIDDM)myocardial infraction, high blood pressure, cerebral stroke resulting from atherosclerosis rapidly increase recently. It is very difficult to diagnose atherosclerosis early since its progress is so slow and there is no sypmtoms in the beginning of the disease. In this study a mechanical characteristic, compliance, of the lower leg arteries was measured noninvasively. Changes of blood volume and pressure were measured using impedance plethysmgraphy and mercury sphygmomanometer, respectively. The compliance was calculated by dividing the change of blood volume by the change of pulse pressure ( systolic-diastolic pressure ) . Subjects were 24 asymptomatic persons ranging (rom 30 Ic 58yeras and 14 diabetics from 41 to 59years. The compliances, mean, and systolic pressures were statistically analyzed using a t-test be- tween the healthy and diabetic groups. The average compliance of the healthy and diabetic group was measured 2.79 and 1.82U1/mmHg/cm, respectively and these were significantly different(p<0.01). It was also found that the compliance is a better parameter in differentiating the vascular disease than mean or systolic blood pressure.

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A Method to Estimate Peripheral Systolic Blood Pressure using Pulse Transit Time during Bicycle Ergometer Exercise of Healthy Korean Subjects in their Twenties

  • Lee Jeong-Chan;Eo Yun-Hye;Park Kyung-Mo;Park Seung-Hun
    • Journal of Biomedical Engineering Research
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    • v.27 no.3
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    • pp.89-93
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    • 2006
  • A simple algorithm that can be used to estimate a healthy person's blood pressure using pulse transit time is proposed in this paper. Fifty healthy students participated in the experiment that was conducted in line with the study. The subjects were asked to exercise on several exercise levels using a bicycle ergometer. Their blood pressures during the succeeding rest period were measured. A simple method was proposed to illustrate the relationship between blood pressure and pulse transit time. The systolic blood pressures as well as the heights and weights of the subjects were regarded as the proper parameters, and a second-order regression curve was produced to estimate the subjects' blood pressures. The mean error of estimation was less than 10 mmHg, which was the mean error of manual measurement. Although our estimation model is so simple, it can be used to estimate continuous blood pressure measurement for bicycle ergometer exercise. The electrocardiograms, photoplethysmograms, and blood pressures, however, could not be measured simultaneously As such, their estimation may be slightly different from the results taken from simultaneous measurements.

In-vivo Evaluation of Pneumatic Ventricular Assist Device and Durability Improvement (공압식 심실보조장치의 in-vivo 평가 및 내구성 개선)

  • 이상훈;이광호;박성식;서필원;김삼현;강봉진
    • Journal of Biomedical Engineering Research
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    • v.25 no.1
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    • pp.65-70
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    • 2004
  • In this paper, we described 23 cases of animal experiment with our pneumatic ventricular assist device and new durability-improvement method. The blood pump consists of blood housing, and back plate made by the injection molding of isoplast, and the diaphragm fabricated by dipping of polyurethane solution onto the aluminum mold. Its volume was 75 $m\ell$ and in-vitro test showed that maximum output was 4.5 $\ell$/min at the 100 mmHg. The adult female sheep with weight of 50 + 10 kg were employed for tile in-vivo experiments and the mean blood flow was sustained at 3.0 1/min. 4 animals survived more than 15 days and the longest survival time was 28 days. In the prior 10 cases, the major causes of death were the tearing of diaphragm at the diaphragm to blood housing junction. By the new mesh and alumina ball milling methods, the durability was enhanced, and its qualitative and quantitative improvement was proved via the in-vivo and in-vitro methods. Animal experiments demonstrated that all the physiologic parameters a ere maintained within the permissible ranges and no thrombus formation was observed through the visual and blood test. The in-vivo experiments demonstrated our pneumatic ventricular assist device to he one month's bridge to transplantation device.

Cloning and Characterization of a Multidomain GH10 Xylanase from Paenibacillus sp. DG-22

  • Lee, Sun Hwa;Lee, Yong-Eok
    • Journal of Microbiology and Biotechnology
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    • v.24 no.11
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    • pp.1525-1535
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    • 2014
  • The xynC gene, which encodes high molecular weight xylanase from Paenibacillus sp. DG-22, was cloned and expressed in Escherichia coli, and its nucleotide sequence was determined. The xynC gene comprised a 4,419bp open reading frame encoding 1,472 amino acid residues, including a 27 amino acid signal sequence. Sequence analysis indicated that XynC is a multidomain enzyme composed of two family 4_9 carbohydrate-binding modules (CBMs), a catalytic domain of family 10 glycosyl hydrolases, a family 9 CBM, and three S-layer homologous domains. Recombinant XynC was purified to homogeneity by heat treatment, followed by Avicel affinity chromatography. SDS-PAGE and zymogram analysis of the purified enzyme identified three active truncated xylanase species. Protein sequencing of these truncated proteins showed that all had identical N-terminal sequences. In the protein characterization, recombinant XynC exhibited optimal activity at pH 6.5 and $65^{\circ}C$ and remained stable at neutral to alkaline pH (pH 6.0-10.0). The xylanase activity of recombinant XynC was strongly inhibited by 1 mM $Cu^{2+}$ and $Hg^{2+}$, whereas it was noticeably enhanced by 10 mM dithiothreitol. The enzyme exhibited strong activity towards xylans, including beechwood xylan and arabinoxylan, whereas it showed no cellulase activity. The hydrolyzed product patterns of birchwood xylan and xylooligosaccharides by thin-layer chromatography confirmed XynC as an endoxylanase.

A Study on a Heat Transfer Characteristics of Direct Contact Heat Exchanger for Steam Condensation According to Various Cooling Water Flow and Internal Pressure(The Purpose of Combination with LNG Evaporator) (증기응축용 직접접촉식 열교환기의 냉각수 유량과 내부압 변화에 따른 열전달 특성연구(LNG 기화기와의 조합목적))

  • Lee, B.C.;Han, S.T.;Kim, C.B.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.3 no.3
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    • pp.153-160
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    • 1991
  • Heat transfer characteristics of a direct contact heat exchanger utilizing sieve trays and spray nozzles for steam condensation for the purpose of combining with a LNG evaporator have been investigated with various cooling water flow rates and different vacuum pressures within the heat exchanger for the purpose of steam condensation. Temperature profiles and the volumetric overall heat transfer coefficients in a direct contact heat exchanger have been obtained for comparisons. The results show that the temperature differences between cooling water and steam along the direct contact heat exchanger height are rapidly decreasing and the volumetric overall heat transfer coefficients of the exchanger improves greatly as the inside vacuum pressure increases. The values of the overall heat transfer coefficients at P=-680mmHg have been increased significantly compared with at atmospheric pressure. At given pressure conditions, it is found that the values of average volumetric overall heat transfer coefficients for the sieve tray are found to be approximately 10% higher than those of the spray nozzle.

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Purification and Characterization of Cellulase from the Edible Snail

  • Yoon, Kyung-Young;Kan, Mi-Jung;Lee, Kwang-Hee;Shin, Seung-Ryeul;Kim, Kwang-Soo
    • Preventive Nutrition and Food Science
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    • v.7 no.1
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    • pp.22-27
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    • 2002
  • The cellulase from internal organs of edible snails was purified by fractionation with ammonium sulfate, DEAE-Sephadex chromatography and gel filtration on Sephacryl S-200 and Superose 12 HR 10/30. The specific activity of the purified cellulase was 85.1 units/mg protein with 24.3 purification fold from crude extract. Molecular weight of the enzyme was estimated to be approximately 74,000 dalton by gel filtration chromatography and SDS-PAGE eletrophoresis. T7e isoelectric point of the enzyme was determined to be pH 4.6. The optimum temperature and pH of the enzyme were 5$0^{\circ}C$ and pH 6.0, respectively. The enzyme was stable at 30~5$0^{\circ}C$ and pH 6.0~10.0. It was activates by Mn$^{2+}$, but inhibited by Li$^{2+}$, Zn$^{2+}$, Ag$^{2+}$ and Hg$^{2+}$./TEX> 2+/.

Influence of Weft's Cotton Count & Weave Construction on the Mechanical Properties & Hand of Cotton Woven Fabrics (위사번수와 조직이 면직물의 역학특성 및 태에 미치는 영향)

  • Bae, Jin-Hwa;Park, Jung-Whan;An, Seung-Kook
    • Fashion & Textile Research Journal
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    • v.7 no.5
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    • pp.553-559
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    • 2005
  • Hand characteristics related with structural properties of fabrics have something to do with mechanical properties of fabric. In this study, the mechanical properties and hand characteristics have been analyzed according to fabric structural parameters such as the weave structure and the linear density of weft of cotton fabric. Mechanical properties have been used by KES-FB system which measures hand characteristics and mechanical properties of fabric. Linear density of weft, tensile, bending, and shear properties are decreasing with increasing weft linear density, and there is no considerable effects on compression and surface properties. In case of formability with weft linear density, B/W, 2HG/G, 2HB/B, 2HB/W, $\sqrt[3]{B/W}$, $\sqrt{2HB/W}$, W/T except MMD/SMD, WC/T, and WC/W have been effected. There is a high correlation between the crimp, tightness, hand, formability and mechanical properties specially tensile linearity, bending, shear, and compression properties. The weft crimp influences the bending rigidity, shear properties, and the tightness which have effects on the tensile linearity, bending, shear, compression properties, hand, and formability.